Preparation technology for neodymium-doped quartz glass used for laser

[0018] A preparation process of quartz glass for neodymium-doped lasers, comprising the following steps:

[0019] One), the preparation of sol

[0020] Using neodymium chloride hexahydrate, aluminum chloride hexahydrate, nano-titanium dioxide, yttrium chloride hexahydrate, silicon alkoxide, organic solvent and water as raw materials, the doping composition range is: Nd 3+ :0.8mol%, Al 3+ :2mol%, Ti 4+ : 1mol%, Y 3+ :0.2mol%, the balance is Si 4+ ; Mix silicon alkoxide, water and organic solvent according to the mass ratio of 1:5:10, then add neodymium chloride hexahydrate, aluminum chloride hexahydrate, nano-titanium dioxide, yttrium chloride hexahydrate, and stir evenly to adjust the pH to 7 to 8, then put it into a drum mixer, and stir for 2 to 5 hours to obtain a sol;

[0021] Two), titration spray

[0022] Put the sol into the titration sprayer, and spray the sol into the self-rotating quartz circular tube in the form of quantitative spraying. The temperature of the out

[0026] A preparation process of quartz glass for neodymium-doped lasers, comprising the following steps:

[0027] One), the preparation of sol

[0028] Using neodymium chloride hexahydrate, aluminum chloride hexahydrate, nano-titanium dioxide, yttrium chloride hexahydrate, silicon alkoxide, organic solvent and water as raw materials, the doping composition range is: Nd 3+ :1.2mol%, Al 3+ :6mol%, Ti 4+ : 3mol%, the balance is Si 4+ ; According to silicon alkoxide: water: the mass ratio of organic solvent is: 1:3.5:15; After mixing silicon alkoxide, water and organic solvent, add neodymium chloride hexahydrate, aluminum chloride hexahydrate, nano-titanium dioxide, Yttrium chloride hexahydrate, stir evenly to adjust the pH to 7-8, then put it into a drum mixer, stir for 2-5 hours to obtain a sol;

[0029] Two), titration spray

[0030] Put the sol into the titration sprayer, and spray the sol into the self-rotating quartz circular tube in the form of quantitative spraying. The

[0034] A preparation process of quartz glass for neodymium-doped lasers, comprising the following steps:

[0035] One), the preparation of sol

[0036] Using neodymium chloride hexahydrate, aluminum chloride hexahydrate, nano-titanium dioxide, yttrium chloride hexahydrate, silicon alkoxide, organic solvent and water as raw materials, the doping composition range is: Nd3+ :0.5mol%, Al 3+ :0.4mol%, Y 3+ :0.8mol%, the balance is Si 4+ ; Silicon alkoxide, water and organic solvent are mixed evenly according to the mass ratio of 1:8:2, then add neodymium chloride hexahydrate, aluminum chloride hexahydrate, nano-titanium dioxide, yttrium chloride hexahydrate, and stir to adjust the pH to 7 to 8, then put it into a drum mixer, and stir for 2 to 5 hours to obtain a sol;

[0037] Two), titration spray

[0038] Put the sol into the titration sprayer, and spray the sol into the self-rotating quartz circular tube in the form of quantitative spraying. The temperature of the outer surface