Protective and decorative yellow ceramic layer on magnesium alloy surface and preparation method thereof

A technology of ceramic layer and magnesium alloy, which is applied in the field of both protective and functional coatings on metal surfaces, can solve the problems of monotonous micro-arc oxidation coating color, unstable and safety hazards in the preparation process of yellow micro-arc oxidation ceramic layers, etc., and achieve enhanced Good protection performance and stability

Inactive Publication Date: 2017-05-31
XIAN TECHNOLOGICAL UNIV
View PDF6 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The technical purpose of the present invention is to provide a magnesium alloy surface with both protective and And a decorative yellow ceramic layer and a preparation method thereof, the ceramic layer has re

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Protective and decorative yellow ceramic layer on magnesium alloy surface and preparation method thereof
  • Protective and decorative yellow ceramic layer on magnesium alloy surface and preparation method thereof
  • Protective and decorative yellow ceramic layer on magnesium alloy surface and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] In this embodiment, the surface of the magnesium alloy is a light yellow micro-arc oxidation ceramic layer, that is, the micro-arc oxidation ceramic layer is prepared by adding a small amount of sodium stannate electrolyte, so that the surface layer of the magnesium alloy substrate is formed in situ. Magnesium oxide porous membrane, the thickness of the ceramic layer is 10 μm.

[0033] The preparation method of the yellow micro-arc oxidation ceramic layer on the surface of the magnesium alloy comprises the following steps:

[0034] Step 1: The wire-cut magnesium alloy samples are firstly subjected to degreasing and degreasing processes, then ground with different water sandpapers, and then washed with water after polishing to prepare for micro-arc oxidation treatment.

[0035] Step 2: Select chemical reagents according to the matching principle of magnesium alloy micro-arc oxidation electrolyte, prepare stannate-based micro-arc oxidation electrolyte, wherein the concentrat

Embodiment 2

[0039] In this example, the surface of the magnesium alloy is a yellow micro-arc oxidation ceramic layer, that is, the micro-arc oxidation ceramic layer is prepared by adding a relatively large amount of sodium stannate electrolyte, so that the surface layer of the magnesium alloy substrate is formed in situ and doped with a relatively large amount of Sn elements. MgO porous membrane, the thickness of the ceramic layer is 15 μm.

[0040] The preparation method of the yellow micro-arc oxidation ceramic layer on the surface of the magnesium alloy comprises the following steps:

[0041] Step 1: The wire-cut magnesium alloy samples are firstly subjected to degreasing and degreasing processes, then ground with different water sandpapers, and then washed with water after polishing to prepare for micro-arc oxidation treatment.

[0042] Step 2: Select chemical reagents according to the matching principle of magnesium alloy micro-arc oxidation electrolyte, prepare stannate-based micro-arc

Embodiment 3

[0046] In this embodiment, the surface of the magnesium alloy is a deep yellow micro-arc oxidation ceramic layer, that is, the micro-arc oxidation ceramic layer is prepared in the electrolyte of adding more sodium stannate, so that the surface layer of the magnesium alloy matrix is ​​formed in situ. Magnesium oxide porous membrane of Sn element, the thickness of the ceramic layer is 20 μm.

[0047] The preparation method of the yellow micro-arc oxidation ceramic layer on the surface of the magnesium alloy comprises the following steps:

[0048] Step 1: The wire-cut magnesium alloy samples are firstly subjected to degreasing and degreasing processes, then ground with different water sandpapers, and then washed with water after polishing to prepare for micro-arc oxidation treatment.

[0049] Step 2: Select chemical reagents according to the matching principle of magnesium alloy micro-arc oxidation electrolyte, prepare stannate-based micro-arc oxidation electrolyte, wherein the conc

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Thicknessaaaaaaaaaa
Current densityaaaaaaaaaa
Corrosion current densityaaaaaaaaaa
Login to view more

Abstract

The invention discloses a protective and decorative yellow ceramic layer on a magnesium alloy surface and a preparation method thereof. The protective and decorative yellow ceramic layer is formed in the way that metal elements in a coloring agent are doped with MgO; and the content of the coloring agent in a micro-arc oxidation electrolyte and electric parameters (mainly including voltage and oxidation time) are regulated and controlled to regulate and control the content of the metal elements doped in a micro-arc oxidation ceramic layer so as to form a MgO yellow micro-arc oxidation ceramic layer with controllable doping content, the doping content of the metal elements is 0.5-10 at.%, the thickness of the ceramic layer is 5-30 [mu]m, and the yellow color is deepened with increase of the doping content. Compared with an existing yellow micro-arc oxidation ceramic layer on the magnesium alloy surface, the protective and decorative yellow ceramic layer on the magnesium alloy surface has the advantages that the process problems of poor solution stability and existence of safety hazards are solved, and particularly, the dark yellow micro-arc oxidation ceramic layer has more excellent protective performance than a traditional white micro-arc oxidation ceramic layer, therefore is more suitable for industrial popularization, and can be applied in the fields of 3C and decoration.

Description

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Owner XIAN TECHNOLOGICAL UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products