Water purification flocculating agent prepared from urea, and preparation method thereof

A flocculant and urea technology, which is applied in the field of water purification flocculant and its preparation, can solve the problems of unfavorable large-scale promotion, high chroma residue, unstable performance, etc., and achieve remarkable treatment effect, high chroma removal rate, and drug use less effect

Inactive Publication Date: 2016-10-05
福建金东阳化工工贸有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Inorganic polymer flocculants and organic polymer flocculants are often used, but the product performance is unstable. In practical applications, there are p

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0017] Example 1

[0018] In the embodiment of the present invention, a water purification flocculant prepared by using urea is weighed 4 kg of urea, 50 kg of polyaluminum ferric chloride, 15 kg of silica, 36 kg of lignin, 25 kg of sodium hydroxide solution, and 11 kg of alum.

[0019] The preparation method of the composite water purification flocculant prepared by using urea, the specific steps include:

[0020] 1) Dissolve urea and alum in water to prepare solution A for later use. The amount of water added is 1 time the total mass of urea and alum;

[0021] 2) Add polyaluminum ferric chloride to the sodium hydroxide aqueous solution at room temperature and stir for 10 minutes to obtain B solution;

[0022] 3) Heat solution B to 75°C, add lignin at this temperature, stir for 30 minutes, add silica, and continue stirring for 15 minutes to obtain solution C;

[0023] 4) Pour solution A into solution C, lower the temperature to 55°C, stir for 1 hour and then cool to room temperature to obta

Example Embodiment

[0024] Example 2

[0025] In the embodiment of the present invention, a water purification flocculant prepared with urea is weighed: 7 kg of urea, 56 kg of polyaluminum ferric chloride, 18 kg of silica, 42 kg of lignin, 32 kg of sodium hydroxide aqueous solution, and 14 kg of alum.

[0026] The preparation method of the composite water purification flocculant prepared by using urea, the specific steps include:

[0027] 1) Dissolve urea and alum in water to prepare A solution for later use. The amount of water added is twice the total mass of urea and alum;

[0028] 2) Add polyaluminum ferric chloride to the aqueous sodium hydroxide solution at room temperature and stir for 15 minutes to obtain B solution;

[0029] 3) Heat solution B to 78°C, add lignin at this temperature, stir for 40 minutes, add silica, and continue stirring for 15 minutes to obtain solution C;

[0030] 4) Pour solution A into solution C, lower the temperature to 55°C, stir for 1 hour and then cool to room temperature to

Example Embodiment

[0031] Example 3

[0032] In the embodiment of the present invention, a water purification flocculant prepared by using urea is weighed separately: 10 kg of urea, 63 kg of polyaluminum ferric chloride, 22 kg of silica, 47 kg of lignin, 38 kg of sodium hydroxide solution, and 18 kg of alum.

[0033] The preparation method of the composite water purification flocculant prepared by using urea, the specific steps include:

[0034] 1) Dissolve urea and alum in water to prepare A solution for later use. The amount of water added is 3 times the total mass of urea and alum;

[0035] 2) Add polyaluminum ferric chloride to the sodium hydroxide aqueous solution at room temperature and stir for 20 min to obtain B solution;

[0036] 3) Heat solution B to 80°C, add lignin at this temperature, stir for 50 minutes, add silica, and continue stirring for 15 minutes to obtain solution C;

[0037] 4) Pour solution A into solution C, lower the temperature to 55°C, stir for 1 hour and then cool to room temperatu

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Abstract

The invention discloses a water purification flocculating agent prepared from urea, and a preparation method thereof. The water purification flocculating agent comprises, by weight, 4-10 parts of urea, 50-63 parts of polyaluminum ferric chloride, 15-22 parts of silica, 36-47 parts of lignin, 25-38 parts of a sodium hydroxide solution and 11-18 parts of alum. The preparation method comprises the following steps: dissolving urea and alum in water to prepare a solution A for later use; adding polyaluminum ferric chloride to an aqueous sodium hydroxide solution, heating the obtained aqueous solution, and adding lignin and silica to obtain a solution C; and pouring the solution A to the solution C, stirring the obtained mixed solution, and cooling the stirred solution to room temperature. Urea is used as a catalyst to promote the sewage treatment effect of polyaluminum ferric chloride, silica and lignin, so the water purification flocculating agent has a substantial treatment effect on printing and dyeing wastewater and other light industry wastewater, and has the advantages of high removal rate of suspensions, CODs and the chroma, small amount of produced sludge, and great improvement of the water quality of treated wastewater.

Description

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Claims

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Application Information

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Owner 福建金东阳化工工贸有限公司
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