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3 results about "Composite ceramic" patented technology

SiC whisker synergistic silicon nitride particle toughened alumina-based ceramic cutter material and preparation process thereof

ActiveCN110818395AImprove corrosion resistanceHigh processing compatibilityComposite ceramicCeramic knife
The invention provides a SiC whisker synergistic silicon nitride particle toughened alumina-based ceramic cutter material and a preparation process thereof. The preparation method comprises the following steps: preparing SiC whiskers and a sintering aid into slurry, uniformly mixing the slurry with Al2O3 and Si3N4, drying to obtain composite ceramic powder, pre-pressing the composite ceramic powder into a green body, and carrying out vacuum hot-pressing sintering on the green body to obtain the alumina-based ceramic cutter material, wherein the heating process of the vacuum hot pressing sintering comprises the following steps: heating to 190-210 DEG C at a first heating rate, keeping the temperature, heating to 1350-1450 DEG C at a second heating rate, keeping the temperature, heating to 1500-1650 DEG C at a third heating rate, and keeping the temperature; in the heating process of vacuum hot-pressing sintering, the green body is firstly kept pre-pressed, when the temperature rises to1050-1150 DEG C, the pressure of the green body is started to be increased and kept, and when the temperature continues to rise from 1350-1450 DEG C, the pressure of the green body continues to be increased until the temperature rising is ended, and the pressure is kept.
Owner:SHANDONG UNIV

Method for preparing carbonitride-silicide solid solution composite ceramic at low temperature by reaction hot pressing sintering technology

PendingCN113999013AFacilitated DiffusionPromote interactionComposite ceramicCarbide
The invention relates to a method for preparing carbonitride-silicide solid solution composite ceramic at a low temperature by a reaction hot pressing sintering technology, and belongs to the field of multiphase ceramic materials. The invention aims to solve the technical problems of poor sinterability and high-temperature performance of the existing multiphase ceramic. The method comprises the following steps: 1, mixing carbide powder, carbonitride powder and silicon powder, and carrying out ball milling to obtain composite powder; and 2, sintering the composite powder obtained in the step 1 to obtain the carbonitride-silicide solid solution composite ceramic. Fourth subgroup carbides and carbonitride capable of generating solid-phase exchange are selected, the solid-phase reaction and the solid-solution coupling synergistic process of original powder in the sintering process are fully utilized, an anion-cation dual solid solution or split-phase solid solution can be formed, and compared with a traditional means, the sintering temperature can be reduced by 300-500 DEG C. And the relatively low sintering temperature ensures that the material prepared by the method has a fine average grain size, and the strength and the hardness of the material are remarkably improved.
Owner:HARBIN UNIV OF SCI & TECH
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