148 results about "Emulsion" patented technology

The invention provides a novel method for preparing a latent nonionic self-emulsifying epoxy curing agent. The method comprises the following steps of: reacting long alkyl chain fatty amine with diglycidyl ether to prepare an addition product of which the middle part is connected with a long hydrophobic side chain and two ends are provided with epoxy groups; and reacting polyamine with a carbonyl compound to prepare an imine compound which contains secondary amine, and sealing the end to prepare the latent nonionic self-emulsifying epoxy curing agent. Under water environment, the imine structure in the curing agent hydrolyzes hydrophilic amino, and the curing agent contains the long hydrophobic alkyl chain, so the curing agent has the functions of emulsifying and curing an epoxy resin. The curing agent can be used for water-based epoxy emulsion coatings, water-based epoxy resin modified emulsified asphalt and cement and the like, and has excellent adhesion performance of ketimine on a wet surface. Due to the introduction of hydrophobic chains, the stability of the imine curing agent is improved in the water environment, and the performance of the curing agent in the aspect of wet surface or underwater adhesion can also be improved.

Non-aqueous taxane pro-emulsion formulations are provided. Pro-emulsion formulations of embodiments of the invention include a taxane, an oil component, a surfactant component and, optionally, a non-aqueous solvent component. Also provided are methods of making and using the pro-emulsion formulations, as well as kits that include the pro-emulsion formulations.

The invention discloses a method for preparing an inorganic aromatic nano-antibacterial agent and antibacterial fabrics. The method for preparing the inorganic aromatic nano-antibacterial agent comprises the following steps: swelling Carbomer resins with surfactants in deionized water, adjusting the PH value to 6.0-7.0 with triethanolamine and forming a stable colloid emulsion; and adding reducing polymers and a silver salt to the colloid emulsion and adding small molecular reducing agents for reduction at 5-100 DEG C in order to improve the purity of silver, thus obtaining the nano silver antibacterial agent. The antibacterial agent is used for padding or soaking the fabrics and the prepared antibacterial fabrics have the characteristics of fast antibacterium, high efficiency, broad spectrum and durability. The preparation methods and the finishing process have the advantages of simpleness, low cost, no pollution and easiness in industrialization.

The invention relates to a catalyst for ternary copolymerization of norbornenes, tetrafluoroethylene and pentenes and a ternary copolymerization method. The catalyst is characterized in that the catalyst is prepared through the following method comprising the steps of: dissolving iron dichloride, a ligand and an alkyl metal compound in a solvent in a dry single-neck glass bottle in an inert gas atmosphere, sealing a bottle mouth through an emulsion pipe, keeping the constant temperature in a water bath at the temperature of 40-50 DEG C for 10-30min, and cooling to obtain an iron complex catalyst. Compared with the prior art, the catalyst provided by the invention is a novel iron complex catalyst which can produce catalytic activity in an nitrogen-protected system at a certain pressure and the temperature of 20-120 DEG C so as to catalyze the ternary copolymerization of the norbornenes with the tetrafluoroethylene and the pentenes, and a product after soaking in methanol is very easy to wash and separate. The catalyst has the characteristics of high copolymer yield, low reaction temperature, low price, easiness in obtainment, high catalytic efficiency and the like.

The invention discloses a double-tail four-functional hydrophilic UV (Ultraviolet) coating hardness assistant and a preparation method thereof. The preparation method comprises the following steps: firstly, reacting polyethylene glycol monomethyl ether, isocyanate and one-generation hyperbranched polymer to form a prepolymer I, and subsequently reacting a prepolymer obtained after crylic acid monomer is reacted with isocyanate with the prepolymer I, thereby preparing the double-tail four-functional hydrophilic UV coating hardness assistant. According to the preparation method, high-functionality hyperbranched molecules are adopted as primary reaction materials, the characteristics that the hyperbranched molecules are high in functionality but low in viscosity are taken, when the prepared hardness assistant is added into an aqueous UV resin, not only is the problem that a coating is always low in curing property but high in viscosity solved, but also the water solubility of the UV resin is improved, the hardness of the aqueous UV resin is also improved, and the application range of the aqueous UV resin is widened. When non-ionic polyethylene glycol methyl ether is connected to molecules, therefore the acid-alkali resistance of the coating is improved, an emulsion system is well stabilized, and experiment shows that the effect is good.

