Device and method for synthesizing organic matters from methanol under assistance of plasma electric field

[0096] Example 1

[0097] Such as figure 1 The plasma electric field assisted methanol produces an organic substance, the apparatus including: the apparatus body 117 and a plasma electric field unit disposed within the apparatus body 117, the apparatus body 117 is a metal barrel, a plasma electric field unit including the first electric field reaction chamber and The electric field type in the second electric field reaction chamber, the first electric field reaction chamber, and the second electric field reaction chamber can be adjusted according to the actual production needs.

[0098] figure 1 In the middle, the first electric field reaction chamber is a pure stainless steel tube reaction chamber 118, and the second electric field reaction chamber is an outer stainless steel tube additional liner glass tube double-layer reaction chamber 111. Among them, the stainless steel tube reaction chamber can be used with one or two parallel stainless steel tubes (not shown in the figure), t

[0104] Example 2

[0105] A method of assisted methanol synthesis organic matter using the plasma electric field of Example 1, including the following steps: three tandem devices, with molar ratio 1: 1 methanol gas and water vapor as a raw material gas, the raw material gas first enters the first device The first electric field (i.e., the high frequency pulse is 10 km of high voltage electric field, the high frequency pulse is 10 kHz, voltage 10-20 kV), 115 degree temperature parts, the raw material gas is decomposed in the positive electric field to obtain a mixed ionized gas, mixed The second electric field (i.e., high-voltage DC negative electric field, voltage 10-20 kV) in the ionized gas access device, and then sequentially enters the second device, third device, repeats the operation in the first device. Get the final product.

[0106] During the preparation process, the temperature of decomposition and synthesis is 115 ° C.

[0107] After GCMS test (such as figure 2 As shown,

[0108] Example 3

[0109] Example 3-1 to Examples 3-6 The apparatus employed is the same as in Example 1, but no first electric field is opened in Examples 3-1 to Examples 3-5, and the first paragraph in Example 3-6 Electric field "High Frequency Positive Electric Field (Table 1)" is a high-frequency high voltage positive electric field. The second segment of the electric field "DC negative electric field (Table 1)" in each embodiment is high voltage DC negative electric field. The main composition of the raw material gas, electric field conditions, and the product of each embodiment is shown in Table 1.

[0110] Table 1

[0111]

[0112] After GCMS test (such as image 3 As shown in the mixture obtained in Example 3-1, 31 wt% ethanol, 62 wt% methanol, and 4 wt% other substances (ethyl acetate, toluene, and methylcarboxydehyde) were contained.

[0113] After GCMS test (such as Figure 4 As shown in the mixture obtained by Example 3-5, 65 wt% ethanol, 30 wt% methanol and 2 wt% other s