Slag-corrosion-resistant lightweight alumina clinker and preparation method thereof

A bauxite clinker and light-weight technology, which is applied in the field of slag corrosion-resistant lightweight bauxite clinker and its preparation, can solve the problems of high cost, large pore size, and large pore size of microporous lightweight bauxite refractory aggregate. Achieve the effect of improving anti-slag ability, improving material strength and low production cost

Active Publication Date: 2021-02-05
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology allows for creation of durable fireproof plugs made up mainly of sintered or pressed balsafe calcium magnesia (BSCM) powders that exhibit excellent properties such as reduced costs, ease of manufacturing processes, flexibility in design options, etc., making it suitable for various applications like water supply systems where there may occur severe environmental conditions.

Problems solved by technology

This patent describes different methods or techniques related to making light weight ceramic material called fine porous refractories from hydrated magnesia crystal powder. These processes involve dry milling and burning them under specific conditions while maintaining their stability during use. However, these technical problem addressed by the patents involves improving the performance of lightweighness refractors made up mostly heavy metal ingredients like molybdenum oxide and tungsten carbons due to environmental concerns associated with mineral resources usage.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A slag corrosion-resistant lightweight alumina clinker and a preparation method thereof. The preparation method of this embodiment is:

[0024] Using 89wt% bauxite raw meal micropowder, 7wt% carbon black and 4wt% plant ash as raw materials; first mix the raw materials uniformly in a planetary ball mill, and then machine press them under 200MPa to obtain a green body; then The green body was dried at 200°C for 12 hours, and kept at 1550°C under the condition of carbon embedding for 8 hours to obtain slag corrosion-resistant lightweight bauxite clinker.

[0025] The slag corrosion-resistant lightweight bauxite clinker prepared in this example is tested: the bulk density is 2.71g / cm 3 ; The average pore diameter is 495nm; the erosion index of the anti-slag test of 1600 ℃ immersion method is 5%, and the permeability index is 15%.

Embodiment 2

[0027] A slag corrosion-resistant lightweight alumina clinker and a preparation method thereof. The preparation method of this embodiment is:

[0028] Using 90wt% bauxite raw meal powder, 9wt% carbon black and 1wt% plant ash as raw materials; firstly mix the raw materials uniformly in a planetary ball mill, and then machine press them under the condition of 160MPa to obtain a green body; then The green body was dried at 160°C for 24 hours, and kept at 1650°C under the condition of carbon embedding for 6 hours to obtain slag corrosion-resistant lightweight bauxite clinker.

[0029] The slag corrosion-resistant lightweight bauxite clinker prepared in this example is tested: the bulk density is 2.84g / cm 3 ; The average pore size is 426nm; the erosion index of the anti-slag test by immersion method at 1600°C is 5%, and the permeability index is 14%.

Embodiment 3

[0031] A slag corrosion-resistant lightweight alumina clinker and a preparation method thereof. The preparation method of this embodiment is:

[0032] Using 94wt% bauxite raw meal micropowder, 4wt% carbon black and 2wt% plant ash as raw materials; first mix the raw materials uniformly in a planetary ball mill, and then machine press them under the condition of 150MPa to obtain a green body; then The green body was dried at 150°C for 18 hours, and kept at 1600°C under the condition of carbon embedding for 5 hours to obtain slag corrosion-resistant lightweight bauxite clinker.

[0033] The slag corrosion-resistant lightweight bauxite clinker prepared in this example is tested: the bulk density is 2.94g / cm 3 ; Average pore size is 316nm; 1600 ℃ immersion method slag resistance test erosion index is 3%, permeability index is 12%.

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Abstract

The invention relates to a slag-corrosion-resistant lightweight alumina clinker and a preparation method thereof. According to a technical scheme in the invention, the preparation method comprises thefollowing steps: with 89-97 wt% of raw alumina micropowder, 1-9 wt% of carbon black and 0.1-4 wt% of plant ash as raw materials, uniformly mixing the raw materials in a planetary ball mill, and carrying out mechanical pressing under the condition of a pressure of 100-200 MPa to obtain a green body; and drying the green body at 110-200 DEG C for 12-36 hours, and carrying out heat preservation at 1550-1750 DEG C under a carbon burying condition for 3-8 hours to obtain the slag-corrosion-resistant lightweight alumina clinker. The method is low in cost and simple in process, and the prepared slag-corrosion-resistant light-weight alumina clinker has the characteristics of small pore diameter, high strength and strong slag resistance.

Description

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Claims

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Application Information

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Owner WUHAN UNIV OF SCI & TECH
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