Ultrahigh-toughness concrete and a preparing method thereof are disclosed. The concrete is prepared from, by weight, 380-580 parts of cement, 150-170 parts of slag powder, 250-380 parts of fly ash, 200-400 parts of quartz sand, 13-15 parts of bamboo wood phenolic alcohol liquified resin, 13-18 parts of polypropylene resin, 0.5-1.5 parts of carboxymethylcellulose, 23-47 parts of core-shell acrylic acid elastic emulsion, 5-10 parts of a chemical-resistant modifier, 14-18 parts of bamboo fibers, 2.5-8.5 parts of nanometer silicon particles, 7-13 parts of nanometer calcium carbonate, 3-5 parts of anionic polyacrylamide, 3.7-8.3 parts of poly(diallyldimethylammonium chloride), 0.4-1 part of poly(ethylene glycol) acrylate, 20-30 parts of an acrylic emulsion, and the like. The ultrahigh-toughness concrete has high tensile strength, high compressive strength, ultrahigh ductility, good energy consumption capacity and good elastic modulus.

The invention discloses a coating having heat-insulation and reflection functions. The coating comprises, by weight, 40-60 parts of a pure acrylic emulsion, 30-40 parts of hollow glass microspheres, 20-30 parts of ceramic microspheres, 10-30 parts of expanded perlite, 10-20 parts of titanium dioxide, 5-15 parts of mica powder, 3-8 parts of kaolin, 5-10 parts of barium sulfate, 2-8 parts of carboxyethyl cellulose, 5-10 parts of nano-silica, 8-15 parts of nanometer metal oxide, 3-8 parts of a filler, 1-5 parts of a film forming assistant, 4-8 parts of an assistant and 30-50 parts of deionized water. The coating having heat-insulation and reflection functions has good economic property, and also has heat-insulation and light and heat reflection functions.

The invention discloses colored continuous-phase silicone-acrylic emulsion reactable with protective glue, prepared from, by weight, 130-180 parts of water, 50-90 parts of methyl methacrylate, 60-90 parts of 2-ethylhexyl acrylate, 10-20 parts of butyl acrylate, 0.5-9 parts of hydrophilic unsaturated organic acid, 3-7 parts of a functional monomer, 0.3-2.5 parts of an anionic emulsifier, 0.2-2 parts of an initiator, 0.05-0.25 part of an oxidant, and 0.05-0.25 part of a reducing agent; the prepared colored continuous-phase silicone-acrylic emulsion reactable with protective glue has excellent transparency, weatherability and paint formulating stability, can engage in directional crosslinking reaction with protective glue, and has excellent water resistance and water white resistance as no thickeners are added to the colored continuous phase.

The invention relates to the field of nano materials and particularly relates to a mildew-resistant and antibacterial nano-silver decorative laminated board. The mildew-resistant and antibacterial nano-silver decorative laminated board is formed by a decorative veneer and a base material which are bonded by an adhesive layer, wherein the decorative veneer and the base material are dipped by nano aqueous solution; the adhesive layer contains nano-silver substances; the decorative veneer and the base material are made of technical wood; the nano-silver aqueous solution is formed by adopting deionized water as a solvent, adopting nano silver as solute to be dissolved into the deionized water, adopting acrylic resin as a complexing agent and a stabilizing agent to be dissolved into the deionized water, and adding a dispersing agent and a first reducing agent simultaneously; the concentration of nano silver in the adhesive is 75-150ppm; the mass content of flour in solution is 18-45%; environmental-friendly glue comprises the following materials in parts by weight: 40-80 parts of acrylic resin solution emulsion with the solid content being 40-55%, 20-40 parts of acrylic resin powder, 5-20 parts of EVA emulsion with the solid content being 40-60%, 1-4 parts of dibutyl phthalate and 7-13 parts of chlorinated polypropylene or polyolefin substrate adhesive-force promoter. The mildew-resistant and antibacterial nano-silver decorative laminated board has the advantages that the stability and the dispersibility are good and the mildew can be fully resisted.

