Preparation method of cordyceps sinensis mycelium extract

A technology of Cordyceps mycelium and extract is applied in the directions of medical preparations, pharmaceutical formulations, plant raw materials, etc. containing active ingredients, which can solve the problems of discount in efficacy and difficulty in fully dissolving, and achieve high safety effects.

Inactive Publication Date: 2013-10-09
SUZHOU TIANLING CHINESE TRADITIONAL MEDICINE SLICE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because the Cordyceps contained in it is difficult to fully dissolve even

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] A preparation method of Cordyceps mycelium extract, comprising the following steps:

[0012] Dry the Cordyceps mycelium in an oven at 55°C for 10 hours in a vacuum with a vacuum degree of 0.05 MPa. After drying, pulverize and sieve through 20 meshes to make a coarse powder; add the coarse powder to a multi-functional extraction tank and add a solvent , heated to 80°C, refluxed for 2 hours, cooled to room temperature, filtered, the filtrate recovered solvent, dried in an oven at 80°C, and made into a dry paste, that is, Cordyceps mycelium extract .

Embodiment 2

[0014] A preparation method of Cordyceps mycelium extract, comprising the following steps:

[0015] Dry the Cordyceps mycelium in an oven at 60°C for 8 hours in a vacuum with a vacuum degree of 0.01MPa. After drying, pulverize and sieve through 20 meshes to make a coarse powder; add the coarse powder to a multi-functional extraction tank and add solvent , heated to 60°C, refluxed for 1.5°C, cooled to room temperature, filtered, the filtrate recovered solvent, dried in an oven at 80°C, and made into a dry paste, that is, Cordyceps mycelium extract .

Embodiment 3

[0017] A preparation method of Cordyceps mycelium extract, comprising the following steps:

[0018] Dry the Cordyceps mycelium in an oven at 58°C for 9 hours in vacuum with a vacuum degree of 0.02MPa. After drying, crush and sieve through 20 meshes to make a coarse powder; add the coarse powder to a multi-functional extraction tank and add a solvent , heated to 70°C, refluxed for 1.8h, cooled to room temperature, filtered, the filtrate recovered solvent, dried in an oven at 80°C, and made into a dry paste, that is, Cordyceps mycelium extract .

[0019] The solvent quality that embodiment 1-3 adopts is such as table 1:

[0020] Table 1

[0021] Example 1 Example 2 Example 3 tributylamine 5 7 10 ethanol 80 70 65 ethyl acetate 20 15 10 petroleum ether 10 20 15 Dry paste / Cordyceps mycelium% 23.45 25.42 24.70

[0022] Compared with the percentage of dry paste / Cordyceps mycelium, the solvent ratio of the examples

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Abstract

The invention relates to a preparation method of a cordyceps sinensis mycelium extract. The preparation method is characterized by comprising the following steps of: putting the cordyceps sinensis mycelium in an oven, and performing vacuum drying at 55-60 DEG C for 8-10 hours, wherein the vacuum degree is 0.01-0.05MPa; after the drying, crushing and screening by a 20-mesh sieve to obtain coarse powder; adding the coarse powder into a multifunctional extraction tank, and adding a solvent; heating to 60-80 DEG C, and refluxing for 1.5-2 hours; cooling to normal temperature, and filtering; recovering the solvent from the filtrate; and drying in the oven at 80 DEG C to obtain a dry paste which is the cordyceps sinensis mycelium extract. The solvent comprises the following components in parts by mass: ethyl alcohol, ethyl acetate, petroleum ether and tributylamine at a mass ratio of (60-85):(5-25):(5-25):(5-10). By adopting the method provided by the invention, the prepared cordyceps sinensis mycelium extract can be added into a Chinese medicine preparation according to the prescription percentage to prepare a preparation; and the pharmacological components of the cordyceps sinensis mycelium are uniformly dispersed and quickly dissolved out in the body to last for long time and promote sufficient absorption by the human body.

Description

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Claims

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Application Information

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Owner SUZHOU TIANLING CHINESE TRADITIONAL MEDICINE SLICE
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