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3 results about "Photocatalytic decomposition" patented technology

The photocatalytic decomposition of AcOH was carried out in a circulation system made of Pyrex, in which a suspension of the photocatalyst powder (200 mg) in an aerated aqueous AcOH solution (5 vol%, 300 mL) was continuously stirred using a magnetic stirrer.

NiCoP nanoparticles grown on surface of g-C3N4 in situ as well as preparation method and application of NiCoP nanoparticles

InactiveCN107617443ASimple and fast manufacturing methodEasy to operatePhysical/chemical process catalystsHydrogen productionHydrogenNanoparticle
The invention provides NiCoP nanoparticles grown on the surface of g-C3N4 in situ as well as a preparation method and application of the NiCoP nanoparticles to production of hydrogen by photocatalytically decomposing water, and belongs to the technical field of photocatalytic decomposition of the water to prepare the hydrogen. The preparation method comprises the following steps: firstly, preparing g-C3N4powder particles; then adding 10mL to 30mL of secondary distilled water into 200mg to 400mg of the g-C3N4 powder particles; after carrying out ultrasonic treatment for 1h to 3h, stirring for 1h to 3h; then adding 10mg to 150mg of a nickel source and 10mg to 150mg of a cobalt source; after carrying out the ultrasonic treatment for 5min to 20min, stirring for 5min to 20min; then adding 50mgto 600mg of a phosphorous source; after carrying out the ultrasonic treatment for 1h to 3h, stirring for 1h to 3h; then drying under the condition that the temperature is 50 DEG C to 80 DEG C; after the water is completely volatilized, sufficiently grinding a product; then calcining for 1h to 3h in a nitrogen atmosphere under the condition that the temperature is 200 DEG C to 400 DEG C; finally, centrifuging and washing by utilizing the secondary distilled water and ethanol; drying a centrifugal product for 10h to 20h under a vacuum condition, so as to obtain the NiCoP nanoparticles grown on the surface of the g-C3N4 in situ.
Owner:JILIN UNIV

Silver sulfide/tungsten trioxide-based z-type photocatalytic material as well as preparation method and application thereof

ActiveCN109926068AShorten the migration pathReduce chance of recombinationPhysical/chemical process catalystsHydrogen productionMaterials preparationPhoto catalytic
The invention relates to the technical field of nano photocatalytic material preparation and hydrogen production application thereof, and in particular relates to a silver sulfide/tungsten trioxide-based z-type photocatalytic material as well as a preparation method and application thereof, the silver sulfide/tungsten trioxide-based z-type photocatalytic material has a zero-dimensional/one-dimensional composite structure, the zero-dimensional structure is silver sulfide nano-particles, the one-dimensional structure is a tungsten trioxide nanorod, and the silver sulfide nano-particles are dispersed on the surface of the tungsten trioxide nanorod. WO3 and Ag2s are respectively provided with one-dimensional and zero-dimensional structures, and the migration path of photogenerated charges canbe shortened, so that the photogenerated charges are rapidly transferred to the surface of the material, and the composite probability of photogenerated carriers in a material body phase is reduced; the photogenerated charge transfer mode between Ag2SNPs and WO3NRs follows a z-type photo-catalytic charge transfer mechanism, while the photogenerated charge oxidation reduction capability is maintained, the separation efficiency of the photongenerated carriers is further improved, and the silver sulfide/tungsten trioxide-based z-type photocatalytic material has better performance of photocatalytic water decomposition for hydrogen production.
Owner:WUHAN UNIV
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