3D honeycomb type paint mist filter bag and preparation method thereof
A paint mist filtration, honeycomb technology, applied in the direction of filtration separation, membrane filter, separation method, etc., can solve the problem of poor paint mist adsorption effect, etc., and achieve the effect of enhancing compactness and connection strength
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Embodiment 1
[0026] A preparation method of a 3D honeycomb paint mist filter bag, comprising the steps of:
[0027] (1) Preparation of pyrrolyl polystyrene: Add 100 g of styrene and 15 g of 1-(4-vinylbenzyl) pyrrolidine to 400 g of hexane solvent, stir to dissolve, then add 30 g of tetramethylethylenediamine and 18 g of n-Butyllithium, carry out polymerization reaction at 80°C for 3 hours, after the reaction is completed, add ethanol to the solvent, evaporate the solvent to dryness, and obtain pyrrolyl polystyrene;
[0028] (2) Preparation of pyrrolyl polystyrene cross-linked glass fiber: take 80g of pyrrolyl polystyrene obtained in step (1) and dissolve it in 600g of carbon tetrachloride, then add 120g of glass fiber to it, after ultrasonic dispersion is uniform, Then add 40g of aluminum chloride to it, carry out crosslinking reaction at 85°C for 24h, after the reaction is finished, filter, wash and dry the reaction product to obtain pyrrolyl polystyrene crosslinked glass fiber;
[0029] (3
Embodiment 2
[0032] A preparation method of a 3D honeycomb paint mist filter bag, comprising the steps of:
[0033] (1) Preparation of pyrrolyl polystyrene: Add 100 g of styrene and 20 g of 1-(4-vinylbenzyl) pyrrolidine to 400 g of hexane solvent, stir to dissolve, then add 35 g of tetramethylethylenediamine and 20 g of n-Butyllithium, carry out polymerization reaction at 60°C for 2 hours, after the reaction is completed, add ethanol to the solvent, evaporate the solvent to dryness, and obtain pyrrolyl polystyrene;
[0034] (2) Preparation of pyrrolyl polystyrene cross-linked glass fiber: take 90g of pyrrolyl polystyrene obtained in step (1) and dissolve it in 800g of carbon tetrachloride, then add 130g of glass fiber to it, and after ultrasonic dispersion is uniform, Then add 50g of aluminum chloride therein, carry out crosslinking reaction at 80°C for 26h, after the reaction is finished, filter, wash and dry the reaction product to obtain pyrrolyl polystyrene crosslinked glass fiber;
[00
Embodiment 3
[0038] A preparation method of a 3D honeycomb paint mist filter bag, comprising the steps of:
[0039] (1) Preparation of pyrrolyl polystyrene: Add 100 g of styrene and 30 g of 1-(4-vinylbenzyl) pyrrolidine to 400 g of hexane solvent, stir to dissolve, then add 32 g of tetramethylethylenediamine and 19 g of n-Butyllithium, carry out polymerization reaction at 70°C for 3 hours, after the reaction is completed, add ethanol to the solvent, evaporate the solvent to dryness, and obtain pyrrolyl polystyrene;
[0040](2) Preparation of pyrrolyl polystyrene cross-linked glass fiber: Weigh 80 g of pyrrolyl polystyrene obtained in step (1) and dissolve in 900 g of carbon tetrachloride, then add 130 g of glass fiber to it, and after ultrasonic dispersion is uniform, Then add 45g of aluminum chloride therein, carry out cross-linking reaction at 90°C for 24 hours, after the reaction is finished, filter, wash and dry the reaction product to obtain pyrrolyl polystyrene cross-linked glass fiber;
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