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72results about How to "Good dispersion" patented technology

Method for producing rare earth ion doped yttrium aluminum garnet nano phosphor powder

The invention discloses a method for producing a rare earth ion doped yttrium aluminum garnet nano phosphor powder. The general formula of the nano powder is (Y1-xLnx)3Al5O12, wherein Ln is one of rare earth elements Ce and Eu, x is more than or equal to 0.0 and less than or equal to 0.1, mixed solution of nitrates or acetates of Al, Y and Ln is used as a mother liquor of salt, and mixed solution of NH4HCO3 and NH3.H2O is used as solution of compound precipitator; the ammonia water is used for adjusting the pH value of the solution of compound precipitator to 10; and the mother liquor of salt undergoes ultrasonic atomization and then is sprayed in the solution of compound precipitator which is continuously stirred, and after complete reaction, the mixed solution if filtered, washed, dried, repeatedly ball-milled and calcined to obtain uniform and dispersed rare earth ion doped YAG nano phosphor powder. The method has the advantages that the produced nano phosphor powder is uniform and dispersed, the granularity is small (between 50 and 70 nanometers), and the generated phase is unitary; and the high-concentration uniform doping of the rare earth ions is realized, so that the rare earth ion doped yttrium aluminum garnet nano phosphor powder can be obtained in high efficiency.
Owner:NINGBO UNIV

Heptatridecafluorooctylpropyl polyhedral oligomeric silsesquioxane and functionalized derivates thereof

InactiveCN103183702AHigh puritySimple processSilicon organic compoundsSilanesEvaporation
The invention provides a preparation method for heptatridecafluorooctylpropyl polyhedral oligomeric silsesquioxane and functionalized derivates thereof. The preparation method comprises the steps as follows: adding tridecafluorooctylpropyl trimethoxy silane into an organic solvent, adding de-ionized water and NaOH, heating, stirring, reacting under reflux condition, washing by a washing solvent, and drying to obtain trisilanol sodium salt of heptatridecafluorooctylpropyl polyhedral oligomeric silsesquioxane; and adding trisilanol sodium salt into an organic reagent, dropwise adding hydrochloric acid, triethylamine and a silane coupling agent, stirring a mixture at normal temperature for reaction, removing generated deposit, carrying out rotary evaporation, removing the solvent, obtaining white crystals, dissolving the crystals in methanol, filtering for collecting insoluble parts, and carrying out vacuum drying to obtain a T8-type monofunctional tridecafluorooctylpropyl POSS (polyhedral oligomeric silsesquioxane) monomer. The preparation method can obtain long branch chain type active fluorine-containing POSS, is simple and easy in process, low in cost, high in yield and higher in product purity, and is suitable for large-scale industrial production.
Owner:HOHAI UNIV

Simple spectrum band up-conversion luminescence nanocrystalline and preparation method thereof

InactiveCN103102880AGood dispersionUniform shapeLuminescent compositionsHafniumSolvent
The invention discloses a rare earth ion doped Na3MF7 (M=Zr, Hf) nanocrystalline with a simple spectrum band up-conversion luminescence characteristic and a preparation method thereof, and belongs to the field of inorganic luminescent materials. The preparation method comprises the following step of: based on zirconium oxychloride or hafnium oxychloride and rare earth ion salt as raw materials, performing solvothermal reaction at 90-130 DEG C in a mixed solvent of ethanol, oleic acid and oleylamine for 1-24 hours to obtain monodisperse Yb / Er or Yb / Tm co-doped Na3MF7 (M=Zr or Hf) nano cubic blocks in uniform dimension and shape. Under radiation of 980 nanometer laser, Yb / Er co-doped nanocrystalline can emit bright red light and Yb / Tm co-doped nanocrystalline can emit strong near-infrared light. The material is expected to be widely applied to the field of solar battery and biomarker.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Method for treating waste emulsion

