Preparation method of bionic carbon negative electrode material used as potassium ion battery negative electrode, and product
A negative electrode material and battery negative electrode technology, applied in the field of biomimetic carbon and its preparation, can solve the problems of insufficient rate performance and fast charge/discharge characteristics, and achieve excellent electrochemical performance, high reversible capacity, and excellent rate performance.
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[0041]Example 1
[0042]Such asfigure 1 As shown, first of all, a nitrogen-carbon compound (C3N4) Intermediate: Put 15mg of melamine precursor in a porcelain boat and put it in a muffle tube furnace at 2℃min-1The heating rate is heated to 550°C and kept at a constant temperature for 5 hours, and then naturally cooled to room temperature to obtain C3N4;
[0043]Secondly, cobalt (Co) catalyst catalyzes high-temperature carbonization treatment: Use an agate mortar to remove C3N4Grind into fine powder, then mix with metal Co at a mass ratio of 1:1, and then mix thoroughly in an agate mortar; put it in a porcelain boat after mixing evenly, and heat it at 2℃ in a tube furnace with an argon atmosphere min-1The rate of heating up to 800 ℃, and constant temperature heating treatment at this temperature for 2h, and then natural cooling to room temperature;
[0044]Finally, acid treatment to remove the metal catalyst; repeated washing with 2mol / L hydrochloric acid (HCl) solution to remove Co, and then r
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