Preparation method of peritectic titanium alloy powder

A technology of alloy powder and titanium alloy, applied in the field of preparation of peritectic titanium alloy powder, can solve the problems of low yield of fine powder, easy hollowing, low atomization efficiency, etc., and achieves good fluidity, low price, surface smooth effect

Inactive Publication Date: 2019-12-03
江苏思睿迪快速制造科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Limited by materials and equipment, most of the atomization efficiency is relatively low, and the yield of fine powder prepared is not high
In addition, most of the atomized metal particles are blown off by inert gas, which is easy

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0022] Example 1

[0023] A preparation method of peritectic titanium alloy powder, comprising the following steps:

[0024] S1. Wash the industrial pure titanium TA1 powder and TC4 alloy powder (the mass fraction of each component is: Al: 6.0%, V: 4.5%, other impurities ≤ 0.01%, and the balance is Ti) in vacuum with pure argon gas respectively;

[0025] S2. Put 60 parts by weight of TA1 powder into a vacuum sintering furnace, and the vacuum degree is 10 -3 Pa was filled with inert argon gas, then heated to 980°C, kept for 30min for microwave smelting, put in 5.5 parts by weight of La and mixed evenly, kept for 30min, cooled to 890°C, added 30 parts by weight of TC4 alloy powder, kept for 60min, placed in the abrasive tool Medium-cooled into an alloy rod with a diameter of 60mm and a length of 500mm;

[0026] S3. Use the rotating electrode atomization method to obtain spherical powder from the alloy rod:

[0027] 1), place the alloy rod as a consumable electrode in the atomiza

Example Embodiment

[0029] Example 2

[0030] A preparation method of peritectic titanium alloy powder, comprising the following steps:

[0031] S1. Wash the industrial pure titanium TA2 powder and TC4 alloy powder (the mass fraction of each component is: Al: 6.0%, V: 4.5%, other impurities ≤ 0.01%, and the balance is Ti) in vacuum with pure argon gas respectively;

[0032] S2. Put 40 parts by weight of TA2 powder into a vacuum sintering furnace, and the vacuum degree is 10 -3 Pa was filled with inert argon gas, then heated to 980°C, kept for 30min for microwave smelting, put in La4 parts by weight and mixed evenly, kept for 30min, cooled to 890°C, added 40 parts by weight of TC4 alloy powder, kept for 60min, and cooled in an abrasive tool The alloy rod is 60mm in diameter and 500mm in length;

[0033] S3. Use the rotating electrode atomization method to obtain spherical powder from the alloy rod:

[0034] 1), place the alloy rod as a consumable electrode in the atomization equipment, and evacuat

Example Embodiment

[0036] Example 3

[0037] A preparation method of peritectic titanium alloy powder, comprising the following steps:

[0038] S1. Wash the industrial pure titanium TA3 powder and TC4 alloy powder (the mass fraction of each component is: Al: 6.0%, V: 4.5%, other impurities ≤ 0.01%, and the balance is Ti) in vacuum with pure argon gas respectively;

[0039] S2, put 20 parts by weight of TA3 powder into a vacuum sintering furnace, and the vacuum degree is 10 -3 Pa was filled with inert argon gas, then heated to 980°C, kept for 30min for microwave smelting, poured into La1 parts by weight and mixed evenly, kept for 30min, cooled to 890°C, added 50 parts by weight of TC4 alloy powder, kept for 60min, and cooled in an abrasive tool The alloy rod is 60mm in diameter and 500mm in length;

[0040] S3. Use the rotating electrode atomization method to obtain spherical powder from the alloy rod:

[0041] 1) Place the alloy rod as a consumable electrode in the atomization equipment, and vac

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Abstract

The invention discloses a preparation method of peritectic titanium alloy powder. The preparation method comprises the steps that CP titanium powder and TC4 alloy powder are washed with pure argon invacuum; then the CP titanium powder, the La alloy powder and the TC4 alloy powder are sequentially put into a vacuum sintering furnace to be smelted to obtain alloy bars, and finally the alloy bars are subjected to a rotary electrode atomization method to obtain spherical powder. The prepared powder is low in hollow rate, good in fluidity and suitable for 3D printing.

Description

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Claims

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Application Information

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Owner 江苏思睿迪快速制造科技有限公司
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