Processing method for preparing imidacloprid wettable powder from crude imidacloprid

A wettable powder, processing method technology, applied in the directions of botanical equipment and methods, biocides, animal repellants, etc., can solve the problems of difficult processing of imidacloprid crude oil and high processing costs, and achieve low processing costs and simple processes. Effect

Inactive Publication Date: 2010-03-17
荆州沙隆达控股有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This technology solves problems with treating certain types of chemicals called imidazolopyridine or pyrim idoxazine that are commonly found on pesticides used for controlling insect populations. It makes it easier than traditional methods because there're only one step needed instead of two steps involved.

Problems solved by technology

The problem addressed in this patents relates to treating imidazoie acid residue (IAA) from purification processes used on industrial scale due to their negative impacts upon human body's natural environment caused by emissions or other environmental concerns associated with fossil fuel combustion products. This issue can lead to increased costs and potential hazards if treated improperly.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0007] First add 120 kg of 200-mesh white carbon black to the gravity-free mixer, then add 240 kg of 60°C imidacloprid crude oil just out of the upstream section at one time, start the mixer, and mix for 30 to 50 minutes. The imidacloprid crude oil must be added while it is hot, because when the temperature is above 50°C, it is a homogeneous oily liquid, which is conducive to the adsorption and dispersion of the crude oil by the filler. When the temperature drops to room temperature, it will gradually precipitate hard lumps, which is not conducive to subsequent processing. After being fully mixed by a gravity-free mixer, stop mixing, and add 15 kg of cleaning agent LS, 20 kg of dispersant sodium lignosulfonate, and 105 kg of kaolin into the mixer. Start the mixer and mix for 30-50 minutes. The mixed powder is sieved through a 40-mesh vibrating sieve. The sieved powder is sent to the jet mill for crushing. After passing the inspection, it is sent to the packaging.

Embodiment 2

[0009] First add 200 mesh white carbon black to the trough mixer, then add 50°C imidacloprid crude oil just out of the upstream section at one time, start the mixer, and mix for 30 to 50 minutes. The imidacloprid crude oil must be added while it is hot, because when the temperature is above 50°C, it is a homogeneous oily liquid, which is conducive to the adsorption and dispersion of the crude oil by the filler. When the temperature drops to room temperature, it will gradually precipitate hard lumps, which is not conducive to subsequent processing. After being fully mixed by the trough mixer, stop mixing, and add detergent LS, dispersant sodium lignosulfonate, and kaolin into the mixer. Start the mixer and mix for 30-50 minutes. The mixed powder is sieved through a 40-mesh vibrating sieve. The sieved powder is sent to the jet mill for crushing. After passing the inspection, it is sent to the packaging. Wherein the weight percent of each component is 10% of imidacloprid, 50% of

Embodiment 3

[0011] First add 300-mesh kaolin to the double-helix conical mixer, then add the 50°C imidacloprid crude oil just out of the upstream section at one time, start the mixer, and mix for 30-50 minutes. After being fully mixed by the double-helix conical mixer, stop mixing, and add detergent LS, sodium dodecylbenzenesulfonate, dispersant sodium lignosulfonate, diatomaceous earth, and bentonite into the mixer. Start the mixer and mix for 30-50 minutes. The mixed powder is sieved through a 40-mesh vibrating sieve. The sieved powder is sent to the jet mill for crushing. After passing the inspection, it is sent to the packaging. Wherein the weight percent of each component is 10% of imidacloprid, 40% of kaolin, 5% of detergent LS, 5% of sodium dodecylbenzenesulfonate, 5% of sodium lignosulfonate, 5% of diatomite, 30% of bentonite %.

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Abstract

The invention relates to a processing method for preparing imidacloprid wettable powder from crude imidacloprid, which comprises the following steps: (1) firstly, adding filler into a mixer; (2) pouring crude imidacloprid of 50 to 60 DEG C into the mixer, starting up the mixer, and mixing for about 30 to 50 minutes; (3) adding wetting agent, dispersing agent and stuffing bulking agent, and mixingfor 30 to 50 minutes; (4) screening the uniformly mixed materials by a vibrating screen of 40 meshes; and (5) feeding the powder after being screened to a jet mill to be grinded, wherein, the weight percent of the components are as follows: 1-25% of imidacloprid, 5-50% of filler, 1-10% of wetting agent, 1-10% of dispersing agent and 5-50% of stuffing bulking agent. The invention can effectively solve the problem that the crude imidacloprid is difficult to be treated, and has the advantages of simple process and low treatment cost.

Description

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Claims

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Application Information

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Owner 荆州沙隆达控股有限公司
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