The invention provides a method for treating waste emulsion. The method comprises the following steps: performing oil slick removal treatment on the waste emulsion to be treated to remove oil slick therein; performing oil-water separation treatment on the waste emulsion without oil slick to remove disperse oil therein; performing electrochemical treatment on the waste emulsion after the oil-water separation treatment to obtain roughly treated waste emulsion in which the oil slick and disperse oil are removed and the emulsified oil and dissolved oil are flocculated; and performing static settlement and ultrafiltration treatment on the roughly treated waste emulsion to obtain clear water without oil slick, disperse oil, emulsified oil or dissolved oil, wherein the electrochemical treatment is performed by use of energized aluminum plate and a nano ceramic membrane, and the ultrafiltration treatment is performed by use of the power-off nano ceramic membrane. Through the treatment of the method provided by the invention, the water quality of the yielding water is good, and the yielding water can completely meet the limitation requirements on the discharge into a public sewage treatment system in the Integrated Discharge Standard of Water Pollutants DB11 / 307-2013 of Beijing.
Owner:BEIJING SINORICHEN ENVIRONMENTAL PROTECTION

Cobalt-aluminum composite oxide catalyst and preparation method and application thereof

The invention relates to the technical field of catalyst preparation, and discloses a cobalt-aluminum composite oxide catalyst and a preparation method and application thereof. The preparation methodcomprises the steps that metal salt solutions of cobalt and aluminum are taken as precursors correspondingly, polymer microspheres are taken as a template agent, templates are soaked in the precursorsolutions, then impregnation and roasting are conducted, and thus the cobalt-aluminum composite oxide catalyst is obtained. A three-dimensional ordered hierarchical pore structure with a mesoporous and macroporous structure is created through the polymer microspheres, thus the specific surface area of the catalyst is increased, the prepared catalyst has a large transmission pore channel, reactantmodules enter the pore channel from all directions advantageously, the diffusion resistance is lowered, thus the convective mass transfer efficiency between gases is improved, and the catalytic activity of the cobalt-aluminum composite oxide catalyst is facilitated; and meanwhile, through the large transmission channel, the situation that the modules are blocked when reacting on the pore wall or the pore channel of the transmission channel, and consequently, the reaction progress is influenced can further be effectively avoided, and the catalytic conversion efficiency of the catalyst is improved.
Owner:FUZHOU UNIV

Amino functional graphene quantum dot and preparation and application thereof

ActiveCN105174403ACo-precipitationThe production method is simple and convenientWater contaminantsWater/sewage treatment by flocculation/precipitationActivated carbonIndustrial waste water
The invention discloses an amino functional graphene quantum dot and the preparation and application thereof, and belongs to the field of material preparation. According to the amino functional graphene quantum dot and the preparation and application thereof, activated carbon serves as the raw material, after the activated carbon is oxidized through nitric acid, filtration is conducted to remove the nitric acid, oxidized activated carbon is washed through water to be close to neutral, and the graphene quantum dot is obtained. The surface of the obtained graphene quantum dot is provided with a large number of oxygen-containing functional groups such as carboxyl and hydroxy, and therefore the graphene quantum dot can be stably dispersed into water under the neutral condition. Complexing of the carboxyl and the hydroxy on the surface of the graphene quantum dot and most heavy metal ions can be achieved, agglomeration can be caused, and coprecipitation of the graphene quantum dot and the heavy metal ions is achieved finally. Therefore, the graphene quantum dot can be used for purification of industrial waste water containing the heavy metal ions. The production method of the graphene quantum dot is simple, convenient, rapid, low in cost and high in yield; the obtained graphene quantum dot has a good effect on removing the heavy metal ions, and the graphene quantum dot which is subjected to desorption and regeneration treatments can be recycled.
Owner:QUANZHOU FUDA TECH CONSULTING CO LTD

Alloy material with high temperature coefficient of resistance and preparation method thereof

InactiveCN102888537AGuaranteed resistivityGuaranteed AntioxidantAlloyTitanium
The invention provides an alloy material with high temperature coefficient of resistance. The alloy material is prepared by adding six metal components as the additives to nickel-ferrum alloy, and smelting same to obtain the product, wherein the six metal components are respectively germanium, zirconium, cerium, titanium, aluminum and ferrum; and the alloy material comprises the following components in percentage by weight: 50-65% of component Ni, 14-21% of component Cr, 0.1-0.9% of component Ge, 0.15-0.5% of component Ce, 0.2-1% of component Zr, 1.1-3.5% of component Ti, 0.5-2% of component Al, and the balance of component Fe. The invention also provides a preparation method of the alloy material. The alloy material prepared by the preparation method provided by the invention is of 8.2g / cm<3> based on the density, and has the resistivity of 1.53 (microhm.megabyte.20 DEG C); and the alloy material has temperature coefficient of resistance of 240aR / *10<-6>DEG / C under 100-800 DEG C; and the temperature is in good linear relation to the resistivity.
Owner:WUHAN XINYUAN TUOER TECH CO LTD

