Super-hydrophobic coating containing candle soot and preparation method of same

A technology of super-hydrophobic coating and hydrophobic coating, applied in the application field, can solve the problems of harsh preparation conditions, unsuitable for industrial production, cumbersome steps, etc., and achieve the effects of wide range of uses, simple method and good adhesion

Inactive Publication Date: 2016-04-27
HUBEI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Nowadays, many superhydrophobic materials are prepared with cumbersome steps or harsh preparation conditions. These methods usually prepare nanoparticles first, and then modify them. Some even use expensive carbon nanotubes to improve

Method used

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  • Super-hydrophobic coating containing candle soot and preparation method of same
  • Super-hydrophobic coating containing candle soot and preparation method of same
  • Super-hydrophobic coating containing candle soot and preparation method of same

Examples

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Example Embodiment

[0023] Example 1

[0024] Preparation of a super-hydrophobic coating containing candle soot:

[0025] S1. The deposition of candle soot on the surface of the glass substrate: After the glass slide (rectangular, 7.6cm*2.6cm) is washed and dried, the surface that needs to be prepared with a hydrophobic coating covers 1 / 3 to 1 of the burning candle / 2 flame and move the glass slide until the surface where the hydrophobic coating needs to be prepared is evenly covered with a layer of candle soot, and the thickness of this layer of candle soot is about 2 μm;

[0026] S2. Preparation of super-hydrophobic coating by vapor deposition: Put the glass slide covered with candle soot prepared in S1 into a cylindrical crucible (diameter 10cm, height 2cm), and add 0.15mL to the crucible (0.44mmol) liquid perfluorodecyltrichlorosilane, heated to 224°C to completely transform the liquid perfluorodecyltrichlorosilane into gaseous state, the concentration of gaseous perfluorodecyltrichlorosilane in a

Example Embodiment

[0027] Example 2

[0028] Preparation of a super-hydrophobic coating containing candle soot:

[0029] S1. The deposition of candle soot on the surface of the glass substrate: After the glass slide (rectangular, 7.6cm*2.6cm) is washed and dried, the surface that needs to be prepared with a hydrophobic coating covers 1 / 3 to 1 of the burning candle / 2 flame and move the glass slide until the surface where the hydrophobic coating needs to be prepared is evenly covered with a layer of candle soot, the thickness of this layer of candle soot is about 3.5 μm; figure 1 Is the scanning electron microscope image of the candle soot deposited on the glass slide. figure 1 It can be seen that the candle soot forms a nano-sized rough structure on the surface of the glass slide.

[0030] S2. Preparation of super-hydrophobic coating by vapor deposition: Put the glass slide covered with candle soot prepared in S1 into a cylindrical crucible (diameter 10cm, height 2cm), and add 0.3mL to the crucible (

Example Embodiment

[0031] Example 3

[0032] Preparation of a super-hydrophobic coating containing candle soot:

[0033] S1. The deposition of candle soot on the surface of the glass substrate: After the glass slide (rectangular, 7.6cm*2.6cm) is washed and dried, the surface that needs to be prepared with a hydrophobic coating covers 1 / 3 to 1 of the burning candle / 2 flame and move the glass slide until the surface where the hydrophobic coating needs to be prepared is evenly covered with a layer of candle soot, the thickness of this layer of candle soot is about 5 μm;

[0034] S2. Preparation of super-hydrophobic coating by vapor deposition: Put the glass slide covered with candle soot prepared in S1 into a cylindrical crucible (diameter 10cm, height 2cm), and add 0.5 mL to the crucible (1.47mmol) Liquid perfluorodecyltrichlorosilane, heated to 230°C to completely transform the liquid perfluorodecyltrichlorosilane into gaseous state, the concentration of gaseous perfluorodecyltrichlorosilane in a clo

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Abstract

The invention belongs to the application fields of self-cleaning and waterproofing and the like, and particularly relates to a super-hydrophobic coating containing candle soot and the preparation method of the super-hydrophobic coating. Compared with the prior art, the method disclosed by the invention uses candle soot to manufacture roughness on the surfaces of glass, steel or ceramic base materials; the method is simple, no special equipment is needed, the operation is simple, convenient and fast; a large number of super-hydrophobic materials can be manufactured in a short time; the carbon which is not burned completely forms spinous bulges on the base material automatically, so that enough roughness is provided for the material, and the enough roughness is in favor of achieving super-hydrophobicity; perfluorodecyltrichlorosilane is deposited, in vapor manner, on the bulges and condensed into chemical bonds to fix the carbons which are only physically connected together, so that the durability is greatly enhanced; meanwhile, a part of the perfluorodecyltrichlorosilane permeates a loose candle soot layer to contact with the base material, so that the whole coating is firmer; the coating is applicable to a plurality of base materials and wide in application.

Description

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Claims

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Application Information

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Owner HUBEI UNIV
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