Multifunctional gas high-pressure in situ Raman test cell and application thereof

An in-situ Raman and test cell technology, applied in Raman scattering, material excitation analysis, etc., can solve the problems of no discovery, few types of in-situ monitoring accessories for Raman spectroscopy, etc., to achieve good performance and expand research fields. Effect

Inactive Publication Date: 2015-12-09
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The use of in-situ Raman spectroscopy under extreme conditions to study the special structure and properties of materials has made great progress, but limited to the harsh requirements of extreme conditions for equipment and accessories, there are still few ty

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0052] Example 1,

[0053] A multifunctional gas high-pressure in-situ Raman test cell, comprising an outer high-pressure cylinder 4, an inner high-pressure cylinder 8 is arranged in the outer high-pressure cylinder 4, and a window 5 is arranged at the front end of the inner high-pressure cylinder 8; The end of the inner high-pressure cylinder 8 extends outside the outer high-pressure cylinder 4, and is fixedly connected to the end of the outer high-pressure cylinder 4 through a fastener 14; the high-pressure gas source passes through the inner high-pressure cylinder 8 to the The front end of the inner high pressure cylinder 8 presses the sample 6 to the window 5.

Example Embodiment

[0054] Example 2,

[0055] A multifunctional gas high-pressure in-situ Raman test cell as described in Example 1, the difference is that a thermocouple hole 11 is provided in the outer high-pressure cylinder 4 for the insertion of the thermocouple.

[0056] A heating part is provided outside the outer high-pressure cylinder 4. The heating part is a heating tube 9.

[0057] An insulation layer 10 is also provided on the outer side of the outer high-pressure cylinder 4.

Example Embodiment

[0058] Example 3.

[0059] A multifunctional gas high-pressure in-situ Raman test cell as described in Example 1, the difference is that a height-adjustable base is provided at the bottom of the outer high-pressure cylinder 4. The height-adjustable base is made of insulating material.

[0060] The height-adjustable base includes a base 3, a connecting screw 1 and a fine adjustment nut 2.

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PUM

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Abstract

A multifunctional gas high-pressure in situ Raman test cell comprises an external high pressure cylinder, an internal high pressure cylinder is arranged in the external high pressure cylinder, and the front end of the internal high pressure cylinder is provided with a diaphragm; the tail end of the internal high pressure cylinder is arranged outside the external high pressure cylinder in an extension manner, and is fixedly connected with the tail end of the external high pressure cylinder through a fastener; and a high pressure gas source goes through the internal high pressure cylinder to the front end of the internal high pressure cylinder in order to press a sample to the diaphragm. The test cell can realize in situ test of the Raman spectrum of a material under high temperature, high pressure, special atmosphere, laser irradiation and other extreme conditions. The test cell can be used to test a powder, a block, a high temperature melt, a film and various forms of samples. The test cell can continuously monitor the Raman spectrum of the material in an in-situ manner in the heating, pressurizing and atmosphere changing process in order to realize continuous in-situ tracking of the structure change, the stability and the chemical reaction process of the material.

Description

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Claims

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Application Information

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Owner SHANDONG UNIV
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