Production method for expanded graphite

A technology of expanded graphite and a production method, which is applied in the chemical industry, can solve the problems of low production efficiency, low heat utilization rate of the furnace cavity, long time for heating up and cooling down of the puffed muffle furnace, etc., and achieve high energy utilization rate and high production efficiency Effect

Active Publication Date: 2016-07-13
宣城亨旺新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional graphite expansion devices mostly produce expanded graphite in batch mode. Specifically, dry intercalated graphite is placed in an expanded muffle furnace at 800-1000°C for expansion. However, in actual production, the temperature of the expanded muffle furnace is raised and lowered. The time is long, which leads to low production efficiency. Not only that, the heating range of the puffed muffle furnace is the furnace cavity of the entire furnace body, and the furnace cavity needs to maintain a certain temperature for a long time, but there is no need for excessive temperature during the feeding and retrieving process. High, which undoubtedly makes the heat utilization rate in the furnace cavity low

Method used

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  • Production method for expanded graphite
  • Production method for expanded graphite

Examples

Experimental program
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Effect test

Example Embodiment

[0020] Example 1: Preparation of expanded graphite by traditional expanded muffle furnace

[0021] 1) Take 15g of intercalated graphite with a purity of 98.5% through an 80 mesh sieve, spread it on the tray, and then quickly put it into the muffle furnace heated to 850℃, close the furnace door, and load the material after 5 seconds Disk removal

[0022] 2) Pour the expanded graphite in the tray into the measuring cup, repeat the measurement of the volume expansion ratio for 5 times, and take the average value. The detection standard of the volume expansion ratio is in accordance with GB10698-89 (the same below).

Example Embodiment

[0023] Example 2: Preparation of expanded graphite by traditional expanded muffle furnace

[0024] 3) Take 15g of intercalated graphite with a purity of 99% passing through a 100 mesh sieve, spread it in the tray, and then quickly put it into the muffle furnace heated to 1000℃, close the furnace door, and load the material after 5 seconds Disk removal

[0025] 4) Pour the expanded graphite in the receiving tray into the measuring cup, repeat the measurement of the volume expansion ratio for 5 times, and take the average value.

Example Embodiment

[0026] Example 3: The production method of the present invention prepares expanded graphite

[0027] 1) Take 15g of intercalated graphite with a purity of 98.5% through an 80-mesh sieve, and spread it evenly on the conveyor belt 20 from the inlet 11 by a swinging sieve. The conveyor belt 20 is driven forward to high frequency at a rate of 3cm / s. The induction coil is heated instantaneously, and the entire cavity of the box 10 is passed through the air inlet 13 with nitrogen as a protective atmosphere, and is convectively cooled with the conveyor belt 20. The effective heating length of the heating zone of the conveyor belt 20 is 15 cm. The induction frequency of the high-frequency induction coil is 120MHz, and the heating rate is 850℃ / s, which instantly raises the surface temperature of the conveyor belt 20 from room temperature to 850℃;

[0028] 2) The heated and expanded graphite enters the cyclone collector 40 through the discharge port 12 for gas-solid separation, and the soli

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Abstract

The invention discloses a production method for expanded graphite.The production method includes the following steps that intercalated graphite is put into a box arranged horizontally from a feed port, the intercalated graphite arranged in the box is conveyed to a discharge port through a material conveying unit to obtain the expanded graphite, and in the conveying process, the intercalated graphite is instantaneously heated to 950-1300 DEG C by a material heating unit arranged in the box.During practical production, the intercalated graphite falls into the box through the feed port and is heated at the high temperature through the material heating unit to be expanded, and the graphite expanded at the high temperature is conveyed to the material conveying unit to the discharge port to be discharged.Compared with the prior art, the production method can achieve continuous expansion production for the expanded graphite and is high in production efficiency and high in energy utilization rate.

Description

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Claims

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Application Information

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Owner 宣城亨旺新材料有限公司
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