Core-shell structure powder for SiC single crystal growth and preparation process of core-shell structure powder

A core-shell structure and preparation process technology, applied in the field of SiC powder, can solve the problems of uneven heating, carbon-rich tendency of powder, etc., to avoid sintering, accelerate sublimation, and achieve the effect of isolation

Inactive Publication Date: 2021-10-08
中科汇通(内蒙古)投资控股有限公司
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  • Application Information

AI Technical Summary

Benefits of technology

This patented technology describes how an improved way to prepare silicon dioxides (SIC) by growing them upwardly within layers made of materials like quartz or ceramic called clathrates. By mixing these raw material together, we aim to efficiently separate certain parts while ensuring their desired properties such as conductivity. Additionally, this technology allows us to control the amount of silica added based upon factors like purity requirements. Overall, this new approach improves efficiency and quality in producing SIC products.

Problems solved by technology

This patented technical solution describes how to improve the performance and yield of producing siliconcarbon monocrystals through thermal decomposition techniques called pyroclotting. However, current processes often result in particles being stuck together when trying to separate them from each other after cool down. To solve this issue, there has been proposed various ways to create special structures within the SiC material without burning out any remaining parts like metal atoms.

Method used

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Embodiment Construction

[0027] The technical solutions of the present invention will be described in detail below in conjunction with specific embodiments.

[0028] A core-shell structure powder for SiC single crystal growth, the powder includes a core, an intermediate layer and a shell, the core is a SiC-Si mixed powder of Si particles with a large particle size and SiC particles with a small particle size, the The middle layer is SiC powder with a large particle size, the outer shell is carbon-rich SiC powder, and the carbon-rich SiC powder in the outer shell is obtained by heating SiC powder at 2000°C to 2400°C in a graphite crucible.

[0029] The powder applied in the present invention is used in the preparation of silicon carbide single crystal by PVT method, and its core, middle layer and shell structure fully utilize the composition and structure of different layer powders, so that in the early stage of growth and the middle and late stages of growth, the powder Both can avoid sintering phenomeno

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Abstract

The invention provides core-shell structure powder for SiC single crystal growth and a preparation process of the core-shell structure powder. The powder comprises a core, a middle layer and a shell, wherein the core is SiC-Si mixed powder of large-particle-size Si particles and small-particle-size SiC particles, the middle layer is large-particle-size SiC powder, the shell is carbon-rich SiC powder, and the carbon-rich SiC powder of the shell is obtained by heating SiC powder in a graphite crucible at a temperature of 2000-2400 DEG C. According to the invention, when a silicon carbide single crystal is prepared by adopting a physical vapor transport method, the core-shell structure powder disclosed by the invention can realize effective isolation of different powder silicon carbide particles, and can realize reasonable adjustment of carbon and silicon components in different heating sublimation stages, so that the problems of sintering and non-uniform heating in the heating sublimation process of the existing silicon carbide powder are effectively improved, and finally, high-quality silicon carbide single crystals can be obtained.

Description

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Claims

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Application Information

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Owner 中科汇通(内蒙古)投资控股有限公司
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