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32 results about "Acrylamide" patented technology

Acrylamide (or acrylic amide) is an organic compound with the chemical formula CH₂=CHC(O)NH₂. It is a white odorless solid, soluble in water and several organic solvents. It is produced industrially as a precursor to polyacrylamides, which find many uses as water-soluble thickeners and flocculation agents. It is highly toxic, likely to be carcinogenic, and partly for that reason it is mainly handled as an aqueous solution.

Method for preparing liquid fluorescent brightener composition of diphenylvinyl triazine compounds

ActiveCN102477227AImprove performanceWith strong fluorescenceStyryl dyesLuminescent/fluorescent substance additionRoom temperatureAniline
The present invention relates to a production process of a chemical additive special for papermaking, in particular to a method for preparing a liquid fluorescent brightener composition of diphenylvinyl triazine compounds. The invention mainly solves the problems of low fluorescence intensity and low brightness of a single-component liquid fluorescent brightener. The method adopts cyanuric chloride, 4,4'-diamino-2,2'-stilbenedisulfonic acid (DSD acid), aniline, monoethanolamine and 1-R1-2-R2-acrylamide as raw material, and employs four-step reaction. The inventive liquid fluorescent brightener composition has convenient usage, good acid resistance, and good storage stability at a room temperature, and is suitable for continuous adding and metering during automatic production.
Owner:JIANGSU JINGUANG CHEM TECH CO LTD

Preparation method and application of surface artemisinin molecule imprinting adsorbing material of vegetable sponge

InactiveCN102600813ASpecific recognition abilityHigh selectivityIon-exchange process apparatusOrganic chemistryCross-linkN dimethylformamide
The invention discloses a surface artemisinin molecule imprinting adsorbing material of a vegetable sponge. The material is characterized characterized by being prepared by the following steps of: preparing a polymer by selecting vegetable sponge as a substrate material, taking artemisinin as a template molecule, taking itaconic acid and acrylamide as functional monomers, taking ethylene glycol dimethacrylate as a cross-linking agent, taking azodiisobutyronitrile as an initiator and taking N,N-dimethylformamide as a solvent; and removing the artemisinin by using a hexane-diethyl ether mixed solution. The invention further provides a preparation method and an application method of the surface artemisinin molecule imprinting adsorbing material of the vegetable sponge. The surface artemisinin molecule imprinting adsorbing material of the vegetable sponge can separate the artemisinin with a structural analogue under normal pressure and temperature conditions; and the surface artemisinin molecule molecular imprinting adsorbing material of the vegetable sponge has the advantages of specificity, selectivity, good mechanical performance, good chemical stability, fast adsorbing speed, easiness for being eluted, biodegradability, simple process, regeneration capability, environmental friendliness and the like.
Owner:UNIV OF JINAN

Coagulating agent for treating wastewater containing fluorine and use process thereof

ActiveCN101492192ALow priceLow investment costWater/sewage treatment by flocculation/precipitationAluminium chlorohydrateWastewater
The invention discloses a coagulating agent for use in the treatment of wastewater containing fluorine and an application process thereof. The coagulating agent for use in the treatment of water containing fluorine is a composite coagulating agent prepared by adding a polymer organic additive during the synthesis of aluminium polychlorid; the polymer organic additive is a cationic polyacrylamide having a 10 to 30 percent amination degree and a 5 to 8 million molecular weight; and the mass of the added polymer organic additive is 1 to 10 percent of that of AlCl3.H20. The application process comprises: adding a modifier of lime milk into the wastewater containing fluorine to adjust the pH value of the wastewater containing fluorine to between 6 and 9; and adding the coagulating agent for use in the treatment of wastewater containing fluorine into the wastewater containing fluorine for coagulation in an amount of 900 to 1,500 milligrams of coagulating agent for use in the treatment of wastewater containing fluorine per liter of wastewater containing fluorine. The coagulating agent for use in the treatment of wastewater containing fluorine is low in raw material price and production cost, and the application process is simple, high in removal efficiency and low in investment cost and has the advantages of high efficiency and economy.
Owner:HANGZHOU CHENGJIE ENVIRONMENTAL PROTECTION

