Medical aluminum oxide ceramic compound material and preparation method thereof
A technology of alumina ceramics and composite materials, which is applied in the field of biomedical materials, can solve the problems of reduced strength of porous alumina ceramics and mechanical strength of ceramics, and achieves the effects of good wear resistance, low cost, and less raw material addition
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Embodiment 1
[0020] A medical alumina ceramic composite material and a preparation method thereof, comprising the following steps: uniformly mixing 99% vol alumina ceramics and 0.15% vol graphene, pressing into a green body, and cooling the green body after sintering at 1550°C.
[0021] The particle size of the alumina ceramic is 150nm.
[0022] The graphene has a thickness of 8nm and a diameter of 20um.
[0023] The mixing is carried out using a ball mill at a speed of 300 r / min for 3 hours.
[0024] The pressing is carried out by a cold isostatic press with a pressure of 300 MPa.
[0025] The relative density of the green body is 55%.
[0026] The sintering time is 3h.
[0027] The temperature was raised to the sintering temperature at 5°C / min.
[0028] During the sintering, a nitrogen-hydrogen mixed gas is introduced, and the nitrogen-hydrogen mixed gas contains 95% vol nitrogen and 5% vol hydrogen.
Embodiment 2
[0030] A medical alumina ceramic composite material and a preparation method thereof, comprising the following steps: uniformly mixing 99.75% vol alumina ceramics and 2% vol graphene, pressing into a green body, and cooling the green body after sintering at 1600°C.
[0031] The particle size of the alumina ceramic is 100 nm.
[0032] The graphene has a thickness of 6nm and a diameter of 15um.
[0033] The mixing is carried out using a ball mill at a speed of 200 r / min for 2 hours.
[0034] The pressing is carried out by a cold isostatic press with a pressure of 200 MPa.
[0035] The relative density of the green body is 45%.
[0036] The sintering time is 2h.
[0037] The temperature was raised to the sintering temperature at 5°C / min.
[0038] During the sintering, an argon-hydrogen mixed gas is introduced, and the argon-hydrogen mixed gas contains 95% vol of argon and 5% vol of hydrogen.
[0039] In summary, it can be seen that the medical alumina ceramic composite mate
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