Coffee slag valuable component separation and recovery method and application

A technology for separation and recovery of coffee grounds, applied in chemical instruments and methods, organic chemistry, inorganic chemistry, etc., can solve the problems of not having good environmental, economic and social benefits, and achieve the effects of simple operation, resource saving and cost saving

Inactive Publication Date: 2018-04-10
GUANGDONG POLYTECHNIC OF ENVIRONMENTAL PROTECTION ENG
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, research on coffee grounds at home and abroad is in its infancy, mainly focusing on component analysis, component extraction, pyrolysis k

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0027] Example 1

[0028] The present embodiment provides a method for separating and recovering valuable components of coffee grounds, which mainly includes:

[0029] Wash and dry coffee grounds. The dried coffee grounds are placed in a pyrolysis activation device, and under the condition of a pyrolysis pressure of -0.02Mpa, the temperature is raised to 190 ° C, so that the coffee grounds are pyrolyzed at this temperature, and the constant temperature is pyrolyzed for 20 minutes. secondary pyrolysis products.

[0030] After the first pyrolysis, the second and third pyrolysis were carried out.

[0031] Under the condition that the pyrolysis pressure is -0.01Mpa, the temperature is continued to be raised to 290° C., constant temperature pyrolysis is performed for 20 minutes, and the second pyrolysis product is separated and recovered. After the recovery, under the condition that the pyrolysis pressure is -0.01MPa, the temperature is continued to be raised to 390° C., constant t

Example Embodiment

[0033] Example 2

[0034] The present embodiment provides a method for separating and recovering valuable components of coffee grounds, which mainly includes:

[0035] Wash and dry coffee grounds. The dried coffee grounds are placed in a pyrolysis activation device, and under the condition of a pyrolysis pressure of -0.09Mpa, the temperature is raised to 210 ° C, so that the coffee grounds are pyrolyzed at this temperature, and the constant temperature is pyrolyzed for 40 minutes. secondary pyrolysis products.

[0036] After the first pyrolysis, the second and third pyrolysis were carried out.

[0037] Under the condition that the pyrolysis pressure is -0.09Mpa, the temperature is continued to be raised to 310°C, constant temperature pyrolysis is carried out for 40min, and the second pyrolysis product is separated and recovered. After the recovery, under the condition that the pyrolysis pressure is -0.09Mpa, the temperature is continued to be raised to 410° C., constant temper

Example Embodiment

[0039] Example 3

[0040] The present embodiment provides a method for separating and recovering valuable components of coffee grounds, which mainly includes:

[0041] Wash and dry coffee grounds. The dried coffee grounds are placed in a pyrolysis activation device, and under the condition of a pyrolysis pressure of -0.07Mpa, the temperature is raised to 205 ° C, so that the coffee grounds are pyrolyzed at this temperature, and the constant temperature is pyrolyzed for 35 minutes. secondary pyrolysis products.

[0042] After the first pyrolysis, the second and third pyrolysis were carried out.

[0043] Under the condition of the pyrolysis pressure of -0.08Mpa, the temperature was continued to rise to 305°C, and the thermolysis was performed at a constant temperature for 35min, and the second pyrolysis product was separated and recovered. After the recovery, under the condition that the pyrolysis pressure is -0.08Mpa, the temperature is continued to be raised to 405° C., constant

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PUM

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Abstract

The invention provides a coffee slag valuable component separation and recovery method and application, and relates to the field of comprehensive utilization of coffee slag. The coffee slag valuable component separation and recovery method comprises pyrolyzing the dried coffee slag at least twice, to be more specific, pyrolyzing the coffee slag under the condition of 190-210DEG C, separating and recovering a first pyrolysis product preferably including caffeine; continuing heating up, pyrolyzing the firstly-pyrolyzed coffee slag under the condition of 290 to 410 DEG C for pyrolysis for at least one time, and respectively separating and recovering pyrolysis products; continuing heating up, and using water vapor to activate the pyrolyzed pyrolysis slag. The method is easy to operate, highly-controllable, reusable in resources, and environmentally-friendly, can be used for mass production. According to the application of the coffee slag valuable component separation and recovery method, the caffeine and pyrolysis oil can be recovered, and the application range of the coffee slag can be broadened.

Description

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Claims

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Application Information

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Owner GUANGDONG POLYTECHNIC OF ENVIRONMENTAL PROTECTION ENG
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