Preparing method of flame-retardant mixed silicone rubber by utilization of platinum compound and vapor-phase-method white carbon black in combination

A technology of fumed white carbon black and silicone rubber mixing, which is applied in the field of rubber products, can solve the problems of poor performance of flame retardant mixing silicone rubber, etc., and achieve the effects of good flame retardant performance, convenient preparation, and positive color

Inactive Publication Date: 2014-11-26
李华顺
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The flame retardant compounded silicone rubb

Method used

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Examples

Experimental program
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Example Embodiment

[0011] Example 1

[0012] A method for preparing flame-retardant mixed silicone rubber by using platinum compound and fumed white carbon black together. The method steps are as follows:

[0013] a. In platinic acid, add vapor-phase white carbon black with a specific surface area of ​​50 square meters / g, and place it at room temperature for 10 hours after mixing to form a mixture of platinum compound and white carbon black;

[0014] b. Add fumed white carbon black, modifier and iron oxide with a specific surface area of ​​200㎡ / g to the methyl vinyl silicone rubber raw rubber with a degree of polymerization of 7000, mix it evenly in a kneader, and heat it at 150℃2 After hours, add the flame retardant additive gas phase titanium dioxide and the mixture of platinum compound and white carbon black and mix it evenly on a two-roll rubber mixer to form a rubber compound.

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Abstract

The invention relates to a preparing method of flame-retardant mixed silicone rubber by utilization of a platinum compound and vapor-phase-method white carbon black in combination, and relates to the technical field of rubber products. The preparing method includes: a) a step of adding vapor-phase-method white carbon black having a specific surface area of 50 m<2>/g into chloroplatinic acid, mixing, and allowing the mixture to stand at room temperature for 10 h to obtain a mixture of the platinum compound and the white carbon black; and b) a step of adding vapor-phase-method white carbon black having a specific surface area of 200 m<2>/g, a modifier and ferric oxide into methyl vinyl silicone raw rubber having a polymerization degree of 7000, uniformly mixing in a kneading machine, performing thermal processing at 150 DEG C for 2 h, adding a flame retardant auxiliary agent that is vapor-phase-method titanium dioxide and the mixture of the platinum compound and the white carbon black, and uniformly mixing at a double-roller rubber mixing machine to obtain a rubber material. The components are simple and preparation is convenient. By adding the platinum compound, the mixed silicone rubber is good in performance, free of odor, just right in color and good in flame retardant performance.

Description

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Claims

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Application Information

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Owner 李华顺
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