Novel anti-electrostatic ceramic glaze as well as preparation method and application thereof

An anti-static, ceramic glaze technology, applied in the field of ceramics, can solve the problems of deep color, application limitation, unstable performance, etc., and achieve the effect of good chemical stability and low price

Active Publication Date: 2018-09-28
ZHONGSHAN ADVANCED ENG & TECH RES INST WUHAN UNIV OF TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This new type of glass used for cooking utensils or other items that require anti-static properties can have an improved appearance without any unwanted foams on it's surfaces. It also prevents water from sticking out during use while still being effective at prevention against static electricity charges caused by friction between objects placed close together.

Problems solved by technology

This patented technical problem addressed in this patents relates to finding ways for making highly resistant surfaces while also having good optical transmission characteristics. Current methods involve mixing different types of ceramic material together before firing it into a final product. However, these techniques have limitations such as poor control over particle size distribution, impurities incorporated within them, difficulty controllably filling void spaces inside the resulting structure, lack of continuity across multiple layers, and slow manufacturing speeds.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Preparation of aluminum-doped zinc oxide conductive powder:

[0034] (1) Combine ZnO and Al 2 o 3 The powder is put into a ball mill jar, where Al 2 o 3 The powder is 2.5% of the total amount of powder, and the weight ratio of powder, balls and ethanol is 1:1.6:1, adding balls and ethanol solution to disperse, milling and mixing on a ball mill, and the ball milling time is 12h;

[0035] (2) Put it into a drying oven after mixing evenly, and dry it at 100°C;

[0036] (3) Put the dried mixed powder into an alumina crucible, place the crucible in a microwave continuous synthesis furnace for synthesis, the microwave power is generally 5kW, the synthesis condition is 1250°C, and the temperature is kept for 1h to obtain the conductive powder;

[0037] (4) Put the conductive powder synthesized by microwave into the ball mill tank, and grind it in the ball mill according to the weight ratio of the conductive powder and the ball at 1:2. The ball milling time is 3 hours. Zinc c

Embodiment 2

[0044] Preparation of aluminum-doped zinc oxide conductive powder:

[0045] (1) Combine ZnO and Al 2 o 3 The powder is put into a ball mill jar, where Al 2 o 3 The powder is 1.25% of the total amount of powder, and then the weight ratio of powder, balls and ethanol is 1:2:0.5, adding balls and ethanol solution to disperse, and performing ball milling on a ball mill for 15 hours;

[0046](2) Put it into a drying oven after mixing evenly, and dry it at 100°C;

[0047] (3) Put the dried mixed powder into an alumina crucible, place the crucible in a microwave continuous synthesis furnace for synthesis, the microwave power is generally selected as 3kW, the synthesis condition is 1300°C, and the temperature is kept for 0.5h to obtain the conductive powder;

[0048] (4) Put the conductive powder synthesized by microwave into the ball mill tank, and grind it in the ball mill according to the weight ratio of the conductive powder and the ball at 1:1.8. The ball milling time is 2 hours

Embodiment 3

[0055] Preparation of aluminum-doped zinc oxide conductive powder:

[0056] (1) Combine ZnO and Al 2 o 3 The powder is put into a ball mill jar, where Al 2 o 3 The powder is 2.0% of the total amount of powder, and then the weight ratio of powder, balls and ethanol is 1:1.8:0.8, adding balls and ethanol solution to disperse, performing ball milling and mixing on a ball mill, and the ball milling time is 10h;

[0057] (2) Put it into a drying oven after mixing evenly, and dry it at 100°C;

[0058] (3) Put the dried mixed powder into an alumina crucible, place the crucible in a microwave continuous synthesis furnace for synthesis, the microwave power is generally selected as 1kW, the synthesis condition is 1200°C, and the temperature is kept for 0.8h to obtain the conductive powder;

[0059] (4) Put the conductive powder synthesized by microwave into the ball mill tank, and grind it in the ball mill according to the weight ratio of the conductive powder and the ball at 1:1.6. Th

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PUM

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Abstract

The invention discloses a novel anti-electrostatic ceramic glaze as well as a preparation method and the application thereof. The preparation method comprises the following steps: carrying out continuous microwave synthesis on a common ceramic transparent glaze which mainly consists of ore materials at a temperature of 1100-1300 DEG C which is kept for 20-30 minutes, melting, directly pouring intowater for cold quenching, grinding prepared melt blocks in a ball milling tank, screening till 400 meshes so as to obtain a melt block powder, further mixing with a screened aluminum-doped zinc oxideconductive powder with150-200 meshes in a mass ratio of 20-30%, carrying out uniform ball milling mixing with 60% deionized water, at the same time adding sodium carboxymethylcellulose to regulate properties of a glaze material, so as to obtain glaze slurry, wherein the prepared glaze slurry is aged and applied to a dry ceramic blank by using a glazing method, and the glaze soaking time is 3 seconds. The ceramic blank after glaze application is dried in a drying tank, and is sintered by using a microwave continuous sintering process. The obtained ceramic glaze has the advantages of being smooth and flat in glaze surface, free of bubbles, transparent, good in chemical stability, non-toxic and environmental-friendly, low in price, and the like.

Description

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Claims

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Application Information

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Owner ZHONGSHAN ADVANCED ENG & TECH RES INST WUHAN UNIV OF TECH
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