Oxygen carrier composition and preparation method thereof
一种组合物、载氧体的技术,应用在石油工业、燃料添加剂、燃料等方向,能够解决载氧量低、释放和吸收氧效果差等问题,达到提高稳定性、提升载氧量、提升载体活性的效果
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Embodiment 1
[0022] A preparation method of an oxygen carrier composition, comprising the steps of:
[0023] Step 1, add aluminum hydroxide to absolute ethanol (1L), stir evenly, then add polyvinylpyrrolidone and ultrasonically disperse completely at low temperature to obtain a uniform dispersion; the concentration of aluminum hydroxide in absolute ethanol is 100g / L , the stirring speed is 1000r / min, the addition of the polyvinylpyrrolidone is 30% of the mass of aluminum hydroxide, the temperature of low-temperature ultrasonic dispersion is 20°C, and the ultrasonic frequency is 50kHz,
[0024] Step 2: Add the uniform dispersion liquid into the mold for constant temperature extrusion, then soak it in absolute ethanol, stir evenly, and dry to obtain a porous body. The temperature of the constant temperature extrusion is 80°C, the pressure is 2MPa, and the uniform stirring The speed is 1000r / min, the drying temperature is 80°C, and the particle size of the porous body particles is 3mm;
[00...
Embodiment 2
[0032] A preparation method of an oxygen carrier composition, comprising the steps of:
[0033] Step 1, add aluminum hydroxide to absolute ethanol (1L), stir evenly, then add polyvinylpyrrolidone and ultrasonically disperse completely at low temperature to obtain a uniform dispersion; the concentration of aluminum hydroxide in absolute ethanol is 200g / L , the stirring speed is 2000r / min, the addition of the polyvinylpyrrolidone is 40% of the mass of aluminum hydroxide, the temperature of low-temperature ultrasonic dispersion is 30°C, and the ultrasonic frequency is 90kHz,
[0034] Step 2: Add the uniform dispersion liquid into the mold for constant temperature extrusion, then soak it in anhydrous ethanol, stir evenly, and dry to obtain a porous body. The speed is 2000r / min, the drying temperature is 100°C, and the particle size of the porous body particles is 10mm;
[0035] Step 3, adding n-butyl titanate to absolute ethanol (1L) and stirring evenly to form a titanium alcohol...
Embodiment 3
[0041] A preparation method of an oxygen carrier composition, comprising the steps of:
[0042] Step 1, add aluminum hydroxide to absolute ethanol (1L), stir evenly, then add polyvinylpyrrolidone and ultrasonically disperse completely at low temperature to obtain a uniform dispersion; the concentration of aluminum hydroxide in absolute ethanol is 150g / L , the stirring speed is 1500r / min, the addition of the polyvinylpyrrolidone is 35% of the mass of aluminum hydroxide, the temperature of low-temperature ultrasonic dispersion is 25°C, and the ultrasonic frequency is 70kHz,
[0043] Step 2: Add the uniform dispersion liquid into the mold for constant temperature extrusion, then soak it in absolute ethanol, stir evenly, and dry to obtain a porous body. The speed is 1500r / min, the drying temperature is 90°C, and the particle size of the porous body particles is 7mm;
[0044] Step 3, adding n-butyl titanate to absolute ethanol (1L) and stirring evenly to form a titanium alcohol so...
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