Method for preparing pure-phase monodisperse ZnS nanocrystalline by using diethylene glycol serving as solvent

InactiveCN102923759AGood dispersionSimple programmingZinc sulfidesNanotechnologyAlcoholRoom temperature
The invention discloses a method for preparing pure-phase monodisperse ZnS nanocrystalline by using diethylene glycol serving as a solvent. The method comprises steps of dissolving Zn (NO3)2.6H2O in the diethylene glycol, regarding the Zn (NO3)2.6H2O which is dissolved in the diethylene glycol as a zinc source precursor solution, dissolving thiacetamide and Polyvinylpyrrolidone (PVP) in the diethylene glycol, regarding the thiacetamide and the PVP which are dissolved in the diethylene glycol as a sulphur source precursor solution, pouring the sulphur source precursor solution into a flask with three necks which is provided with a condenser tube, feeding a nitrogen flow, heating, injecting the zinc source precursor solution of which the mol ratio of Zn and S is 1:1, conducting reflux for 10 minutes at the temperature from 180 DEG C to 200 DEG C, cooling to the room temperature by using water, cleaning centrifugally by using absolute ethyl alcohol, dispersing zinc oxide nanocrystalline in alcohol and sealing and storing the zinc oxide nanocrystalline. The zinc blende ZnS nanocrystalline which does not have any impure phases and is good in dispersibility is synthesized, the process is free from pollution, the device is simple, the preparation cost is low and the scale industrial production can be applied.
Owner:TIANJIN UNIV

Spherical nano-porous hydroxylapatite prepared through shells and preparation method thereof

ActiveCN105347322AGood dispersionLarge specific surface areaPhosphorus compoundsAcetic acidApatite
The invention discloses spherical nano-porous hydroxylapatite prepared through shells and a preparation method thereof, and belongs to the technical field of material preparation. According to the hydroxylapatite prepared through the method, the hydroxylapatite is in a spherical shape, the diameter is 4-5 micrometers, the dispersity is good, the specific surface area is 270 cm<2>/g, the average pore diameter is 18 nm, carbonate radicals are contained, the components are similar to those of hydroxylapatite in the bones, and the biocompatibility is good. The preparation method comprises the following steps that the shells are washed, dried and ground, acetic acid with the concentration of 0.1 g/mL is added to fully react with the ground shells, an H3PO4 solution is dropwise added into a prepared calcium acetate solution, trisodium citrate is added, urea is added after reacting under stirring are performed, a prepared solution is stirred to be subjected to a reaction for 5 min in a water bath at the temperature of 80 DEG C-90 DEG C, standing is performed until precipitates occur, and the obtained precipitates are filtered, washed, dried and then collected. According to the method, shell powder does not need to be calcined, the reaction time is short, the pH does not need to be adjusted, operation is easy, the repeatability is good, the raw materials are easy to obtain, and not only is waste utilization achieved, but also energy conservation and emission reduction are facilitated.
Owner:ZHEJIANG SCI-TECH UNIV

Waterborne polyester resin and preparation method thereof

InactiveCN106893087AImprove hydrolysis resistanceGood dispersionPolyester coatingsWater dispersibleAdipic acid
The invention discloses waterborne polyester resin, comprising polyols and polyacids; the polyols include 8-12% of trimethylol propane, 12-24% of neopentyl glycol, 6-12% of ethylene glycol, and 8-12% of propylene glycol; the polyacids include 5-15% of purified terephthalic acid, 12-24% of isophthalic acid, 6-12% of phthalic acid, 10-18% of trimellitic anhydride, 6-12% of hexahydro-phthalic acid, 10-20% of maleic anhydride, and 5-10% of adipic acid; the waterborne polyester resin also comprises 0.1-0.3% of p-methoxyphenol, 6-24% of ethylene glycol butyl ether, 8-16% of dimethylethanolamine, and 60-100% of deionized water. The waterborne polyester resin can gain improved hydrolysis resistance, water dispersibility and storage stability, has improved stability of polyester main chain hydrolysis and is widely applicable to waterborne insulating devices, the defects of the prior art can be overcome, and the requirement on actual use can be met.
Owner:CHUZHOU QUAN FENG MATERIALS CO LTD

