High-bonding-strength conductive adhesive for repairable microelectronic assembly and preparation method thereof

A technology of microelectronics and conductive adhesives, applied in the direction of conductive adhesives, adhesives, epoxy resin glue, etc., can solve the problems of poor bonding strength, irremovable repair, poor conductivity of conductive adhesives, etc., and achieve excellent electrical properties Effect

Inactive Publication Date: 2021-04-23
CHINA ZHENHUA GRP YUNKE ELECTRONICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology allows for better performance when connecting components together with solder or other materials that are sensitive to high temperatures such as those found on computer chips during manufacturing processes.

Problems solved by technology

This patented technical problem addressed by this patents relates to improving the quality and reliance for joining electrically active devices together during manufacturing processes due to their small sizes and strict requirements such as being able to connect at various types of surfaces without damaging them while maintaining stable connections over time under severe conditions like extreme temperatures and moisture environments.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] The resin is 20%-30%, the conductive filler is 60%-80%, the curing agent is 4%-8%, the active diluent is 1%-2%, and the additive is 1% %~5%.

[0041] The raw materials of the resin are composed by weight percentage: the bisphenol A epoxy resin is 40%-60%; the bisphenol F epoxy resin is 40%-60%.

[0042] The raw materials of the conductive filler are composed by weight percentage: the flaky silver powder is 60%-80%; the spherical silver powder is 20%-40%.

[0043] The raw material of the curing agent is composed of 10% to 20% of the 2-ethyl-4-methylimidazole; the 1-cyanoethyl-2-ethyl-4-methylimidazole 30% to 60%; the polyetheramine 400 is 5% to 10%; the triethanolamine is 30% to 60%.

[0044] The active diluent raw material is composed by weight percentage: the polyethylene glycol diglycidyl ether is 30%-50%; the polypropylene alcohol diglycidyl ether is 50%-70%.

[0045] The additive is polyamide wax.

Embodiment 2

[0047] The resin is 30%, the conductive filler is 60%, the curing agent is 8%, the reactive diluent is 1%, and the additive is 1%.

[0048] The raw materials of the resin are composed by weight percentage: 50% of bisphenol A epoxy resin and 50% of bisphenol F epoxy resin.

[0049] The raw materials of the conductive filler are composed by weight percentage: 50% of flake silver powder (particle size 10-20um) and 50% of spherical silver powder (particle size 3-8um).

[0050] The curing agent raw material is composed of 20% of 2-ethyl-4-methylimidazole, 50% of 1-cyanoethyl-2-ethyl-4-methylimidazole, 10% of polyetheramine 400, Triethanolamine 20%.

[0051] The active diluent raw material is composed of 60% of polyethylene glycol diglycidyl ether and 40% of polypropylene glycol diglycidyl ether by weight percentage.

[0052] The additive is polyamide wax added according to 100%.

[0053] Accurately weigh according to the ratio of the above raw materials, mix 2-ethyl-4-methylimidazo

Embodiment 3

[0057] The resin is 20%, the conductive filler is 70%, the curing agent is 6%, the reactive diluent is 2%, and the additive is 2%.

[0058] The raw materials of the resin are composed by weight percentage: 50% of bisphenol A epoxy resin and 50% of bisphenol F epoxy resin.

[0059] The raw materials of the conductive filler are composed by weight percentage: 50% of flake silver powder (particle size 10-20um) and 50% of spherical silver powder (particle size 3-8um).

[0060] The curing agent raw material is composed of 20% of 2-ethyl-4-methylimidazole, 50% of 1-cyanoethyl-2-ethyl-4-methylimidazole, 10% of polyetheramine 400, Triethanolamine 20%.

[0061] The active diluent raw material is composed of 60% of polyethylene glycol diglycidyl ether and 40% of polypropylene glycol diglycidyl ether by weight percentage.

[0062] The additive is polyamide wax added according to 100%.

[0063] Accurately weigh according to the ratio of the above raw materials, mix 2-ethyl-4-methylimidazole

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Abstract

The invention relates to a high-bonding-strength conductive adhesive for repairable microelectronic assembly and a preparation method thereof. The high-bonding-strength conductive adhesive comprises the following raw materials in percentage by weight: resin, conductive filler, a curing agent, an active diluent and an additive, wherein the resin is prepared from the following raw materials in percentage by weight: bisphenol A epoxy resin and bisphenol F epoxy resin; the conductive filler is prepared from the following raw materials in percentage by weight: flake silver powder and spherical silver powder; the curing agent is prepared from the following raw materials in percentage by weight: 2-ethyl-4-methylimidazole, 1-cyanoethyl-2-ethyl-4-methylimidazole, polyether amine 400 and triethanolamine; the reactive diluent is prepared from the following raw materials in percentage by weight: polyethylene glycol diglycidyl ether and polypropylene glycol diglycidyl ether; and the additive is a substance capable of achieving a thickening effect. The problems that an existing conductive adhesive is poor in conductivity, poor in bonding strength, incapable of being detached and repaired after bonding and the like are solved. The adhesive is widely applied to bonding materials for circuit connection of electronic components.

Description

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Claims

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Application Information

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Owner CHINA ZHENHUA GRP YUNKE ELECTRONICS
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