Graphene magnetic injection molding masterbatch for nylon electrical appliance plastics, and preparation method thereof

[0029] (1) Add sulfonated graphene, iron salt and ferrous salt to deionized water, and prepare graphene-Fe by hydrothermal reaction in lye 3 o 4 Nanocomposite magnetic particles;

[0030] The iron salt is ferric chloride; the ferrous salt is ferrous chloride; the temperature of the hydrothermal reaction is 160°C, the pressure is 1.6MPa, and the time is 5h;

[0031] Wherein: 21 parts by weight of sulfonated graphene, 17 parts by weight of iron salt, 15 parts by weight of ferrous chloride, 62 parts by weight of deionized water;

[0032] (2) First, the graphene-Fe obtained in step (1) 3 o 4 Nanocomposite magnetic particles are surface treated with a coupling agent, then monocarboxyl-terminated nylon 6 and dispersant are added, mixed evenly, and then melted and extruded in an extruder to obtain a nylon 6 melt dispersed with nanocomposite magnetic particles; The coupling agent is isopropyl tris (dioctyl phosphate acyloxy) titanate; the dispersant is sodium methylene bis-naphthalen

[0037](1) Add sulfonated graphene, iron salt and ferrous salt to deionized water, and prepare graphene-Fe by hydrothermal reaction in lye 3 o 4 Nanocomposite magnetic particles;

[0038] The iron salt is ferric bromide; the ferrous salt is ferrous chloride; the temperature of the hydrothermal reaction is 150°C, the pressure is 1MPa, and the time is 7h;

[0039] Wherein: 20 parts by weight of sulfonated graphene, 16 parts by weight of iron salt, 15 parts by weight of ferrous chloride, 64 parts by weight of deionized water;

[0040] (2) First, the graphene-Fe obtained in step (1) 3 o 4 Nanocomposite magnetic particles are surface treated with a coupling agent, then monocarboxyl-terminated nylon 6 and dispersant are added, mixed evenly, and then melted and extruded in an extruder to obtain a nylon 6 melt dispersed with nanocomposite magnetic particles; The coupling agent is isopropyl dioleic acid acyloxy (dioctyl phosphate acyloxy) titanate; the dispersant is sodium methylene bi

[0045] (1) Add sulfonated graphene, iron salt and ferrous salt to deionized water, and prepare graphene-Fe by hydrothermal reaction in lye 3 o 4 Nanocomposite magnetic particles;

[0046] The iron salt is ferric sulfate; the ferrous salt is ferrous chloride; the temperature of the hydrothermal reaction is 170°C, the pressure is 2MPa, and the time is 5h;

[0047] Wherein: 22 parts by weight of sulfonated graphene, 19 parts by weight of iron salt, 14 parts by weight of ferrous chloride, 59 parts by weight of deionized water;

[0048] (2) First, the graphene-Fe obtained in step (1) 3 o 4 Nanocomposite magnetic particles are surface treated with a coupling agent, then monocarboxyl-terminated nylon 6 and dispersant are added, mixed evenly, and then melted and extruded in an extruder to obtain a nylon 6 melt dispersed with nanocomposite magnetic particles; The coupling agent is bis(dioctyloxypyrophosphate) ethylene titanate; the dispersant is sodium methylene bis-naphthalene sulfon