Preparation method of copper alloy spectral standard sample

A spectral standard sample and copper alloy technology, which is applied in the field of preparation of copper alloy spectral standard samples

Active Publication Date: 2012-03-07
白银有色西北铜加工有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] With the rapid development of my country's economy, copper alloys are more and more widely used, especially cast silicon bronze is widely used in shipbuilding, mechanical processing, railway transportation and other industries. At the same time, product competition is more intense, and users have higher and higher requirements for product quality. , continuous improvement of detection methods, advanced chemical composition detection instruments, and the wide application of photoelectric direct reading spectrum plasma emission spectrometers have rapidly expanded the market for standard samples for spectral analysis. Currently, standard samples on the market cannot meet the requirements for use. In order to meet the needs of the market, Developed Qsi0.6-2 copper alloy standard sample, on the basis of GB / T5321-2001 product standard, added three elements (Zn, Al, Sn,) to meet market demand

Method used

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  • Preparation method of copper alloy spectral standard sample

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] The weight content of each element in the copper alloy spectral standard sample is:

[0020] Si 0.10±0.01% Ni 4.5±0.2% Fe 0.02±0.002% Pb 0.005±0.001% Mn 0.05±0.006% Sn 0.50±0.03% Al 0.040±0.01% Zn 1.50±0.1%

[0021] (1) Material preparation: Calculated by 50Kg thrown into the furnace. 37.008Kg of pure metal copper, Cu-Si (20% by weight of Si) 0.25Kg, 10.598Kg of Cu-Ni (21.23% by weight of Ni), 10.598Kg of Cu-Mn (20% by weight of Mn content of 31.58%) 0.079Kg, Cu-Fe (the weight percentage of Fe is 4.34%) 0.230Kg, Cu-Zn (the weight percentage of Zn is 49.47%) 1.516Kg, Cu-Al (the weight percentage of Al content of 32.2%) 0.062Kg, pure Pb 0.0025Kg, pure Sn 0.25Kg;

[0022] (2) Melting: High-frequency furnace is used, and the melting temperature is 1130~1170°C. After the oven, according to the proportion of each element and the degree of oxidation difficulty, the order of feeding is to add copper + charcoal first, and then add Cu-Si to dissolve→Cu-Ni to dissolve→Cu-Mn to ...

Embodiment 2

[0027] The weight content of each element in the copper alloy spectral standard sample is:

[0028] Si 0.25±0.02% Ni 1.0±0.06% Fe 0.04±0.005% Pb 0.010±0.002% Mn 0.20±0.02% Sn 0.02±0.01% Al 0.010±0.002% Zn 0.10±0.02%

[0029] Get the raw materials ready: in embodiment 2, use pure metal copper 46.09Kg, Cu-Si (the weight percent composition of Si is 20%) 0.625Kg, Cu-Ni (the weight percent composition of Ni is 21.23%) 2.355Kg, Cu -Mn (31.58% by weight of Mn) 0.317Kg, Cu-Fe (4.34% by weight of Fe) 0.461Kg, Cu-Zn (49.47% by weight of Zn) 0.101Kg, Cu-Al (the weight percentage of Al is 32.2%) 0.016Kg, pure Pb 0.005Kg, pure Sn 0.010Kg;

[0030] Melting, ingot casting, homogenization treatment and wagon steps are the same as in Example 1.

Embodiment 3

[0032] The weight content of each element in the copper alloy spectral standard sample is:

[0033] Si 0.50±0.05% Ni 2.10±0.2% Fe 0.10±0.25% Pb 0.020±0.002% Mn 0.10±0.02% Sn 0.010±0.01% Al 0.005±0.001% Zn 0.05±0.002%

[0034] Raw materials: 40.144Kg of pure metal copper, Cu-Si (20% by weight of Si) 1.25Kg, 4.946Kg of Cu-Ni (21.23% by weight of Ni), 4.946Kg of Cu-Mn (20% by weight of Mn The percentage content is 31.58%) 0.158Kg, Cu-Fe (the weight percentage of Fe is 4.34%) 1.152Kg, Cu-Zn (the weight percentage of Zn is 49.47%) 0.051Kg, Cu-Al (the weight percentage of Al is The weight percentage is 32.2%) 0.008Kg, pure Pb 0.010Kg, pure Sn 0.005Kg;

[0035] Melting, ingot casting, homogenization treatment and wagon steps are the same as in Example 1.

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Abstract

The invention discloses a preparation method of a copper alloy spectral standard sample. The copper alloy spectral standard sample comprises the following elements by weight percent: 0.09-2.50% of Si, 0.40-4.70% of Ni, 0.018-0.55% of Fe, 0.004-0.17% of Pb, 0.03-1.20% of Mn, 0.008-0.60% of Sn, 0.004-0.10% of Al and 0.04-1.60% of Zn. The preparation method comprises the following steps of: preparing materials, smelting, casting an ingot, performing homogenizing treatment and lathing the skin. The copper alloy spectral standard sample contains not only copper, but also a defined amount of Si, Ni, Pb, Fe, Mn, Zn, Al and Sn elements and can meet the requirements of the chemical composition analysis and control of the copper alloy.

Description

technical field [0001] The invention relates to a preparation method of a copper alloy spectrum standard sample, which is used for the analysis and detection of eight elements in the Qsi0.6-2 copper alloy. Background technique [0002] With the rapid development of my country's economy, copper alloys are more and more widely used, especially cast silicon bronze is widely used in shipbuilding, mechanical processing, railway transportation and other industries. At the same time, product competition is more intense, and users have higher and higher requirements for product quality. , continuous improvement of detection methods, advanced chemical composition detection instruments, and the wide application of photoelectric direct reading spectrum plasma emission spectrometers have rapidly expanded the market for standard samples for spectral analysis. Currently, standard samples on the market cannot meet the requirements for use. In order to meet the needs of the market, Developed ...

Claims

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Application Information

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IPC IPC(8): G01N1/28C22C9/00C22C9/02C22C9/04C22C9/05C22C9/06C22C9/10C22C1/03
Inventor 赵振林杨永刚赵义刘艳杨桂平李文军景卫军薛永庆任妍利
Owner 白银有色西北铜加工有限公司
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