Water-based aramid coating slurry and water-based aramid/ceramic mixed coating liquid and preparation methods and application thereof

InactiveCN109181523AGood air permeabilityGood dispersionCell component detailsPolyamide coatingsAcrylateAdhesive
The invention provides water-based aramid coating slurry, water-based aramid/ceramic mixed coating liquid, preparation methods and application thereof. The water-based aramid coating slurry comprisesaramid, an acrylate adhesive, a fluorocarbon surfactant, a cellulose ether dispersant, a hydrophilic emulsifier and water. The water-based aramid/ceramic mixed coating liquid is obtained by mixing thewater-based aramid coating slurry with ceramic coating slurry. The ceramic coating slurry comprises aluminum oxide, a dispersant, an adhesion agent, a wetting agent and water. The water-based aramid/ceramic mixed coating liquid can be used for preparing a lithium ion battery separator. The lithium ion battery separator prepared by the water-based aramid/ceramic mixed coating liquid combines the advantages of the traditional oily aramid coating and the water-based ceramic coating, and has excellent performances such as high temperature resistance, high strength, good gas permeability, excellent wettability and strong adhesive force; the water immersion treatment is not needed in the coating process; the coating technology is simple; the environment is not polluted in the coating process, and the ceramic dropping phenomenon is effectively improved.
Owner:HEBEI GELLEC NEW ENERGY MATERIAL SCI&TECHNOLOY CO LTD

Preparation method of Cu2CdSnS4 nanometer crystal

InactiveCN101905901AEasy to prepareLow costTin compoundsDispersityDevice material
The invention discloses a preparation method of Cu2CdSnS4 nanometer crystal with low cost and high quality. In the method, the high-quality Cu2CdSnS4 nanometer crystal is finally obtained by adding reactant presoma oleamide, copper acetylacetonate, cadmium acetate, tin acetate and sulphur in a reaction flask and then rising the temperature for reaction. The invention has the advantages of simple nanometer crystal preparation method, low-cost used presoma material; and the prepared nanometer crystal particles have good dispersity and favorable crystallinity. The prepared nanometer crystal can be used as thermo-electric device materials.
Owner:SHANGHAI INST OF TECHNICAL PHYSICS - CHINESE ACAD OF SCI

High-strength composite fiber non-woven cloth and preparation method thereof

ActiveCN106427147AFirmly connectedClosely connectedProtective equipmentSynthetic resin layered productsEpoxyAlcohol
The invention discloses high-strength composite fiber non-woven cloth and a preparation method thereof. Ultrahigh-strength high-modulus polyethylene fibers are used as base materials, the polyethylene fiber obtained after fiber placement is subjected to a series of homogenization, parallelization and straight and upright arrangement and placed in a modified epoxy resin solution for sizing treatment in an environment of 60-80 DEG C, then the formed polyethylene fiber layers are subjected to composite lamination, and the non-woven cloth is prepared, wherein the modified epoxy resin solution is prepared by adding and mixing an adhesion agent, a filling agent, an insulating filler, fire retardant, white carbon black and ethyl alcohol, the mass of hydroxyl chemigum accounts for 8-12% of the mass of the modified epoxy resin solution, and the content of vinyl cyanide accounts for 18-30% of the content of hydroxyl chemigum. The non-woven clothes with different thicknesses are prepared by lamination of the polyethylene fiber layers, an antiknock device can be made from different types of non-woven cloths according to explosion sites and use environment, and the non-woven cloths with different thicknesses are different in anti-explosion range so as to sufficiently withstand the impact of a bullet.
Owner:JIANGSU LINRY NEW MSTAR TECH

Method for manufacturing fluorescence semiconductor quantum dots containing cadmium

