Spherical magnesium hydroxide particle, spherical magnesium oxide particle, and method for producing same

A technology of magnesium oxide particles and magnesium hydroxide, applied in magnesium hydroxide, magnesium oxide and other directions, can solve problems such as insufficient resin dispersion and achieve the effect of easy production

Active Publication Date: 2013-12-11
TATEHO CHEM IND CO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the method described in Patent Document 1 cannot stably obtain spherical magnesium hydroxide, and there is a mixture of plate-shaped and columnar magnesium hydroxide, and there is a problem that such magnesium hydroxide particles have insufficient dispersibility to resins and the like.

Method used

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  • Spherical magnesium hydroxide particle, spherical magnesium oxide particle, and method for producing same
  • Spherical magnesium hydroxide particle, spherical magnesium oxide particle, and method for producing same
  • Spherical magnesium hydroxide particle, spherical magnesium oxide particle, and method for producing same

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0102] [Example 1]

[0103] In a solution containing 0.4% by mass of zinc oxide and 1 liter of ion-exchanged water with respect to the magnesium oxide used in the reaction, 0.5% by mass of aluminum chloride·hexahydrate and 0.03 mol of propionic acid relative to 100 g of magnesium oxide was used to prepare a reaction liquid.

[0104] The temperature of the prepared reaction liquid was raised to 60° C., and 100 g of magnesium oxide having an average particle diameter of 8.8 μm was introduced to obtain a mixed liquid. After adding magnesium oxide, the temperature of the reaction liquid was raised to 95° C., using a stirrer (T.K. HOMO DISPER manufactured by PRIMIX Corporation), the peripheral speed was adjusted to 9 m / s, and the reaction was performed for 1 hour.

[0105] After that, stirring was carried out at 90°C for 4 hours at a rotation speed sufficient to stir the slurry to prepare a magnesium hydroxide slurry. The prepared magnesium hydroxide slurry is filtered, washed with water

Example Embodiment

[0106] [Example 2]

[0107] Except the addition amount of zinc oxide being 3.0 mass %, it carried out similarly to Example 1.

Example Embodiment

[0108] [Example 3]

[0109] Except that the addition amount of zinc oxide was 0.1% by mass, the same procedure as in Example 1 was carried out.

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Abstract

The purpose of the present invention is to provide a spherical magnesium hydroxide particle and magnesium oxide particle having excellent dispersion properties, and to provide a method for producing the same. Provided are a magnesium hydroxide particle and magnesium oxide particle having a spherical shape in which flake-shaped primary particles are aggregated, the pore distribution having a mode volume of at least 1.4 mL/mg and a mode diameter of at least 0.4 [mu]m.

Description

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Claims

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Application Information

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Owner TATEHO CHEM IND CO
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