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4 results about "Tetramine" patented technology

Tetramine is a typical name for a chemical containing four amine groups. Tetramine is also used as a synonym for the tetramethylammonium cation.

Preparation method of corrosion inhibitor of methanol gasoline

The invention provides a preparation method of a corrosion inhibitor of methanol gasoline, and belongs to the technical field of metal corrosion protection. The preparation method comprises steps as follows: alpha-methylstyrene dimer, maleic anhydride, dicumyl peroxide and dimethylbenzene are added into a reactor, and then, the mixture is heated in an atmosphere of nitrogen for reacting; after the mixture is cooled to the room temperature, octadecanol, polyethylene glycol, p-toluenesulfonic acid, n-butyl alcohol and ethyl acetate are added, the mixture is heated for reacting and then cooled to the room temperature, and a mixture I is obtained; the mixture I is washed with a sulfuric acid aqueous solution, then washed with an NaOH aqueous solution and finally washed with an aqueous solution, and a mixture II is obtained; and benzotriazole, 2, 6-tert-butyl-4-methyl phenol, hexamethylene tetramine, ethanol, propargyl alcohol, trimellitate, a surface active agent and a combustion improver are added into the mixture II and uniformly stirred, and the corrosion inhibitor is obtained. The provided methanol gasoline has good solubility with various oils, the additive amount is small, and the corrosion-resistant effect is superior to that of a similar product.
Owner:南通市通州区五接农业机电管理站有限公司

Rapid analysis method for sodium hydroxide and ammonia content in sodium cyanide reaction solution and its liquid products

InactiveCN102269753AReduce consumptionAvoid interferenceChemical analysis using titrationLiquid productSodium cyanide
The invention discloses a rapid analysis method for sodium hydroxide and ammonia content in sodium cyanide reaction solution and its liquid products, which uses excess formaldehyde and ammonia to react to generate hexamethylenetetramine, and then divides into two groups of titration with hydrochloric acid, Obtain two sets of values ​​of ammonia-containing acid consumption and ammonia-removing acid consumption, and then calculate the content of sodium hydroxide and ammonia in the sample through data measurement, thereby effectively reducing the interference of free ammonia on the analysis of sodium hydroxide content, and quickly and accurately analyzing cyanide. Sodium hydroxide content and ammonia content in sodium chloride reaction liquid and its liquid products. The method of the invention is fast and effective, has obvious mutations in analysis and titration, accurate and reliable measured values, simple and convenient operation and easy mastery.
Owner:ANQING NEW SHUGUANG FINE CHEM CO LTD

Purification method of triethylene tetraamine base hexamethylene phosphonic acid

ActiveCN106380482BHigh yieldTo achieve the purpose of purifying TTHMPGroup 5/15 element organic compoundsTetramineSolvent
A method of purifying triethylene tetraamine hexamethylene phosphonic acid (TTHMP) is disclosed. The method includes dissolving a TTHMP crude product into water, adjusting the pH value by using an alkaline compound until reaching strong basicity, adding a poor solvent, allowing an oily compound to be separated from the bottom of the container, allowing the mixture to stand, collecting the oily compound, dissolving the collected oily compound with water, heating until refluxing, adding the poor solvent until a turbid phenomenon occurs, maintaining a refluxing state, adding water again until the solution is clear, stopping heating, allowing the solution to stand and be cooled, allowing an oily compound to be separated from the bottom of the container, collecting the oily compound, repeating the steps to collect the oily compound, dissolving the oily compound with water, adding an acidic compound to adjust the pH value to acidity, adding the poor solvent, allowing an oily compound to be separated from the bottom of the container, allowing the solution to stand, collecting the oily compound, washing the oily compound with a mixed solvent comprising water and the poor solvent, collecting the oily compound, and drying in a vacuum dryer to obtain white solid powder that is a purified TTHMP product. The method is used for separating impurities properties of which are similar in the TTHMP crude product. The yield of the final product is high, and purity is higher than 99%.
Owner:INST OF NUCLEAR PHYSICS & CHEM CHINA ACADEMY OF
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