Preparation method of Allium tenuissimum L. essential oil

A technology of fine-leaved leek and leek essence, which is applied in the directions of essential oils/spices, fat production, etc., can solve the problems of scattered distribution of wild fine-leaved leek, sharp increase in harvesting cost, and difficult harvesting, and achieve low implementation cost and separation Good effect, good safety effect

Inactive Publication Date: 2017-07-07
YULIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The present invent describes an improved process for extracting crude tall oils (or other valuable substances) from finely leafed plants like Leu tar). By combining these materials together through various methods such as heat treatment or solvation techniques, they can be separated into different fractions without damaging them during processing steps. This results in higher yields compared to traditional ways of separating crude vegetable products.

Problems solved by technology

This patented technical problem addressed in this patent relates to extracting valuable materials like carbohydrils, lignosulphiles, steroidal sapors, polysaccharide gums, tannery reserves, amlacipes seeds, nepetriolids, phytotherapy products containing these active ingredients.

Method used

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Effect test

Embodiment 2

[0024] The preparation method of Chinese chive essential oil of the present invention comprises the following steps: (1) picking the flower buds of Chinese chives that are about to open, and drying them in the shade; Mix at a ratio of 1:30 and add to the still; (3) use steam to heat the mixture in the still to boiling, continue heating, and control the evaporation rate in the still by adjusting the steam pressure connected to the coil, and control the steam pressure to 0.08MPa-0.12MPa, the distillation time is 3-4h; (4) Cooling water control: When the temperature in the still is 65°C, turn on the condenser and connect the cooling water; within 0.5h after boiling, use the cooling water The temperature of the effluent liquid cooled by the condenser is controlled at 20°C-25°C; after 0.5h, the temperature of the effluent liquid rises to 25°C-30°C and remains stable, and the oil-water mixture cooled by the condenser is introduced into the oil-water separator; oil-water separation The

Embodiment 3

[0026] The preparation method of the Chinese chive essential oil of the present invention comprises the following steps: (1) picking the flower buds of Chinese chives that are about to open; (2) mixing the fresh Chinese chive flower buds with a 0.7% salt solution in a mass ratio of 1: 10 mixed and added to the distillation kettle; (3) use steam to heat the mixture in the distillation kettle to boiling, continue heating, and control the evaporation rate in the distillation kettle by adjusting the steam pressure connected to the coil, and control the steam pressure to be 0.08 MPa~0.12MPa, the distillation time is 3-4h; (4) Cooling water control: When the temperature in the still is heated to 50°C, open the condenser and connect the cooling water; within 0.5h after boiling, use cooling water to The temperature of the effluent liquid cooled by the condenser is controlled at 20°C-25°C; after 0.5h, the temperature of the effluent liquid rises to 25°C-30°C and remains stable, and the oil

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PUM

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Abstract

The invention discloses a preparation method of Allium tenuissimum L. essential oil. The method comprises the following steps: (1) picking Allium tenuissimum L. flower buds, and adding the Allium tenuissimum L. flower buds and a 0.5 to 2.5 percent by mass table salt solution into a distillation kettle together; (2) heating a mixture in the distillation kettle to a boiling state with steam, and performing distillation; (3) when the temperature in the kettle is 50 to 70 DEG C, introducing cooling water, controlling the temperature of liquid flowing out of a condenser at 20 to 25 DEG C through the cooling water after boiling, heating the effluent liquid to 25 to 30 DEG C 0.5 hour later, and introducing the heated effluent liquid into an oil-water separator; (4) returning distillate separated by the oil-water separator into the distillation kettle by reflowing, wherein reflowing lasts for 3 to 4 hours; (5) after oil and water are delaminated fully, opening the oil-water separator, and collecting an oil layer to obtain the Allium tenuissimum L. essential oil. The plant essential oil prepared by the method is closer to the natural fragrance of the Allium tenuissimum L. flower buds, and the quality, yield and purity of the Allium tenuissimum L. essential oil are ensured.

Description

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Claims

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Application Information

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Owner YULIN UNIV
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