Tackifier for drilling fluid and preparation method thereof

ActiveCN104311730AImproved rock carrying capacityThe preparation method is simple and feasibleDrilling compositionCross-linkSalt resistance
The invention relates to a tackifier for drilling fluid and a preparation method thereof, and belongs to the technical field of synthesis of processing agents for oil-field drilling fluids. The tackifier is a net-like polymer obtained by mixing acrylamide, a sulfo-group-containing monomer A and a pyrrolidone monomer B according to the mass ratio of 10:(3-5):(0.7-1.5), adjusting the pH value of the solution, adding a cross-linking agent C, a molecular-weight adjusting agent D and an initiator and performing copolymerization crosslinking. The preparation method is simple and practicable, and short in reaction time. The obtained tackifier has good salt resistance, has the temperature resistance up to 135 DEG C, has good effects of increasing shear viscosity and reducing filter loss when being applied to drilling fluids, is capable of substantially improving the cutting carrying capability of the drilling fluids under the condition of high temperature, has the effect obviously better than a tackifier normally used on site, is widely applicable to fresh-water drilling fluids and saturated brine drilling fluids, and has relatively good application prospect.
Owner:CHINA PETROCHEMICAL CORP +1

Waterproof reinforced composite and preparation method thereof

The invention discloses a waterproof reinforced composite and a preparation method thereof. The waterproof reinforced composite is prepared from the following raw materials in parts by weight: 60-90 parts of epoxy resin modified polyurethane emulsion, 15-30 parts of organic silicon styrene-acrylic emulsion, 10-30 parts of methyl methacrylate, 10-20 parts of polyacrylate, 2-4 parts of N-hydroxymethyl acrylamide, 6-12 parts of oxide-coated titanium dioxide, 10-30 parts of composite filler, 3-8 parts of silane coupling agent, 3-6 parts of propanediol butyl ether, 3-6 parts of diethylene glycol monobutyl ether, 5-10 parts of sodium polyphosphate, 4-8 parts of polyvinyl butyral, 2-5 parts of urea-isobutyraldehyde-formaldehyde resin, 0.3-0.6 part of sodium perfluorous nonenoxybenzene sulfonate,0.4-0.9 part of polypropylene wax emulsion, 0.3-0.7 part of polyether modified polysiloxane, 0.5-1 part of hydroxypropyl methyl cellulose, 1-3 parts of epoxy phosphate ester, 1-5 parts of compound antiaging agent and 10-20 parts of water.
Owner:SUZHOU FUZHONG PLASTIC CO LTD

Phosphorus-free corrosion and scale inhibitor applicable to high-chlorine high-concentration-multiple circulating cooling water and preparation method of phosphorus-free corrosion and scale inhibitor

InactiveCN110655206AStrong targetingLow toxicitySpecific water treatment objectivesScale removal and water softeningMeth-Biology
The invention relates to a phosphorus-free corrosion and scale inhibitor applicable to high-chlorine high-concentration-multiple circulating cooling water and a preparation method of the phosphorus-free corrosion and scale inhibitor, belonging to the technical field of water treatment. The technical problem to be solved by the invention is to provide the phosphorus-free corrosion and scale inhibitor with low toxicity, chloride resistance and low cost for high-concentration-multiple circulating cooling water containing high-concentration chloride ions. The phosphorus-free corrosion and scale inhibitor is prepared from the following raw materials in parts by weight: 3 to 5 parts of zinc sulfate, 4 to 7 parts of sodium gluconate, 2 to 4 parts of sodium molybdate, 0.5 to 2 parts of benzotriazole, 5 to 9 parts of and acrylic acid-2-acrylamide-2-methylpropanesulfonic acid copolymer, 7 to 12 parts of polyepoxysuccinic acid and 3 to 5 parts of hydrolyzed polymaleic anhydride. Compared with similar corrosion and scale inhibitors, the phosphorus-free corrosion and scale inhibitor for high-concentration-multiple circulating cooling water provided by the invention has the advantages of strongtargeting performance, low toxicity, chloride resistance, low cost, simple operation, convenience, rapidness, environmental friendliness, safety, high efficiency and the like.
Owner:RUITIAN SECURITY & ENVIRONMENTAL PROTECTION CO LTD PANZHIHUA GANGCHENG GRP

Epoxy emulsion cured at room temperature with high aquosity and weather resistance as well as preparation method of epoxy emulsion

