Production method of vanadium nitrogen alloy

[0019] A production method of vanadium nitrogen alloy, the steps of the method are as follows:

[0020] a) Stir and mix the powdered vanadium-containing compound, carbonaceous reducing agent, binder and fluoride mineralizer evenly, and press to form a regular mixed billet, wherein the weight ratio of each component is:

[0021] The vanadium-containing compound uses 139 parts of vanadium pentoxide; the carbonaceous reducing agent uses 44 parts of graphite powder; the binder uses 14 parts of dextrin aqueous solution; the fluoride mineralizer uses 5 parts of sodium fluoride;

[0022] b) Put the obtained mixed blank into a heat-resistant stainless steel container under the protection of nitrogen atmosphere for carbonization reaction pretreatment to obtain a pretreated product, wherein the temperature of the carbonization reaction in the heat-resistant stainless steel container is kept at 590 ° C, and the carbonization reaction time is 3 hours;

[0023] c) Put the pretreated product

[0029] A production method of vanadium nitrogen alloy, the steps of the method are as follows:

[0030] a) Stir and mix the powdered vanadium-containing compound, carbonaceous reducing agent, binder and fluoride mineralizer evenly, and press to form a regular mixed billet, wherein the weight ratio of each component is:

[0031] The vanadium-containing compound uses 145 parts of ammonium metavanadate; the carbonaceous reducing agent uses 49 parts of carbon black powder; the binder uses 19 parts of starch aqueous solution; the fluoride mineralizer uses 1 part of potassium fluoride;

[0032] b) Put the obtained mixed blank into a heat-resistant stainless steel container under the protection of nitrogen atmosphere for carbonization reaction pretreatment to obtain a pretreated product, wherein the temperature of the carbonization reaction in the heat-resistant stainless steel container is kept at 775°C, and the carbonization reaction time is 9 hours;

[0033] c) Put the pretreated pr

[0039] A production method of vanadium nitrogen alloy, the steps of the method are as follows:

[0040] a) Stir and mix the powdered vanadium-containing compound, carbonaceous reducing agent, binder and fluoride mineralizer evenly, and press to form a regular mixed billet, wherein the weight ratio of each component is:

[0041] The vanadium-containing compound adopts 142 parts of vanadium pentoxide; the carbonaceous reducing agent adopts 47 parts of a mixture of graphite powder and carbon black powder; the binder adopts 16 parts of dextrin aqueous solution; the fluoride mineralizer adopts 4 parts of sodium fluoride;

[0042] b) Put the obtained mixed blank into a heat-resistant stainless steel container protected by a nitrogen atmosphere for carbonization reaction pretreatment to obtain a pretreated product, wherein the temperature of the carbonization reaction in the heat-resistant stainless steel container is kept at 650°C, and the carbonization reaction time is 5 hours;

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