Visible light responded photocatalyst LiBGe3O8 and preparation method thereof

[0018] (1) The analytically pure chemical raw material Li 2 CO 3 , B 2 o 3 and GeO 2 powder of LiBGe 3 o 8 The composition weighs the ingredients.

[0019] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind, take out and dry, and pass through a 200-mesh sieve.

[0020] (3) Pre-fire the uniformly mixed powder in step (2) at 950°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then pulverize it with a ball mill to make the average particle diameter smaller than 2 μm, and then LiBGe is obtained 3 o 8 powder.

[0021] The prepared photocatalyst has a methyl orange removal rate of 97.7% in 60 minutes under the irradiation of visible light with a wavelength greater than 420nm.

[0023] (1) The analytically pure chemical raw material Li 2 CO 3 , B 2 o 3 and GeO 2 powder of LiBGe 3 o 8 The composition weighs the ingredients.

[0024] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind, take out and dry, and pass through a 200-mesh sieve.

[0025] (3) Pre-fire the uniformly mixed powder in step (2) at 980°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then pulverize it through a ball mill to make the average particle diameter smaller than 2 μm, and then LiBGe is obtained 3 o 8 powder.

[0026] The prepared photocatalyst has a methyl orange removal rate of 98.9% in 60 minutes under the irradiation of visible light with a wavelength greater than 420nm.

[0028] (1) The analytically pure chemical raw material Li 2 CO 3 , B 2 o 3 and GeO 2 powder of LiBGe 3 o 8 The composition weighs the ingredients.

[0029] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind, take out and dry, and pass through a 200-mesh sieve.

[0030] (3) Pre-fire the uniformly mixed powder in step (2) at 1000°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then pulverize it with a ball mill to make the average particle diameter smaller than 2 μm, and then LiBGe is obtained 3 o 8 powder.

[0031] The prepared photocatalyst has a methyl orange removal rate of 98.5% in 60 minutes under the irradiation of visible light with a wavelength greater than 420nm.