InactiveCN102604047AGood film formingGood physical and mechanical propertiesCoatingsEpoxyBenzoyl peroxide
The invention discloses epoxy emulsion cured at room temperature with high aquosity and weather resistance as well as a preparation method of the epoxy emulsion. The epoxy emulsion comprises the following components in percentage by weight: 15-20 percent of E-20 epoxy resin, 5-10 percent of E-12 epoxy resin, 1.0-1.5 percent of benzoyl peroxide, 4.0-6.0 percent of methacrylic acid, 3.0-8.0 percent of hexafluorobutyl acrylate, 0.5-2.5 percent of diacetone acrylamide, 0.5-2.5 percent of adipic acid dihydrazide, 10-20 percent of ethylene glycol monobutyl ether, 5-10 percent of n-butyl alcohol, 3.5-5.5 percent of N,N-dimethylethanolamine and 22-40 percent of water. The preparation method comprises the following steps: firstly, adding E-20 epoxy resin, E-12 epoxy resin, n-butyl alcohol and ethylene glycol monobutyl ether to be evenly dissolved; then, dipping mixed solution of benzoyl peroxide, methacrylic acid, hexafluorobutyl acrylate, diacetone acrylamide and adipic acid dihydrazide to be reacted; and adding N,N-dimethylethanolamine and water to prepare the epoxy emulsion. The epoxy emulsion and the preparation method of the epoxy emulsion have the characteristics of weather resistance, abrasive resistance, water resisting property, alkali resistance, corrosion resistance, flexibility, washable resistance, environment protection and simple preparation process.
Owner:JIANGSU UNIV OF SCI & TECH

Straight-chain liquid AKD surface sizing agent and preparation method thereof

InactiveCN110983856ALimit hydrolysisLimit migratory propensityWater-repelling agents additionFiberPolymer science
The invention discloses a straight-chain liquid AKD surface sizing agent and a preparation method thereof. The straight-chain liquid AKD surface sizing agent is prepared from the following raw materials in parts by weight, 100-200 parts of starch, 1000-2000 parts of water, 4-8 parts of sodium hydroxide, 25-50 parts of a cationic etherifying agent, 5-10 parts of a dilute acid, 15-30 parts of a cationic monomer, 25-50 parts of acrylamide, 1-2 parts of an initiator, 5-10 parts of a dispersing agent, 20-50 parts of an AKD special cationic polymer emulsifier, and 60-150 parts of liquid AKD. The molecular structure of the straight-chain liquid AKD adopted by the invention has a lactone ring structure; reacting under neutral and alkaline conditions; the reaction functional groups and hydroxyl groups on fiber molecules are subjected to esterification reaction to be firmly bonded on the surfaces of the fibers; the hydrophobic long-chain fatty group turns to the paper surface, so that the hydrophobic effect is obtained, the stability and the sizing effect of the AKD surface sizing agent are remarkably improved by adding the AKD special cationic polymer emulsifier, meanwhile, the hydrolysis and migration tendency of AKD is limited, and AKD latex is well protected.
Owner:JINING MING SHENG NEW MATERIALS CO LTD

Transparent flashing polyester chain tooth, preparation method and zip fastener

ActiveCN109306156AEvenly dispersedPromote cross-linking reactionSlide fastenersPolyesterAntioxidant
The invention relates to the technical field of chain teeth and in particular relates to a transparent flashing polyester chain tooth, a preparation method and a zip fastener. The transparent flashingpolyester chain tooth is prepared from PET (Polyethylene Terephthalate), TPU (Thermoplastic Polyurethane) modified master batch, a lubricant, an antioxidant and an ultraviolet absorbent, wherein theTPU modified master batch is prepared from isocyanate, polyol, a chain extender, a crosslinking agent and flashing powder; the flashing powder is composed of a micron-grade prism pyramid monomer polyacrylamide layer. According to the transparent flashing polyester chain tooth, the TPU modified master batch with relatively good toughness is added into a PET material, so that the transparent flashing polyester chain tooth has good toughness and anti-impact performance; furthermore, the surface of a micron-grade prism pyramid monomer is covered with the polyacrylamide layer and the crosslinking agent participates, so that the micron-grade prism pyramid monomer is uniformly dispersed in the PET material; compared with a manner of directly adding the micron-grade prism pyramid monomer or the flashing powder into the PET material, the transparent flashing polyester chain tooth has a more uniform and bright flashing property.
Owner:东莞市瑞翔新型材料科技有限公司

Binary retention system for spherical polyelectrolyte brush and method for improving retention rate of paper pulp

InactiveCN105088859ASimple structureStrong shear resistanceRetention agents additionPolyelectrolyte brushesPapermaking
The invention provides a binary retention system for a spherical polyelectrolyte brush for improving the retention rate of paper pulp. The binary retention system is composed of a cationic spherical polyelectrolyte brush and anionic polyacrylamide, wherein the cationic spherical polyelectrolyte brush regards SiO2 as an inner core and a copolymer of acrylamide and methacryloyloxyethyl trimethyl ammonium chloride as an outer brush. The invention further provides a method for improving the retention rate by using the binary retention system. The method comprises: sequentially adding the binary retention system composed of the cationic spherical polyelectrolyte brush and anionic polyacrylamide into scattered paper pulp to improve the retention rate of the slurry. The cationic spherical polyelectrolyte brush provided by the invention has high symmetric or quasi-symmetric structures, so that the anti-shear ability is relatively strong. The system has both the characteristics of a highly branched structure and high charge density and is easily to induce flocculation in high speed papermaking so as to improve the retention performance of a modern papermaking system. The binary system adopted by the invention remarkably improves the retention rate of the paper pulp and is simple and convenient to operate and less in use level of auxiliaries.
Owner:WUHAN UNIV

