Method for preparing rare-earth-waste-residue coagulant
A technology of rare earth waste residue and coagulant, which is applied in the direction of flocculation/sedimentation water/sewage treatment, etc., which can solve the problems of application limitation and high production cost.
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Embodiment 1:①7,3mol/L100ml(12g);②100℃1h;③,;④,60℃2h,;⑤,182.1NTU,pH5.5,1000ml preparation 4ml, experiment ,3.2NTU, to 98.2%。 Embodiment 2:①7,4mol/L100ml(16g);②100℃2h;③,;④,70℃2h,;⑤,176.5NTU,pH5.5,1000ml preparation 4ml, experiment ,2.7NTU, to 98.5%。 Embodiment 3
[0004] Example 1: ① Take 7 grams of dried rare earth waste residue, put it into a flask and slowly add 100ml of 3mol / L sodium hydroxide solution (that is, contain 12g of sodium hydroxide); ② Boil at 100°C Heating for 1 hour; ③ After the reaction, the mother liquor was vacuum filtered, and the filtrate was used for subsequent concentration; ④ The filtrate was placed in a water bath, heated and matured at 60°C for 2 hours, and the transparent liquid obtained was the obtained mixture. coagulant; ⑤Taking a certain coking biochemical effluent as the treatment water quality, the measured turbidity is 182.1NTU, pH5.5, take 1000ml of it and put it into the prepared coagulant 4ml, carry out coagulation experiment, measure the turbidity of the effluent after precipitation The degree is 3.2NTU, and the turbidity removal rate reaches 98.2%. Example 2: ① Take 7 grams of dried rare earth, put it into a flask and slowly add 100ml of 4mol / L sodium hydroxide solution (that is, contain 16g of s...
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