Production method for preparing polyvinyl chloride fibers for hair by melting method

A technology of polyvinyl chloride fiber and production method, applied in the direction of fiber chemical characteristics, application, wigs, etc., can solve the problems such as the decline of the use performance of PVC fiber, the migration of small molecules of processing aids, and the influence of product strength, so as to reduce shrinkage, The effect of avoiding small molecule migration and improving dimensional stability

Active Publication Date: 2015-05-13
邵阳美丽来发制品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This technology improves how well fibers made from vinyl chloride resin have reduced shrinking rates compared with traditional materials while maintain their strength properties for longer periods without losing them overtime or causing any issues like cracks that may occur when used repeatedly.

Problems solved by technology

This patents discusses two methods used commonly known techniques: wet or dry spinning processes for producing polymer materials like vinylchloride fiber. These technical problem addressed include poor properties caused by adding too much process aid when manufacturing them, resulting in decreased durability over time, increased risk of environmental pollution if released into our environment, difficulty achieving consistently high yields while maintaining desired mechanical characteristics, and potential health hazards associated with residual chemicals present on finished products made from this type of raw material.

Method used

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  • Production method for preparing polyvinyl chloride fibers for hair by melting method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] 100 parts by weight of PVC resin, 35 parts of DOP, 15 parts of DBP, 3 parts of organotin heat stabilizer, 3 parts of glyceryl monostearate and 1.5 parts of tetrakis[β-(3,5-di-tert-butyl- 4-Hydroxyphenyl) propionic acid] pentaerythritol ester was plasticized and mixed for 30 minutes, and the mixed material was plasticized, melted and spun through a screw extruder. °C, the temperature in the third zone is 188°C, the temperature in the fourth zone is 182°C, the screw speed is 20r / min, and the spinning speed is 30m / min.

[0028] The extruded PVC fiber is post-stretched, the stretching ratio is 4 times, and then the obtained fiber is treated with ether, the weight ratio of ether and PVC fiber is 9:1, the processing time is 45min, and finally the finished product is obtained after 4 times stretching PVC fibers.

[0029] After testing, the amount of plasticizer extracted with ether is 28.5%; the amount of residual plasticizer in the fiber is 4.8%, and the shrinkage rate is 4

Embodiment 2

[0031] 100 parts by weight of PVC resin, 40 parts of DOP, 20 parts of DBP, 3 parts of organotin heat stabilizer, 3 parts of glyceryl monostearate and 1.5 parts of tetrakis[β-(3,5-di-tert-butyl- 4-Hydroxyphenyl)propionic acid]pentaerythritol ester is plasticized and mixed, and the mixed material is plasticized, melted and spun through a screw extruder. The temperature of the first zone of the screw extruder is 150°C, and the temperature of the second zone is 175°C. , the temperature in the third zone is 185°C, the temperature in the fourth zone is 180°C, the screw speed is 25r / min, and the spinning speed is 35m / min.

[0032] The extruded PVC fiber was post-stretched, the stretching ratio was 5 times, and then the obtained fiber was treated with ether, the weight ratio of ether and PVC fiber was 10:1, the treatment time was 45 min, and finally stretched 5 times to obtain Finished PVC fiber.

[0033] After testing, the amount of plasticizer extracted with ether was 32.6%; the a

Embodiment 3

[0035] 100 parts by weight of PVC resin, 45 parts of DOP, 25 parts of DBP, 3 parts of organotin heat stabilizer, 3 parts of glyceryl monostearate and 1.5 parts of tetrakis[β-(3,5-di-tert-butyl- 4-Hydroxyphenyl)propionic acid]pentaerythritol ester is plasticized and mixed, and the mixed material is plasticized, melted and spun through a screw extruder. The temperature of the first zone of the screw extruder is 150°C, and the temperature of the second zone is 170°C. , the temperature in the third zone is 180°C, the temperature in the fourth zone is 175°C, the screw speed is 20r / min, and the spinning speed is 35m / min.

[0036] The extruded PVC fiber is post-stretched, the stretching ratio is 4 times, and then the obtained fiber is treated with ether, the weight ratio of ether and PVC fiber is 10:1, the treatment time is 1h, and finally the finished product is obtained after 4 times stretching PVC fibers.

[0037] After testing, the amount of plasticizer extracted with ether was

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Abstract

The invention relates to a production method for preparing polyvinyl chloride fibers for hair by a melting method, which belongs to the production field of polyvinyl chloride fibers. The production method is realized through the following steps: (1) mixing PVC resins, a plasticizer, a stabilizing agent, a lubricant, an antioxygen agent, and organic montmorillonite according to a certain proportion; (2) performing melting and spinning by a screw extruder; (3) stretching fibers spun in the step (2), processing the stretched fibers by an extraction agent, further stretching the processed fibers so as to obtain dimensionally stable PVC fibers for hair; (4) recycling the plasticizer separated by distilling residual treating liquids, and the extraction agent with a low boiling point. The residual volume of the plasticizer in the PVC fibers prepared by the production method disclosed by the invention is small, the migration of small molecules during the use of products is effectively avoided, and the contractility of the fibers is greatly lowed, so that the lustrousness of the fibers is more similar to that of human hair. The technological method is simple, the cost is saved, and continuous high-efficiency production can be realized.

Description

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Claims

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Application Information

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Owner 邵阳美丽来发制品有限公司
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