Preparation method of polyacrylamide reverse-phase emulsion

InactiveCN107226875AImprove securityLess heat of polymerizationPolymer scienceEmulsion
The invention belongs to the field of water-soluble high molecular materials, and in particular relates to a method for industrially preparing polyacrylamide reverse-phase emulsion. A polyacrylamide reverse-phase emulsion product is obtained by adopting a multi-step polymerization step. The method comprises the following steps: step 1, by taking acrylamide and acrylic acid or 2-acrylamido-2-methylpropanesulfonic acid as a polymerization monomer and taking Span and octylphenol polyoxyethylene ether (OP) as an emulsifier, carrying out a small amount of polymerization to prepare the polyacrylamide reverse-phase emulsion, wherein polymerization heat is less so as to ensure that implosion dangers, caused by the fact that heat is not dissipated in time, do not occur in a polymerization process; step 2, polymerizing: carrying out further polymerization on the basis of the polymerization in the step 1, wherein partial polymerization is carried out, so that polymerization heat generated by the polymerization in step 2 is greatly reduced, an implosion phenomenon does not occur, and gel or emulsion breaking is not generated in the polymerization process. In a subsequent polymerization process, the released amount is determined according to the size of a polymerization kettle and heat releasing efficiency when one part of product is released each time. By adopting the method provided by the invention, the safety of polymerization reaction is greatly improved, the large-size polymerization kettle can be utilized, and the implosion possibility does not need to be worried, so that industrial production can be stably and safely carried out.
Owner:SHANDONG UNIV

Preparation method of composite efficient coagulant for treatment of textile printing and dyeing wastewater

InactiveCN110980909AEasy to reuseReduce processing costsWater treatment parameter controlWaste water treatment from textile industryTextile printerDyeing wastewater
The invention provides a preparation method of a composite efficient coagulant for treatment of textile printing and dyeing wastewater, belonging to the technical field of wastewater treatment. The preparation method comprises the following steps: roasting fly ash, carrying out secondary acid leaching extraction, performing filtering, collecting filtrates, and combining the filtrates for later use; dissolving sodium silicate in a certain amount of deionized water, adjusting a pH value with hydrochloric acid, carrying out a reaction for 3-6 h, dropwise adding the filtrate and a cerium oxide solution, carrying out a stirring reaction for 10-15 min, adding chitosan, carrying out a reaction for 5-10 min, adjusting the pH value with sodium hydroxide, and carrying out a stirring reaction for 3-6h; adding disodium hydrogen phosphate into the reaction solution, and then carrying out stirring and heating to 40-50 DEG C; then, adding polydimethyldiallyl ammonium chloride and starch modified polyacrylamide, continuing stirring for a reaction for 1-2 h, performing standing, and carrying out curing for 20-25 h. According to the invention, a variety of coagulation components are matched with one another, so the composite efficient coagulant has good treatment effect on textile printing and dyeing wastewater, wherein the removal rate of COD achieves 94%, and the removal rate of TOC achieves97.9%; and the composite efficient coagulant has outstanding charge neutralization ability.
Owner:安徽子延科技有限公司

Bone gelatin wastewater treatment method

InactiveCN114873840ALow acid valueDoes not increase concentrationTreatment using aerobic processesTreatment with anaerobic digestion processesGelatinPolyacrylamide
The invention provides a bone gelatin wastewater treatment method. The bone gelatin wastewater treatment method comprises the following steps: S1, collecting liming workshop wastewater; s2, collecting wastewater of a pickling workshop; s3, collecting other wastewater in the production process; s4, all the wastewater is introduced into a comprehensive adjusting tank to be mixed, and mixed wastewater is obtained; s5, introducing the mixed wastewater into a reaction tank, adding Na2CO3, then adding polyacrylamide, and fully reacting to obtain a reaction solution; s6, carrying out solid-liquid separation on the reaction liquid, and feeding obtained sludge into a sludge tank for recycling and post-treatment; s7, the supernate enters a pH adjusting pool, dilute sulphuric acid is added, and a mixed solution is obtained after reaction; s8, enabling the mixed solution to pass through an anaerobic tank, an anoxic tank and an aerobic tank to obtain a treatment solution; and S9, introducing the treated liquid into a secondary sedimentation tank, separating, metering and discharging the supernatant, returning the settled sludge to an anaerobic tank, supplementing the sludge concentration, and carrying out dewatering treatment on the residual sludge. The bone gelatin wastewater treatment method disclosed by the invention is low in calcium ion content and small in impact on the biochemical environment.
Owner:池州市琼琚信息技术服务有限公司 +1

