Preparation method of carbon nano-tube/amorphous carbon/epoxy resin composite material

[0020] The preparation method of carbon nanotube / amorphous carbon / epoxy resin composite material in the present embodiment is realized according to the following steps:

[0021] 1. Place the clean quartz substrate in the middle of the quartz reaction chamber of the high-temperature furnace, then seal the quartz reaction chamber, adjust the heating program and start to heat up; during the heating process, 800mL / min of argon gas is introduced to remove the air in the reaction chamber to maintain the atmosphere Stable; when the temperature rises to 820~940℃, adjust the argon gas flow rate to 2000mL / min, and introduce hydrogen gas at 100~500mL / min, turn on the precision syringe pump, and inject dihydrogen at a concentration of 20~100mg / mL into the reaction chamber Ferrocene / dichlorobenzene carbon source reaction solution, the feed rate is 0.1~0.3mL / min, and the reaction time is 0.5~4h. Subsequently, stop feeding the ferrocene / dichlorobenzene carbon source reaction s

[0026] The preparation method of carbon nanotube / amorphous carbon / epoxy resin composite material in the present embodiment is realized according to the following steps:

[0027] 1. Place the clean quartz substrate in the middle of the quartz reaction chamber of the high-temperature furnace, then seal the quartz reaction chamber, adjust the heating program and start to heat up; during the heating process, 800mL / min of argon gas is introduced to remove the air in the reaction chamber to maintain the atmosphere Stable; when the temperature rises to 880°C, adjust the flow rate of argon to 2000mL / min, and inject 300mL / min of hydrogen, turn on the precision syringe pump, and inject ferrocene / dichlorobenzene with a concentration of 60mg / mL into the reaction chamber Carbon source reaction solution, the feed rate is 0.1mL / min, and the reaction time is 2h. Subsequently, stop feeding the ferrocene / dichlorobenzene carbon source reaction solution and turn off the hydrogen, a

[0031]The preparation method of carbon nanotube / amorphous carbon / epoxy resin composite material in the present embodiment is realized according to the following steps:

[0032] 1. Place the clean quartz substrate in the middle of the quartz reaction chamber of the high-temperature furnace, then seal the quartz reaction chamber, adjust the heating program and start to heat up; during the heating process, 800mL / min of argon gas is introduced to remove the air in the reaction chamber to maintain the atmosphere Stable; when the temperature rises to 880°C, adjust the flow rate of argon to 2000mL / min, and inject 300mL / min of hydrogen, turn on the precision syringe pump, and inject ferrocene / dichlorobenzene with a concentration of 60mg / mL into the reaction chamber Carbon source reaction solution, the feed rate is 0.1mL / min, and the reaction time is 2h. Subsequently, stop feeding the ferrocene / dichlorobenzene carbon source reaction solution and turn off the hydrogen, an