Transparent polyimide film
a polyimide film and transparent technology, applied in the direction of coatings, etc., can solve the problems of poor dimensional stability of metal lines attached to the polyimide film, insufficient heat stability, adverse effects,
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example 1
[0024][Preparation of a Copolymerized Polyamide Acid Solution]
[0025]20.1 g of TFMB (0.0627 mole, 0.315 of the total diamine molar ratio) is added to 412.5 g of DMAc, 11.723 g of CBDA (0.0598 mole, 30% of the total anhydride molar percentage) is added after complete dissolution, and the reaction is performed for 6 h while stirring, and the temperature is continuously maintained at 25° C. to obtain a semi-aromatic polyamide acid solution. 43.711 g of TFMB (0.1365 mole) is added to the semi-aromatic polyamide acid solution and is stirred until being completely dissolved, and 61.965 g of 6FDA (0.1395 mole) is added, and dissolution and reaction are performed after stirring for a certain period of time, and the temperature of the solution is maintained at 25° C., to finally obtain the copolymerized polyamide acid solution having a solid content of 25%.
[0026][Preparation of a Transparent Polyimide Film]
[0027]54.4 g of the copolymerized polyamide acid solution is taken out, and the solid cont
example 2
[0029][Preparation of a Copolymerized Polyamide Acid Solution]
[0030]27.800 g of TFMB (0.0868 mole, 0.42 of the total diamine molar ratio) is added to 412.5 g of DMAc, 16.214 g of CBDA (0.0827 mole, 40% of the total anhydride molar percentage) is added after complete dissolution, and the reaction is performed for 6 h with stirring, and the temperature is continuously maintained at 25° C. to obtain a semi-aromatic polyamide acid solution. 38.391 g of TFMB (0.120 mole) is added to the semi-aromatic polyamide acid solution and is stirred until completely dissolved, and 55.094 g of 6FDA (0.124 mole) is added, and dissolution and reaction are performed after stirring for a certain period of time, and the temperature of the solution is maintained at 25° C., to finally obtain the copolymerized polyamide acid solution having a solid content of 25%.
[0031][Preparation of a Transparent Polyimide Film]
[0032]54.4 g of the copolymerized polyamide acid solution is taken out, and the solid content is d
example 3
[0033][Preparation of a Copolymerized Polyamide Acid Solution]
[0034]42.972 g of TFMB (0.1342 mole, 0.625 of the total diamine molar ratio) is added to 412.5 g of DMAc, 21.053 g of CBDA (0.1074 mole, 50% of the total anhydride molar percentage) is added after complete dissolution, and the reaction is performed for 6 h with stirring, and the temperature is continuously maintained at 25° C. to obtain a semi-aromatic polyamide acid solution. 25.783 g of TFMB (0.0805 mole) is added to the semi-aromatic polyamide acid solution and is stirred until completely dissolved, and 47.691 g of 6FDA (0.1074 mole) is added, and dissolution and reaction are performed after stirring for a certain period of time, and the temperature of the solution is maintained at 25° C., to finally obtain the copolymerized polyamide acid solution having a solid content of 25%.
[0035][Preparation of a Transparent Polyimide Film]
[0036]54.4 g of the copolymerized polyamide acid solution is taken out, and the solid content i
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