Core-shell structure powder for SiC single crystal growth and preparation process of core-shell structure powder
A core-shell structure and preparation process technology, applied in the field of SiC powder, can solve the problems of uneven heating, carbon-rich tendency of powder, etc., to avoid sintering, accelerate sublimation, and achieve the effect of isolation
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[0027] The technical solutions of the present invention will be described in detail below in conjunction with specific embodiments.
[0028] A core-shell structure powder for SiC single crystal growth, the powder includes a core, an intermediate layer and a shell, the core is a SiC-Si mixed powder of Si particles with a large particle size and SiC particles with a small particle size, the The middle layer is SiC powder with a large particle size, the outer shell is carbon-rich SiC powder, and the carbon-rich SiC powder in the outer shell is obtained by heating SiC powder at 2000°C to 2400°C in a graphite crucible.
[0029] The powder applied in the present invention is used in the preparation of silicon carbide single crystal by PVT method, and its core, middle layer and shell structure fully utilize the composition and structure of different layer powders, so that in the early stage of growth and the middle and late stages of growth, the powder Both can avoid sintering phenomeno
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