Preparing method for Reso octanoic acid manganese

[0020] Example 1

[0021] The preparation method of the granular manganese risoxanoate includes the following steps:

[0022] 1. Salt formation reaction steps

[0023] Into a 100-liter reactor with heating device, electric stirring, and thermometer.

[0024] Add 100 moles of Rexoctanoic acid, 1500 moles of water, 65 moles of manganese sulfate, and 20 moles of the initiator under stirring while heating at 70-80°C to react, reacting under stirring for 6 hours, stop heating, and complete the salt formation reaction.

[0025] 2. Crystallization and drying steps

[0026] The granular product obtained by centrifugal separation of crystals is dried in a drying box in a stainless steel drying sieve with upper and lower ventilation. After 24 hours, the obtained product is sieved to obtain a finished product with a content greater than 99%.

[0027] Example 2

[0028] The preparation method of the granular manganese risoxanoate includes the following steps:

[0029] 1. Salt formation reaction steps

[0030] Into a 100-liter reactor equipped with a heating device, electric stirring and a thermometer, put 100 moles of lesothic acid, 1500 moles of water, 65 moles of manganese sulfate, and 30 moles of initiator into a 100-liter reactor with stirring and heating at 70-80℃. The reaction was stirred for 6 hours, the heating was stopped, and the salt formation reaction was completed.

[0031] 2. Drying steps

[0032] The granular product obtained by centrifugal separation of crystals is dried in a drying box in a stainless steel drying sieve with upper and lower ventilation. After 24 hours, the obtained product is sieved to obtain a finished product with a content greater than 99%.

[0033] Example 3

[0034] The preparation method of the granular manganese risoxanoate includes the following steps:

[0035] 1. Salt formation reaction steps

[0036] Into a 100-liter reactor equipped with a heating device, electric stirring, and a thermometer, put 100 moles of lesothic acid, 1500 moles of water, 65 moles of manganese sulfate, and 35 moles of initiator into a 100-liter reaction kettle with heating at 70-80℃ under stirring. The reaction was stirred for 6 hours, the heating was stopped, and the salt formation reaction was completed.

[0037] 2. Drying steps

[0038] The granular product obtained by centrifugal separation of crystals is dried in a drying box in a stainless steel drying sieve with upper and lower ventilation. After 24 hours, the obtained product is sieved to obtain a finished product with a product content greater than 99%.