Method for characterizing average thickness of alpha polluted layer of cylindrical titanium-alloy sample

A technology of α-contamination layer and average thickness, which is applied in the preparation of test samples, measuring devices, and material analysis through optical means, can solve the problems of metallographic structure damage, incomplete characterization, and influence on the accuracy of results, etc., to achieve Accurately Characterized Effects

Inactive Publication Date: 2017-01-25
PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this method, titanium and titanium alloy samples are ground and dyed, and then the entire α layer is observed under a microscope, and the most serious field of view measurement result is determined to be the thickness of the α contamination layer of the sample. The sample preparation of this method must be wire cutting, and requires Grinding and dyeing are complex methods, and there is a risk of metallographic structure being destroyed during th

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0036] Example 1

[0037] Machining contains the original alpha pollution layer The M12 ZTC4 titanium alloy cylindrical tensile sample was used (WEW-600) universal testing machine to perform tensile experiment at room temperature to obtain the tensile fracture. The prepared tensile fracture was observed under the flat light source of the LeiCaM80 stereo microscope Appearance, adjust the brightness 10, the contrast 90, adjust the focal length to make the pollution layer appear white and bright, the matrix is ​​off-white, take a color photo including the entire fracture surface, see details figure 1 . Open the second phase content determination program in the Micro-imageAnalysis&process special software, load the magnification, perform threshold segmentation to extract the phase to be tested, determine the percentage content of the α-contaminated layer in the picture to be 4.3%, and deduct the background in the picture to be the α in the sample The area content of the pollution layer

Example Embodiment

[0038] Example 2

[0039] Machining contains the original alpha pollution layer The M12 ZTC4 titanium alloy cylindrical tensile sample was pickled in hydrofluoric acid and nitric acid for 20 minutes to obtain a tensile sample containing a part of the α-contaminated layer, and the (WEW-600) universal testing machine was used to perform the tensile experiment at room temperature. Stretch the fracture, observe the morphology of the fracture under the LeiCa M80 stereo microscope flat light source, adjust the brightness to 20, the contrast to 80, and adjust the focus to make the pollution layer appear white and bright, the substrate is gray and white, and the entire fracture morphology is captured. Color photos of figure 2 . Open the second phase content determination program in the Micro-image Analysis&process special software, load the magnification, and perform threshold segmentation to extract the phases to be tested, open the second phase content determination program in the Micro

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Abstract

The invention relates to a method for characterizing the average thickness of an α-contaminated layer of a cylindrical titanium alloy sample, and belongs to the technical field of metallographic structure detection. The technical problem solved by the present invention is to provide a method for measuring the average thickness of the α-contaminated layer of cylindrical titanium alloy samples. This method takes advantage of the different characteristics of the fracture surface of the α-contaminated layer and the substrate, and uses the fracture method to directly measure the area content of the α-contaminated layer without grinding and dyeing the metallographic sample. The average thickness is calculated indirectly. The invention can conveniently and comprehensively characterize the average thickness of the polluted layer. Compared with other technologies, it is more intuitive, fast, convenient, efficient and accurate, and can accurately characterize the average thickness of the polluted layer.

Description

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Claims

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Application Information

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Owner PANZHIHUA IRON & STEEL RES INST OF PANGANG GROUP
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