The invention discloses the preparation method of semiconductor quantum dots with cadmium fluorescence, which adopts CdO as the source of cadmium, and adopts Se source and S source, and oleic acid, diesel oil or soybean oil are respectively regarded as the solvents of CdO, Se and S so as to form the precursor solutions of Cd, Se and S, oleic acid is also regarded as the stabilizer of the generated quantum dots, then the precursor solutions of Cd, Se and S react with the temperature of 150 to 250 DEG C, so as to get the quantum dots of CdSe; and CdS, CdO is regarded as the source of cadmium, and with the source of Te, oleic acid, capric acid, octanoic acid, and caproic acid, diesel oil or soybean oil are respectively regarded as the solvents of CdO and Te so as to form the precursor solutions of Cd and Te, the Cd precursor solution and the Te precursor solution are mixed together in the system of diesel oil with the temperature of 80 to 180 DEG C to get CdTe quantum dots, the method of the invention can get quantum dots with good dispersibility, uniformity and optical performance in low temperature, and cheap quantum dots can be put into mass production.
Owner:HUNAN UNIV

Microcapsule Type Thermochromic Pigment and Preparation Method and Use Thereof, Thermochromic Ink and Use Thereof

ActiveUS20220145106A1Good dispersionGood optical performanceInksOrganic dyesEpoxyPolymer science
The disclosure provides a microcapsule type thermochromic pigment and a preparation method and use thereof, and a thermochromic ink and use thereof. The microcapsule type thermochromic pigment provided by the disclosure includes a core material and a wall material wrapping the core material, wherein the core material includes the following components: a leuco dye, a developer and stearic acid 2-[4-(phenylmethoxy)phenyl]ethyl ester, and the wall material is self-emulsifying polyurethane or self-emulsifying epoxy resin.
Owner:WUHAN ZHONGKE ADVANCED MATERIAL TECH CO LTD

Tomato fertilizer containing rich nucleic acid and preparation method of tomato fertilizer

InactiveCN106007932AImprove water holding capacityImprove stabilityCalcareous fertilisersAlkali orthophosphate fertiliserHeavy metal chelationPolyvinyl alcohol
The invention discloses a tomato fertilizer containing rich nucleic acid. The tomato fertilizer is prepared from raw materials in parts by weight as follows: 200-210 parts of rice straw, 20-21 parts of kaoline, 10-11 parts of urea, 10-11 parts of furnace dust, 5-6 parts of hawthorn seeds, 7-8 parts of nucleic acid wastewater, 0.3-0.4 parts of ammonium polyphosphate, 0.1-0.2 parts of a urease inhibitor, 1-2 parts of gypsum powder, 1-2 parts of amino acid powder, 15-16 parts of polyvinyl alcohol, 1-1.1 parts of tea polyphenol, 1-1.1 parts of carbon nanotubes, 1.2-1.3 parts of beta-cyclodextrine and 800-810 parts of 28% ammonia water. Amino groups are introduced to biomass charcoal prepared from the rice straw and can be chelated with heavy metal, the heavy metal adsorption capability is improved, and the pollution influence of the heavy metal on soil and the environment is reduced. The carbon nanotubes are added to a film coating liquid, the mechanical strength of a film can be improved, and added tea polyphenol can improve the slow-release property of the film; besides, the tomato fertilizer contains rich nucleic acid, the activity of tomatoes can be enhanced, decaying of the tomatoes is delayed, and the yield is increased.
Owner:ANHUI YONGGUAN AGRI TECH CO LTD

Material comprising ultrafine cellulose fibers

ActiveUS20180265597A1Good dispersionPaper/cardboardCellulose pulp after-treatment modificationCellulose fiberAqueous medium
An object of the invention is to provide a material comprising ultrafine cellulose fibers, having good dispersibility of fine particles in an aqueous medium containing ultrafine cellulose fibers. According to the invention, there is provided a material comprising ultrafine cellulose fibers, wherein the content of the ultrafine cellulose fibers is 80% by mass or more, and the haze value of a sample, which has been prepared by adding the material comprising ultrafine cellulose fibers to pure water to a solid concentration of 0.4% by mass, and stirring the mixture with a disperser under conditions of 1500 rpm and 5 minutes, is 20% or less.
Owner:OJI HLDG CORP

Waterborne polyurethane super wear-resistant finish paint and preparation process thereof

