Process for extracting lotus leaf flavone
A lotus leaf flavonoids and extraction method technology, applied in the direction of organic chemistry, etc., can solve the problems of failure to meet the requirements of extract purity and low extract purity, and achieve the effect of safe extraction method, good water solubility, and stable chemical properties
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[0018] 1. Wash with 5 kg of dried lotus leaves, air-dried and crushed to obtain lotus leaf powder;
[0019] 2. Put the lotus leaf powder into the percolation device, extract with 50-75 liters of 70%-85% ethanol, concentrate the percolate under reduced pressure to 5 liters, filter to remove the solid precipitate, and obtain a concentrated percolate;
[0020] 3. Dilute the concentrated percolate with 15-25 liters of distilled water and slowly add it to the upper end of the D140 macroporous adsorption resin column. The lower layer of the macroporous adsorption resin column contains 6-7 kg of D140 macroporous adsorption resin. Use 60-75 liters of D140 macroporous adsorption resin. Wash the macroporous adsorption resin column with distilled water, then wash the macroporous adsorption resin column with 40-60 liters of 10-15% ethanol, then wash the macroporous adsorption resin column with 40-60 liters of 40-50% ethanol, and concentrate under reduced pressure for 40-50 % Ethanol eluent to 2.
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