Extraction method of erythritol

An extraction method, erythritol technology, applied in the field of functional sugar processing and extraction, can solve the problems of many process control points, low cooling efficiency, high equipment cost, etc., and achieve the effect of simplifying the process flow, fast speed, and reducing equipment cost

Pending Publication Date: 2022-03-04
新疆苏源生物工程有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 1. The extraction period is long;
[0005] 2. Traditional ultrafiltration requires secondary investment in equipment, and the cost of equipment is high;
[0006] 3. It is easy to produce a large amount of crystal scale during cooling, and in order to control crystal scale, the general process adopts forced circulation and slow cooling. The general cooling time is 15h/batch, and

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A kind of extraction method of erythritol provided by the invention is characterized in that: comprise the following steps:

[0037] S1: After the fermentation liquid is inactivated, the temperature of the feed liquid is 70°C to 75°C, filter the clear liquid with a ceramic membrane filter element, and wait for use. Rinse the bacteria with pure water to 10g / L when the washing is complete, filter the same, and then mixed with serum;

[0038] S2: filter the clear liquid obtained in S1 with plate and frame carbon to remove some impurities in the clear liquid;

[0039] S3: Pour the clear liquid after carbon filtration in S2 into the decolorization tank, the temperature of the feed liquid is ≧70°C, and then add 3‰~5‰ powdered activated carbon, the stirring time is ≧0.5h, and then filter out the clear liquid with a plate frame;

[0040] S4: Use a multi-effect evaporator to condense the clear liquid after decolorization in S3 to 700g / L-800g / L, and send it out to the crystal

Embodiment 2

[0057] A kind of extraction method of erythritol provided by the invention is characterized in that: comprise the following steps:

[0058] S1: After the fermentation liquid is inactivated, the temperature of the feed liquid is 70°C, filter the clear liquid with a ceramic membrane filter element, and wait for use. Rinse the bacteria with pure water to 10g / L when the washing is over, filter in the same way, and then mix with the clear liquid mix;

[0059] S2: filter the clear liquid obtained in S1 with plate and frame carbon to remove some impurities in the clear liquid;

[0060] S3: Pour the clear liquid after carbon filtration in S2 into the decolorization tank, the temperature of the feed liquid is ≧70°C, then add 3‰ powdered activated carbon, the stirring time is ≧0.5h, and then filter out the clear liquid with a plate frame;

[0061] S4: condense the clear liquid after decolorization in S3 to 700g / L with a multi-effect evaporator, and go out to the crystallization tank;

Embodiment 3

[0078] A kind of extraction method of erythritol provided by the invention is characterized in that: comprise the following steps:

[0079] S1: After the fermentation liquid is inactivated, the temperature of the feed liquid is 72.5°C, filter the clear liquid with a ceramic membrane filter element, and wait for use. Rinse the bacteria with pure water to 10g / L when the washing is over, filter in the same way, and then mix with the clear liquid mix;

[0080] S2: filter the clear liquid obtained in S1 with plate and frame carbon to remove some impurities in the clear liquid;

[0081] S3: Pour the clear liquid after carbon filtration in S2 into the decolorization tank, the temperature of the feed liquid is ≧70°C, then add 4‰ powdered activated carbon, the stirring time is ≧0.5h, and then filter out the clear liquid with a plate frame;

[0082] S4: condense the clear liquid after decolorization in S3 to 750g / L with a multi-effect evaporator, and go out to the crystallization tank

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PUM

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Abstract

The invention relates to the technical field of functional sugar processing and extraction, and discloses an erythritol extraction method, which comprises the following steps: fermentation liquid preparation, ceramic membrane filtration, carbon filtration, decoloration, primary crystallization, dissolution and condensation, secondary crystallization, centrifugation, and drying and packaging, the original process flow requiring two times of dissolution and condensation is changed, the process flow is simplified, the production cost is reduced, and the production efficiency is improved. The defect of long extraction period of the original process is changed, the production cost is reduced, and the production efficiency is improved; ultrafiltration of a traditional process is replaced by carbon filtration, secondary investment of equipment is avoided, and the equipment cost is greatly reduced; through vacuum cooling, the speed is high, the defects of forced circulation, slow cooling and 15 h/batch cooling time of a traditional process are overcome, 5 h/batch of products in each batch can be controlled, and the crystal form is good.

Description

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Claims

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Application Information

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Owner 新疆苏源生物工程有限公司
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