Process for preparing nylon salt and its polymerization

a technology of nylon salt and polymerization, which is applied in the field of process for preparing nylon salt, can solve the problems of complex unit operation setup, inability to prepare nylon salt in melt, and inability to meet the requirements of nylon salt preparation, etc., and achieves the effect of effective and efficien

Active Publication Date: 2020-03-17
DSM IP ASSETS BV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The technical effect of this patented method described by the inventor is that it allows for more precise control over how well different chemicals are used during production processes compared with previous methods such as mixing them together or adding other substances like plasticizers beforehand.

Problems solved by technology

The technical problem addressed in this patented solution relates how to improve upon existing methods for analyzing data from large amounts of data without sacrificing accuracy or efficiency.

Method used

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Embodiment Construction

[0021]The effect of the process according to the invention, comprising flashing of an aqueous salt mixture at elevated temperature, is that a solid salt in the form of a granular material is obtained in an effective and efficient manner. With the process the granular nylon salt material is obtained in a much faster and simpler manner than crystallization or spray drying. Less water is needed, also because a slurry can be used, and no controlled droplet size atomization is required. The aqueous mixture can be flashed by a flash valve having a relatively large opening, without the need of spray nozzles with a small opening, which significantly reduces the risk of blocking of the opening and also allows the use of slurries, which have a salt content well above the solubility level. Because of the high temperature and the relatively low water content, the water is evaporated adiabatically, or at least essentially so, without the need for applying a large countercurrent of heated inert gas.

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Abstract

The present invention relates to a process for preparing a granular nylon salt material, wherein an aqueous mixture, comprising at least 65 wt. % of salt components, and at most 35 wt. % of an aqueous medium, the weight percentages (wt. %) being relative to the total weight of the aqueous mixture, is flashed from a pressure vessel via a flash valve into a flash chamber, thereby evaporating the aqueous medium in an amount sufficient to result in a residual moisture content of at most 7.5 wt. %, and forming a granular nylon salt material. The invention also relates to a process for preparing a nylon polymer, comprising direct solid state polymerization of the granular salt material prepared by flash granulation.

Description

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Claims

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Application Information

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Owner DSM IP ASSETS BV
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