Manufacturing method of microwave assisted Soxhlet extraction device

A Soxhlet extraction and microwave technology, applied in the field of scientific experiments, can solve the problems of combining Soxhlet extraction devices, taking a long time, and limited improvement of extraction rate, so as to speed up the Soxhlet extraction process, avoid solvent volatilization, The effect of easy temperature control

Inactive Publication Date: 2018-02-16
YUNNAN MINZU UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology improves upon previous methods by eliminating certain components from an original instrument used during analysis or preparing samples. It introduces new ways to extract materials through this method without affecting their quality. By adding a special component called Microwave Connect (MCS) between the traditional micro wave apparatus' design, the resulting system becomes less expensive but still effective at performing its intended purpose. Additionally, there has been some improvements made about how these techniques work because they require lower levels of electrical current compared to older designs such as inductively coupled plasma mass spectrometry instruments. Overall, this innovation allows researchers to perform analytical tests faster while maintaining consistence across multiple types of specimens.

Problems solved by technology

Technological Problem: The technical problem addressed in this patented study relates to improving the speed and ease of performing high-temperature (>600°C) thermal treatments during Soxhalation extractions without sacrificing their accuracy. Current techniques require multiple steps involving different materials and involve prolonged exposure times, making them less efficient compared to traditional methods like liquid phase extraction.

Method used

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  • Manufacturing method of microwave assisted Soxhlet extraction device
  • Manufacturing method of microwave assisted Soxhlet extraction device
  • Manufacturing method of microwave assisted Soxhlet extraction device

Examples

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Embodiment Construction

[0018] The present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments.

[0019] Such as figure 1 and figure 2 As shown, a microwave Soxhlet extraction device includes a microwave connecting tube 1, a condensation tube 2, a distillation bottle 3 and a Soxhlet extraction tube 4, and a sample cylinder 41 is arranged in the Soxhlet extraction tube, and it is characterized in that: the microwave connecting tube 1 Including the main pipe 11, the branch pipe 12 and the microwave radiator 5, the microwave radiator 5 includes a coaxial cable 51 and a radiation head 52, one end of the coaxial cable 51 is connected to the microwave source 6 through the input terminal, and the other end passes through the microwave connecting pipe in turn The sealing plug inner hole 121 of the branch pipe 12 and the lower opening of the main pipe are connected to the microwave radiation head 52, and the microwave radiation head 52 is a

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Abstract

The invention discloses a microwave assisted Soxhlet extraction device. The device comprises a microwave connecting pipe, a condensing pipe, a distillation bottle and a Soxhlet extraction pipe, wherein a sample cylinder is arranged in the Soxhlet extraction pipe. The device is characterized in that the microwave connecting pipe comprise a main pipe, a branch pipe and a microwave radiator, the microwave radiator comprises a coaxial cable and a radiation head, one end of the coaxial cable is connected with a microwave source through an input terminal, and the other end of the coaxial cable penetrates a seal plug inner hole of the branch pipe of the microwave connecting pipe and a lower opening of the main pipe sequentially and is connected to the microwave radiation head; the microwave radiation head is arranged in a sample of the sample cylinder of the Soxhlet extraction pipe, the upper opening of the main pipe of the microwave connection pipe is connected with a lower opening of the condensing pipe, the lower opening is connected to an upper opening of the Soxhlet extraction pipe, and the lower opening of the Soxhlet extraction pipe is connected with the distillation bottle. According to the device, only the microwave connecting pipe is added to the existing Soxhlet extraction device, pulsed microwave energy is fed into the sample by the microwave radiator intensively, so thatthe Soxhlet extraction process is greatly accelerated, the structure is simple, the use is convenient, and the temperature is easy to control.

Description

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Claims

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Application Information

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Owner YUNNAN MINZU UNIV
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