The invention discloses waterborne polyurethane super wear-resistant finish paint and a preparation process thereof, and relates to the technical field of preparation of finish paint, aiming at solving the problem that the finish paint is poorer in wear resistance, so that local damage is easily caused in a using process. The finish paint is prepared from a component A and a component B, wherein the component A is prepared from the following raw materials: 50-60 parts of waterborne polyurethane resin AH-1618, 12-18 parts of polyurethane color paste, 0.8-1.2 parts of a leveling agent BYK346, 0.3-0.5 part of an aqueous leveling agent BYK333, 0.3-0.6 part of a polyurethane rheological agent SN612NC, 0.3-0.5 part of a defoaming agent BYK024, 0.08-0.1 part of a defoaming agent Tego901W, 0.8-1.5parts of rutile titanium dioxide, 8-10 parts of wear-resistant ball powder, 0.8-1.5 parts of an aqueous scratch-resistant agent, 1.2-1.6 parts of propylene glycol methyl ether and 12-18 parts of deionized water; the component B is prepared from 95-100 parts of a polyurethane curing agent; the ratio of parts by weight of the component A to parts by weight of the components B is equal to (4-6) to 1. The waterborne polyurethane super wear-resistant finish paint has good wear resistance after being cured.
Owner:SHANGHAI BOGE BUILDING MATERIALS CO LTD

Novel neodymium-doped near-infrared fluorescent material and preparation method thereof

InactiveCN104130775AGood physical and chemical stabilityGood dispersionLuminescent compositionsPhysical chemistryLight excitation
The invention discloses a novel neodymium-doped near-infrared fluorescent material and a preparation method thereof. The material is mainly characterized in that the composition is X1SiO2-2Al2O3-3Na2O-4Nd2O3 (X1=20-30%, X2=5-10%, X3=2-5%, and X4=1-10%); and the preparation method of the material comprises: (1) uniformly mixing zeolite and neodymium nitrate, heating to 500-600 DEG C, and keeping warm for 2-5 h, so as to obtain a neodymium-doped zeolite precursor; (2) performing hot-pressing forming on the neodymium-doped zeolite precursor, controlling the pressure intensity to be 10 MPa-3 GPa and the heating temperature to be 700 DEG C-1200 DEG C, and keeping the high temperature for 1 hour or more; and (3) naturally cooling in the furnace. The rare-earth fluorescent material with stable physical and chemical properties, which is obtained by using the method, is characterized in that fluorescence is generated at 1064 nm when 582 nm yellow light is employed for exciting the glass, the transmission scope is 300-400 mu s, and the material is widely applicable to fields such as substance analysis, infrared detection, optical communication and the like.
Owner:CHONGQING LEADING NEW MATERIAL CO LTD

Nanoscale activated calcium carbonate and processing method thereof

InactiveCN110358328AReduce surface polarityOleophilic and hydrophobicMaterial nanotechnologyPigment physical treatmentCalciteHigh velocity
The invention discloses nanoscale activated calcium carbonate. The nanoscale activated calcium carbonate comprises calcite, a dispersant and a coupling agent; a mass part ratio of the calcium carbonate to the dispersant in a grinding process is 100:(0.2-5); and a mass part ratio of the dried nanometer calcium carbonate to the coupling agent in a high-speed mixing and stirring process is 100:(0.5-8). The method reduces the surface polarity of the nanometer calcium carbonate, so the surface of the nanometer calcium carbonate has strong oleophilic and hydrophobic properties, the dispersion property is improved, the dispersibility of the nanometer calcium carbonate in the composite material and the compatibility of the nanometer calcium carbonate with an organic high polymer are improved, andthe nanoscale activated calcium carbonate is obtained. The invention also discloses a processing method of the nanoscale activated calcium carbonate. The processing method comprises the following steps: 1, raw material washing; 2, choosing; 3, coarse crushing; 4, intermediate crushing; 5, addition of the dispersant, and grinding; 6, ATP grading (fine powder + coarse powder); 7, addition of the coupling agent, and high-speed mixing and stirring; and 8, cooling and packaging. The processing method adopting dry process modification has the advantages of low production cost, and suitableness for large-scale industrial production.
Owner:LIANG DE NANO POWDER LNNOVATION & TECH (ANHUI) CO LTD
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