ncc‑g‑ech method to enhance EP performance
A performance, rectangular technology, applied in the field of NCC-g-ECH enhanced EP performance, can solve the problems of anti-peeling, anti-cracking and impact resistance, low dielectric constant and dielectric loss, stress cracking, etc., to achieve a wide range of applications , large industrial value, the effect of mild reaction conditions
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[0022] Example 1:
[0023] A method for NCC-g-ECH to enhance EP performance. The method includes the following steps:
[0024] (1) Alkalization of nanocellulose;
[0025] (2) Nano-cellulose grafted with epichlorohydrin;
[0026] (3) Blend the product after grafting into epoxy resin;
[0027] (4) Curing the blended epoxy resin.
Example Embodiment
[0028] Example 2:
[0029] According to the method of NCC-g-ECH to enhance EP performance as described in Example 1, the alkalization of nanocellulose: Take 1g of nanocellulose and pour into a three-necked flask, add 15ml of 95% ethanol-water solution, and add 15ml of 2%. The NaOH-aqueous solution was stirred at 65℃ for 1 h;
Example Embodiment
[0030] Example 3:
[0031] According to the method of NCC-g-ECH to enhance EP performance described in Example 1 or 2, the nanocellulose grafted with epichlorohydrin was injected into a three-necked flask with 2 ml of epichlorohydrin, and the mixture was stirred for 2 hours to prepare 70 % Isopropanol-water solution, repeatedly wash the grafted nanocellulose with the prepared isopropanol solution, and pour the washed white precipitate into a clean small beaker to dry;
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