Continuous extraction separator

A separation device and extraction technology are applied in the direction of carboxylic acid nitrile purification/separation, extraction water/sewage treatment, liquid solution solvent extraction, etc. Less dosage, high extraction efficiency and small footprint

Inactive Publication Date: 2017-08-04
SHANGHAI APPLIED TECHNOLOGIES COLLEGE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If the stirring effect is not good, the organic phase and the aqueous phase will be separated. At this time, the extraction of acetonitrile and ethanol only occurs at the interface between the aqueous phase and the extractant, and the extraction efficiency is extremely low. Moreover, the extraction cannot be continuous. If the stirring speed is too high Fast, the solution is emulsified and not easy to separate

Method used

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Example Embodiment

[0022] The present invention will be further described below in conjunction with the drawings:

[0023] As shown in the drawings, the present invention provides a continuous extraction and separation device, specifically a device that uses a hydrophobic organic solvent to extract the organic solvent in the water phase. The device includes a spray component and an extraction guide component. 6. The cylinder assembly 9 and the extraction agent distribution assembly 15, the spray assembly, the extraction guide assembly 6, the cylinder assembly 9, and the extraction agent distribution assembly 15 are connected in sequence from top to bottom. The spray assembly is connected by the shower head 1 and the sealing The spray head 1 is connected to the top of the head 2, and the bottom of the head 2 is provided with a flange 3. The extraction and diversion assembly 6 includes a diversion sleeve one and two diversion sleeves arranged up and down. The first sleeve is connected with the second gu

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Abstract

The invention relates to a continuous extraction separator, which comprises a spray assembly, an extraction and diversion assembly, a cylinder assembly and an extractant distribution assembly, wherein the spray assembly comprises a spray head and a seal head; a flange I is arranged at the bottom of the seal head; the extraction and diversion assembly comprises a guide sleeve I and a guide sleeve II; a flange II is arranged at the top end of the guide sleeve I; the flange II is connected with the flange I; a flange III is arranged at the middle part of the guide sleeve I; the cylinder assembly comprises a cylinder I and a cylinder II; a flange IV is arranged at the top end of the cylinder I; the flange IV is connected with the flange III; a connection pipe III and a connection pipe I are arranged at the left side and the right side of the cylinder I separately; a connection pipe IV and a connection pipe II are arranged at the left side and the right side of the bottom of the cylinder II; a liquid level meter is arranged on the front side of the cylinder II; the extractant distribution assembly extends into the cylinder assembly; a plurality of through holes are distributed in two sides of the extractant distribution assembly; and a flange V is arranged at an open end. According to the continuous extraction separator, the dissolving distribution ratio of acetonitrile or ethyl alcohol in methylbenzene is improved, the floor area is small, the operation cost is low and the extraction efficiency is high.

Description

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Claims

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Application Information

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Owner SHANGHAI APPLIED TECHNOLOGIES COLLEGE
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