Preparation method of high-water solubility polyacrylamide

InactiveCN110885390AWill not polluteImprove purityGas liquid chromatographicInfrared lamp
Belonging to the field of water-soluble polymer material synthesis, the invention provides a preparation method of high-water solubility polyacrylamide. The preparation method of the high-water solubility polyacrylamide includes the specific steps of: preparing a composite initiator, preparing raw materials for polymerization to form a preparation auxiliary material, dissolving the auxiliary materials in distilled water in a three-necked bottle to prepare an acrylamide solution, adding nitrogen into the acrylamide solution for reaction to form a reactant, pouring the reactant into a beaker toobtain a white solid, drying the obtained white solid under an infrared lamp, conducting detection, storage and warehousing. The method has the characteristics of complete reaction, no by-product or impurities, and no environmental pollution. The acrylamide involved in the invention does not contain metal copper ions, ion exchange is not needed for removal of copper ions generated in the production process, and the process flow is simplified, in addition, gas chromatography analysis indicates that the acrylamide product almost does not contain free acrylonitrile and has high purity.
Owner:WUDI RONGYE NET CO LTD

3D honeycomb type paint mist filter bag and preparation method thereof

InactiveCN113499647AStrong resilienceSimple structureOther chemical processesDispersed particle filtrationCarboxymethyl starchGlass fiber
The invention discloses a 3D honeycomb type paint mist filter bag and a preparation method thereof. The preparation method comprises the four steps of preparing pyrrole-based polystyrene, preparing pyrrole-based polystyrene cross-linked glass fibers, preparing a 3D honeycomb type filter material and preparing the paint mist filter bag. According to the invention, acrylamide, polyvinyl alcohol and the pyrrole-based polystyrene cross-linked glass fibers are compounded to obtain the 3D honeycomb type filter material, the filter material is endowed with good recovery capacity through the dynamic ionic cross-linking effect of hydroxyl and borate ions of polyvinyl alcohol, and the pyrrole-based polystyrene cross-linked glass fibers and the polyvinyl alcohol form a good 3D network structure. In addition, carboxymethyl starch and acrylamide form a layer of compact composite filter membrane on the surfaces of the glass fibers, and the 3D honeycomb type filter material can be effectively fixed on the surfaces of the glass fibers. Meanwhile, the compactness and the connection strength of the glass fibers are enhanced, and the network structure of the 3D honeycomb type filter material and abundant pore structures on the surfaces of the glass fibers are beneficial to adsorption of paint mist.
Owner:深创高新产业研究中心(深圳)有限公司

Waterproof material for polystyrene boards and gypsum boards of building walls

InactiveCN110951329AEliminate anti-alkaliInhibit sheddingWax coatingsCellulosePolystyrene
The invention discloses a waterproof material for polystyrene boards and gypsum boards of building walls. The waterproof material is prepared from the following raw materials in parts by weight: 8-10parts of cement clinker, 6-10 parts of quick lime, 10-15 parts of a polyethylene emulsion, 15-20 parts of a paraffin emulsion, 4-8 parts of glass fibers, 3-6 parts of borax, 3-6 parts of sodium alginate, 3-5 parts of a grinding aid, 3-4 parts of sodium methyl silicate, 2-6 parts of hydroxyethyl cellulose, 2-4 parts of sodium tripolyphosphate, 2-4 parts of triethanolamine, 2-3 parts of aluminum potassium sulfate, 2-3 parts of dodecyl ethyoxyl sulphobetaine, 1-3 parts of polyacrylamide, 1-2 parts of calcium lignosulphonate and 50-80 parts of water. During construction, only 1mm of the material needs to be smeared on a polystyrene board wall body and a gypsum board wall body, after air drying, the surface layer of the wall surface is cleaned and polished to be flat, construction is convenient, time and labor are saved, the polystyrene board wall body and the gypsum board wall body treated through the material can completely eradicate the phenomena of alkali efflorescence, falling, moisture regain, mildewing and hollowing of the wall bodies, the service life of the polystyrene board and the gypsum board of the building wall body is greatly prolonged, and the cost is low.
Owner:天津志清建筑工程有限公司
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