3 results about "Sample chamber" patented technology

The electrode for high-voltage in-situ impedance spectroscopy measurement of the present invention and its preparation method and application belong to the technical field of in-situ measurement of electrical quantities under high-voltage conditions. The electrode consists of an aluminum oxide protective layer (3) deposited on the surface of the diamond anvil (2) and a metal film electrode (1); the metal film electrode (1) is circular in the center of the anvil surface of the diamond anvil (2), Copper wire (5) is bonded to the metal film electrode (1) on the side of the diamond anvil (2); the metal spacer (4) is used as another electrode, forming an axisymmetric electrode together with the metal film electrode (1) system. Electrodes are prepared by magnetron sputtering, molybdenum coating, aluminum oxide deposition, photolithography and chemical corrosion. The invention solves the problems of electrode fixing and sample cavity insulation, and can ignore the influence of the parasitic capacitance and inductance of the system on the measurement results, making it possible to measure the material impedance spectrum in situ with the diamond anvil under high pressure.