The invention provides plant growth type porous concrete suitable for plant growth. The concrete comprises a porous concrete body with thickness and mixed fine loam covering the surface layer of the porous concrete body. The porous concrete body comprises components by volume density as follows: 150-325 kg/m<3> of cement, 1,495-1,550 kg/m<3> of ceramsite, 40-86 kg/m<3> of fly ash, 10-12 kg/m<3> oflimestone powder, 100-120 kg/m<3> of fine loam, 2-3 kg/m<3> of plant ash, 15-30 kg/m<3> of rice husk charcoal, 2.5-4 kg/m<3> of a water reducing agent, 10-20 kg/m<3> of EVA latex powder, 17-40 kg/m<3> of butadiene-styrene rubber powder, 13-23 kg/m<3> of a polyacrylate emulsion, 20-30 kg/m<3> of organic compost, 15-20 kg/m<3> of vermiculite, 2-3 kg/m<3> of seaweed meal, 0.5-0.7 kg/m<3> of tea seedmeal, 2-3 kg/m<3> of neem cakes, 0.7-1.2 kg/m<3> of polyacrylamide, 0.5-1 kg/m<3> of ferrous sulfate, 3-4 kg/m<3> of modified loofah fiber, 0.8-1 kg/m<3> of an organic silicon defoamer and 60-90 kg/m<3> of water.

The invention provides an environment-friendly water-based paint, the formula of which includes a composite color block and component A, and the component A includes the following components in mass percentage: 85.0%-95.0% of water-based elastic acrylic emulsion; 0.1% of defoamer ~0.5%; preservative 0~3.0%; thickener 0.1%~5.0%; film-forming aid 1.2%~8.0%; antifreeze 1.0%~3.0%; softener 1.0~21.0% and water 0~20.0% ; The mass ratio of component A to the composite color block is 5:100 to 65:100. The invention also provides monochrome semi-finished products and color block semi-finished products for preparing composite color blocks, and their preparation methods. The present invention can prepare environment-friendly water-based paint with imitation stone effect through the combination of these raw materials and A component. This kind of coating not only has excellent environmental protection, but also has the effect of imitating stone, which can meet the needs of market diversification, human culture, creativity and individualization, and solve the problem of single color of the coating without increasing the load-bearing load of the building.

The invention discloses a preparation method of octahedral porous molybdenum dioxide and an application of the octahedral porous molybdenum dioxide in a lithium-ion battery. The preparation method comprises the steps of: adding trimesic acid and tetramethyl ammonium hydroxide to a solution containing a copper salt and a phosphomolybdic acid and/or phosphomolybdate for stirring to form an emulsion; transferring the emulsion into a hydrothermal reaction kettle for hydrothermal reaction to obtain a precursor compound; and putting the precursor compound into a protective atmosphere, carrying out thermal treatment at a high temperature and then washing the product to obtain a porous octahedral molybdenum dioxide material which is formed by stacking and assembling ultrafine nanoparticles, is uniform in shape and form and good in stability and has a porous characteristic. The molybdenum dioxide material is applied to the lithium-ion battery as a negative electrode material, so that the rate capability and the cycling stability of the electrode material are improved under the premise of ensuring the specific capacity; the preparation technology of the molybdenum dioxide material is simple; the cost is low; and the molybdenum dioxide material has a relatively good research prospect.

