Method for improving specific surface area and adsorption performance of opoka

A technology of specific surface area and adsorption capacity, which is applied in the fields of non-metallic mineral processing and environmental engineering, can solve the problems of specific surface area and adsorption performance reduction and loss, and achieve the effect of pore transparency, permeability improvement and good adsorption

Active Publication Date: 2019-01-11
山西智汇创鑫科技材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are pores in a single protein soil, so it has a strong adsorption capacity. When it is used as a filter aid in industry, it is generally expanded and surface treated by roasting. On the one hand, it can remove some impurities and at the same time make the internal The debris sticks into larger particles, which reduces the resistance to the fluid and improves the filtration performance. However, this treatment often leads to a great reduction or even loss of its specific surface area and adsorption performance, which greatly limits its application.

Method used

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  • Method for improving specific surface area and adsorption performance of opoka
  • Method for improving specific surface area and adsorption performance of opoka

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0017] Example 1

[0018] (1) take by weighing natural protein soil 9g, NaOH 1g respectively, utilize vortex mixer to stir 30min, make it mix well, obtain preliminary protein soil powder;

[0019] (2) Weigh 1.9g MgCl 2 Mix it with 2.7g glycerol to make 1L mixed solution, take 50mL mixed solution, mix it with the preliminary protein soil powder evenly, and then add it into a 75mL ceramic crucible according to the solid-liquid mass ratio of 1:5. Put it in a high-pressure reactor and react at 160 °C for 12 hours; oxygen is not released during the heating process, so as to ensure that the reaction process is in an aerobic environment;

[0020] (3) After the reaction is completed, the protein soil is taken out and cooled to room temperature. After filtration, it is fully dried at 100° C., and pulverized to below 74 μm using a pulverizer to finally obtain protein soil powder with high specific surface area and adsorption performance.

Example Embodiment

[0021] Example 2

[0022] This example is basically the same as Example 1, except that the consumption of natural protein soil is 8.5g, and the consumption of NaOH is 1.5g.

Example Embodiment

[0023] Example 3

[0024] This example is basically the same as Example 1, the difference is: the consumption of natural protein soil is 9.5g, NaOH is replaced with CaO, and its consumption is 0.5g, the autoclave reaction temperature is 180 ℃, and the reaction time is unchanged.

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Abstract

The invention relates to a method for improving the specific surface area and adsorption performance of opoka. According to the method, natural or roasted opoka, an alkali source, MgCl2 and glycerol serving as raw materials are uniformly mixed and subjected to aerobic autoclave treatment, zeolite facies generated on the opoka shell surface can be used for enhancing the adsorbability, and the microporous structure of the opoka surface is more complicated and diversified, so that the specific surface area of the opoka is remarkably increased in the process, and the adsorption performance is further promoted. The method can greatly increase the application effect and value of opoka in the fields of adsorbents, filter aids and the like.

Description

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Claims

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Application Information

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Owner 山西智汇创鑫科技材料有限公司
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