Nano-crystalline NiAl-Al2O3-Y composite material and preparation method thereof
A composite material and nanocrystalline technology, which is applied in the field of nanocrystalline NiAl-Al2O3-Y composite material and its preparation, can solve the problems of reducing the oxidation resistance of NiAl and limiting its application
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[0006] 1. Mechanical alloying
[0007] Preparation of NiAl-Al by High Energy Ball Mill 2 o 3 In situ composite powder.
[0008] Select the nickel and aluminum element powders whose purity and particle size are 99.9% and 300 mesh respectively. According to the nominal ratio NiAl-(5~15)vol.%Al 2 o 3 Weigh nickel powder and aluminum powder and mix well. Then measure absolute ethanol according to 3-5% of the mass fraction of the mixed powder; add the prepared mixed powder and the measured absolute ethanol into the stirring high-energy ball mill, and the ball mill tank is cooled by circulating water. Ball mill under the condition of 250-280r / min. After 2 hours of ball milling, open the ball mill tank, let in air, and continue ball milling in the air atmosphere for 20 hours, and the mechanical alloying is completed. Obtain fully alloyed and grain-refined NiAl-Al 2 o 3 In situ composite material powder, Al in powder 2 o 3 The content varies according to the content of nickel
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