Medical aluminum oxide ceramic compound material and preparation method thereof

A technology of alumina ceramics and composite materials, which is applied in the field of biomedical materials, can solve the problems of reduced strength of porous alumina ceramics and mechanical strength of ceramics, and achieves the effects of good wear resistance, low cost, and less raw material addition

Inactive Publication Date: 2019-04-05
周琪
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology allows for better control over how well an implant made from this new type of metal oxides works when placed near body parts that are prone to damage during surgery such as hip joints. It also improves its durability against environmental factors (humidity) while maintaining their effectiveness.

Problems solved by technology

This patented technical solution describes various types of ceramsurgery techniques involving use of biomaterials like calcium phosphate (CaP) ceramies and metals called platins. These ceramices provide excellent physical properties including flexion durability without losing its ability to bond within human hard tissues. Additionally, some ceramicians prefer to avoid damaging surrounding structures while others want to maintain healthy blood vessels through surgery procedures. Therefore, the focus on improving the compatibility of certain ceramites towards different applications needs remains unexplored despite advances in understanding them over recent decades.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A medical alumina ceramic composite material and a preparation method thereof, comprising the following steps: uniformly mixing 99% vol alumina ceramics and 0.15% vol graphene, pressing into a green body, and cooling the green body after sintering at 1550°C.

[0021] The particle size of the alumina ceramic is 150nm.

[0022] The graphene has a thickness of 8nm and a diameter of 20um.

[0023] The mixing is carried out using a ball mill at a speed of 300 r / min for 3 hours.

[0024] The pressing is carried out by a cold isostatic press with a pressure of 300 MPa.

[0025] The relative density of the green body is 55%.

[0026] The sintering time is 3h.

[0027] The temperature was raised to the sintering temperature at 5°C / min.

[0028] During the sintering, a nitrogen-hydrogen mixed gas is introduced, and the nitrogen-hydrogen mixed gas contains 95% vol nitrogen and 5% vol hydrogen.

Embodiment 2

[0030] A medical alumina ceramic composite material and a preparation method thereof, comprising the following steps: uniformly mixing 99.75% vol alumina ceramics and 2% vol graphene, pressing into a green body, and cooling the green body after sintering at 1600°C.

[0031] The particle size of the alumina ceramic is 100 nm.

[0032] The graphene has a thickness of 6nm and a diameter of 15um.

[0033] The mixing is carried out using a ball mill at a speed of 200 r / min for 2 hours.

[0034] The pressing is carried out by a cold isostatic press with a pressure of 200 MPa.

[0035] The relative density of the green body is 45%.

[0036] The sintering time is 2h.

[0037] The temperature was raised to the sintering temperature at 5°C / min.

[0038] During the sintering, an argon-hydrogen mixed gas is introduced, and the argon-hydrogen mixed gas contains 95% vol of argon and 5% vol of hydrogen.

[0039] In summary, it can be seen that the medical alumina ceramic composite mate

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Abstract

The invention discloses a medical aluminum oxide ceramic compound material and a preparation method thereof. The preparation method of the medical aluminum oxide ceramic compound material comprises uniformly mixing 98-99.75% vol aluminum oxide ceramics with 0.25-2% vol graphene, pressing the mixture into a blank, and then sintering the blank at 1450-1650 DEG C and cooling down to obtain the medical aluminum oxide ceramic compound material. The medical aluminum oxide ceramic compound material has the advantages of being less prone to ageing, good in wearing resistance, bending strength, breaking tenacity and biocompatibility and the like. Traditional aluminum oxide added zirconium oxide materials are significantly reduced in mechanical performance during long-term application at 100-400 DEGC particularly in damp conditions and accordingly form microcosmic or macroscopic cracks on the surface.

Description

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Claims

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Application Information

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Owner 周琪
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