Anti-sublimation silica gel printing coating and preparation method thereof

A technology of silica gel and printing, applied in dyeing, textile and papermaking, etc., can solve the problems of unfavorable printing color effectively, insufficient transparency, dark color, etc., achieve uniform and effective adsorption, increase adsorption effect, and good transparency.

Pending Publication Date: 2022-03-25
广东省良展有机硅科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the anti-sublimation primer using carbon adsorption is darker in color, which is not conducive to the effective presentation of printing colors; when other anti-sublimation agents with lighter colors are used, there are problems of insufficient transparency or poor adsorption effect, which cannot meet the application requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0035] The preparation method includes the following steps:

[0036] Step 1, prepare anti-lifting base silica gel: Ethylene polysiloxane, orthosilicate and n-heptane are prepared in a mixture of 500-1000 rpm rotational speeds of 15-30 min, and mix evenly, add deionized water. The mixture was continued for 5-10 min to give a mixed solution, and the mixed solution was placed in a pressure-resistant hydrothermal reaction kettle, and the reaction was reacted at 120-150 ° C for 8-10 h to obtain a lifted base silicone;

[0037] Step 2, prepare a component: Add white carbon black and platinum catalyst to the anti-lifting base silica gel, uniformly dispersed by the planetary mixer, and remove the residual n-heptane and deionized water at a temperature of from 100 to 10 ° C. A component;

[0038] Step 3: Preparation of B components: Silicone oil and inhibitors are uniformly dispersed in a mixer of 500-1000 rpm to 5-10 min to obtain B components;

[0039] Step 4: Preparation of anti-lifting...

Embodiment 1

[0044] This example uses a method of preventing subtilizing silica gel printing coatings, which is prepared for the preparation of anti-lifting silicone printing coatings;

[0045] The preparation method includes the following steps:

[0046] Step 1: Preparation of anti-lifting base silica gel: 100 parts of the two-terminal vinyl polymethylsiloxane, 5 parts of n-silicate and 10 parts of n-heptane are uniformly dispersed in a mixer of 500 rpm rotational speeds 30 min, and mix Uniform, then 0.05 parts of deionized water, continued for 10 min to obtain a mixed solution, and the mixed solution was placed in a pressure-resistant hydrothermal reaction kettle, and the reaction was reacted at 120 ° C for 8 h, resulting in anti-lifting base silica gel; wherein said The viscosity of the double-end vinyl polymethylsiloxane is 1000 mPa · s, and the vinyl content is 0.2%;

[0047] Step 2, prepare a component: 10 parts of the surface-treated gas phase method white charcoal black and 0.9 parts of ...

Embodiment 2

[0052] This example uses a method of preventing subtilizing silica gel printing coatings, which is prepared for the preparation of anti-lifting silicone printing coatings;

[0053] The preparation method includes the following steps:

[0054] Step 1: Preparation of anti-lifting base silica gel: 100 parts of the two-end polyimethylsiloxane, 15 parts of n-silicate and 15 n-heptane in the mixer of 500 rpm rotational speed 30 min, both mix Uniform, then 0.08 parts of deionized water, continued for 5 min to give a mixed solution, and the mixed solution was placed in a pressure-resistant hydrothermal reaction kettle, and the reaction was reacted at 120 ° C for 8 h, resulting in anti-lifting base silica gel; wherein said The viscosity of double-end vinyl polymethylsiloxane is 2000 MPa · S, and the vinyl content is 0.18%;

[0055] Step 2, prepare a component: add 5 partially treated gas phases to the anti-lifting base silica gel and 0.9 parts of H. 2 PTC l6 The isopropyl alcohol solution ...

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Abstract

The invention discloses an anti-sublimation silica gel printing coating. The anti-sublimation silica gel printing coating is composed of a component A and a component B according to the mass ratio of 10: 1.5-10: 0.6, wherein the component A is prepared from the following components in parts by mass: 100 parts of vinyl polysiloxane, 0.05 to 0.1 part of deionized water, 5 to 30 parts of tetraethoxysilane, 10 to 15 parts of n-heptane, 5 to 10 parts of white carbon black and 0.9 to 1.5 parts of platinum catalyst; the component B is prepared from the following components in parts by weight: 100 parts of hydrogen-containing silicone oil and 5-10 parts of an inhibitor; the invention further discloses a preparation method of the anti-sublimation silica gel printing coating. According to the silica gel printing paste and the preparation method thereof, by adopting an in-situ dispersed distribution nano filling technology, anti-sublimation nano-particles are introduced into the silica gel printing paste, the particles hardly influence the original performance of the silica gel paste, and meanwhile, the approximate transparent and anti-sublimation effects can be achieved.

Description

Technical field [0001] The present invention relates to the technical field of wire mesh silica printing, and more particularly to anti-lifting silica gel printing coatings and preparation methods thereof. Background technique [0002] In the field of textile printing, the dyes or pigments used on Dark T-shirts, swimsuits, children's wear, bags, tents, etc. are prone to sublimation and migrated to glue or silica gel printing surface, which makes printed to be contaminated and lost the original color. It has caused the printing product to be unqualified and even scrapped. Since the process often occurs after the production of product production, it is difficult to repair and make up. Once the above situation, the company's loss is large. [0003] The sublimation of dyes or pigments is mainly related to molecular movement at high temperatures. When the dye or pigment is poor, it occurs at high temperatures, when printed glue or silica gel, if there is a gap between the printed laye...

Claims

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Application Information

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IPC IPC(8): D06P1/52D06P1/673
CPCD06P1/5292D06P1/67383
Inventor 王志良
Owner 广东省良展有机硅科技有限公司
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