The invention relates to the field of organic high-molecular compounds. In order to solve the problem of deficiency in long residual action and environment friendliness in the existing oil-based fluorine-containing low-surface-energy anti-doodling paint, the invention provides a water-based anti-doodling paint and a preparation method thereof. The preparation method comprises the following steps: adding a pigment, a filler and a dispersing agent into a toning cylinder, mixing, adding into a grinder, and grinding until the fineness is less than 20 mu m to obtain a color paste; and adding deionized water, the color paste, a fluorine-silicon-modified polyurethane core-shell emulsion, a preservative and a mildew preventive into a dispersion cylinder, mixing, sequentially adding a film forming assistant, a defoaming agent a thickener, mixing, and discharging to obtain the water-based anti-doodling paint. The film formed by the paint has the characteristics of excellent weather resistance, excellent ultraviolet resistance, excellent wear resistance, low surface energy, excellent pollution resistance, excellent doodling resistance, low VOC (volatile organic compound) emission, environment friendliness and no toxicity.

The invention discloses color concrete. The color concrete comprises 420-480 parts of cement, 650-800 parts of sand, 980-1,150 parts of cobblestones, 150-180 parts of limestone powder, 100-150 parts of white carbon black, 165-175 parts of water, 30-45 parts of a pigment, 2.0-3.5 parts of acrylic acid emulsion powder and 4.5-6.2 parts of an admixture. A preparation method comprises the following steps: (1) the raw materials are weighed in a predetermined ratio; (2), the pigment, the white carbon black and the acrylic acid emulsion powder are placed into water and stirred uniformly, and color water is formed; (3) the sand, the cobblestones and the limestone powder are fed to a stirrer for stirring, then the cement is fed, stirring continues, the color water and the admixture well weighed in the step (1) are added to the stirrer jointly and slowly during stirring, and the materials are stirred continuously after addition until uniform stirring is realized. The color concrete is higher in strength, is not prone to cracking and is uniform in color, and the preparation method has the advantages of simple production process and convenience in construction.

The invention discloses a preparation method of a waterborne polyurethane emulsion and the waterborne polyurethane emulsion prepared by the preparation method. The preparation method comprises the following steps: (1) synthesizing a polyurethane prepolymer: mixing and dehydrating polypropylene oxide polyether glycol and polycarbonate diol, dropwise adding toluene diisocynate after dehydrating for heat-preserving reaction, and finally dropwise adding prepared mixed solution of dihydroxybutyric acid, 1, 4-butanediol and acetone for heat-preserving reaction to finally prepare the prepolymer; (2) adding aminoalkyl silicon oil, an inner crosslinking agent and hydroxy-propyl acrylate to modify; (3) neutralizing to salify: dropwise adding an acetone solution of a neutralizer triethylamine into the modified prepolymer prepared in the step (2) for reaction so as to prepare a polyurethane salified solution; and (4) dissolving disulfamate and a diamido chain extender in water, quickly adding to the polyurethane salified solution which is stirred at a high speed, quickly dispersing and extending chains, and heating the emulsion to remove the solvent through evaporation to obtain the waterborne polyurethane emulsion.

This invention relates to automatic test field and to emulsion liquid concentration automatic testing system and its method, which comprises sensor, A/D conversion unit, CPU unit, and single machine and display unit. The invention is characterize by the following: the sensor comprises one 850nm infrared laser diode tube, scattering and transparent mode tester and electric meter; the sensor converts the concentration signals into relative analogue voltage signals to convert voltage signal into digital signals through A/D conversion unit to send the digital signals into single machine memory unit for data processing and displaying the results.

The invention discloses inorganic water-based metallic paint and a preparation method thereof. The paint is prepared from raw materials in percentage by weight as follows: deionized water, an anti-freezing agent (ethylene glycol), a film-forming aid (dodecanol carbonate), a bactericide (Rohm and Haas LXE), an organic silicon defoaming agent (Rohm and Haas 505), a leveling agent (Rohm and Haas RM2020), nano titanium dioxide or nano zinc dioxide, sericite powder, nano calcium carbonate powder, potassium trimethylsilanolate, silica sol NM-1020, fumed silica, pearl powder, an emulsion and an associative alkali swelling thickener. The inorganic water-based metallic paint is uniform to spray during construction, the pearl powder is arranged orderly, the color is uniform, the luster of the pearl powder is completely restored, the surface is fine and smooth, and the hand feeling is fine and smooth.