Pressure-sensitive adhesive composition and pressure-sensitive adhesive sheet
a technology of pressure-sensitive adhesives and compositions, applied in the direction of film/foil adhesives without carriers, film/foil adhesives, adhesive types, etc., can solve the problems of deteriorating stability impaired appearance of pressure-sensitive adhesive sheets
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example 1
[0086]After 0.05 parts by mass of “IRGACURE 651” (product name, made by BASF) and 0.05 parts by mass of “IRGACURE 184” (product name, made by BASF), as photo-polymerization initiators, were blended and mixed into 100 parts by mass of 2-ethylhexyl acrylate (2EHA) as a monomer component, the mixture was irradiated with ultraviolet (UV) rays before the viscosity thereof (BH viscometer, No. 5 rotor, 10 rpm, measurement temperature: 30° C.) became approximately 9.0 Pa·s to produce a composition (syrup) in which part of the monomer component was polymerized. Thereafter, 1.00 part by mass (converted into solid content) of a fluorochemical surfactant (F-477 made by DIC Corporation) as a surfactant and 0.10 parts by mass of NK-Ester A-HD-N (made by SHIN-NAKAMURA CHEMICAL Co., Ltd.) as a cross-linking agent were added to the partially polymerized monomer syrup to produce a precursor of a pressure-sensitive adhesive composition (sometimes referred to as a “precursor A of a pressure-sensitive adhe
example 2
[0089]A precursor of a pressure-sensitive adhesive composition (sometimes referred to as a “precursor B of a pressure-sensitive adhesive composition”) was produced in the same way as in Example 1, except that 91.5 parts by mass of 2-ethylhexyl acrylate (2EHA), 7 parts by mass of N-vinyl-2-pyrrolidone (NVP), and 1.5 parts by mass of N-(2-hydroxyethyl)acrylamide (HEAA) were used as monomer components. After the monomer components and the photo-polymerization initiators were mixed together, the mixture was irradiated with UV rays before the viscosity thereof (BH viscometer, No. 5 rotor, 10 rpm, measurement temperature: 30° C.) became approximately 9.8 Pa·s to produce a composition in which part of the monomer components were polymerized.
[0090]A pressure-sensitive adhesive composition (sometimes referred to as a “pressure-sensitive adhesive composition B”) was obtained in the same way as in Example 1, except that the precursor B of a pressure-sensitive adhesive composition was used. Furthe
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