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8 results about "Iodine" patented technology

Iodine is a chemical element with the symbol I and atomic number 53. The heaviest of the stable halogens, it exists as a lustrous, purple-black non-metallic solid at standard conditions that melts to form a deep violet liquid at 114 degrees Celsius, and boils to a violet gas at 184 degrees Celsius. The element was discovered by the French chemist Bernard Courtois in 1811. It was named two years later by Joseph Louis Gay-Lussac from this property, after the Greek ἰώδης "violet-coloured".

Method for preparing 2-iodine amyl -2-ene-1,4-diketone derivative by adopting visible light catalysis

The invention discloses a method for preparing a 2-iodine amyl -2-ene-1,4-diketone derivative by adopting visible light catalysis. The method comprises the steps of adding allene, perfluorobutyl iodide, an additive and a photocatalyst as shown in a formula (I) to an organic solvent at the molar ratio of 1:(1-2):(1-2):(0.005-0.1), stirring under the conditions of an oxygen atmosphere, visible light illumination, room temperature and ordinary pressure for 10-20h, carrying out post-treatment on a reaction liquid to obtain a 2-iodine amyl -2-ene-1,4-diketone derivative as shown in a formula (II), wherein the additive is NaI, NH4I or KI; the organic solvent is ethanol, dichloromethane, benzene, methylbenzene, tetrahydrofuran or acetonitrile; the photocatalyst is selected from one of the following components: Ir(ppy)3, Eosin Y, Rose Bengal, [Ir(dF-CF3-ppy)2(dtbbpy)]PF6, [Ir(ppy)2(tbbpy)]PF6, Ru(bpy)3(BF4)2. The method is mild in reaction condition, simple in operation, high in selectivity and good in yield; a substituent group can be expanded; and visible light catalysis is adopted, so that the method has the characteristics of being free of pollution and environment-friendly. The formulas are as shown in the specification.
Owner:ZHEJIANG UNIV OF TECH

Method for recovering gold from printed circuit board of waste mobile phone

ActiveCN108642289AImprove adsorption efficiencyAchieve reuseOther chemical processesProcess efficiency improvementElectrolysisResource utilization
The invention provides a method for recovering gold from a printed circuit board of a waste mobile phone. The method comprises the following steps that the gold in a gold leaching liquid of the printed circuit board of the waste mobile phone is adsorbed by adopting an adsorbent so as to obtain gold-loaded carbon, wherein the adsorbent is selected from biochar or iodine-loaded biochar; and the gold-loaded carbon is subjected to desorption, and then a desorption solution is electrolyzed so as to obtain the gold. According to the method, after gold leaching is carried out on the printed circuit board of the waste mobile phone, the iodine-loaded biochar is adopted for adsorption, liquid gold is concentrated, then the gold can be recovered through electrolysis, meanwhile, the gold leaching liquid (iodine) can be recovered, so that the production cost can be lowered, and the resource utilization efficiency can be improved; modification is carried out on the biochar by using an ethanol solution of iodine so as to prepare the iodine-loaded carbon, so that the gold adsorption efficiency can be improved, and meanwhile, the utilization rate of the iodine can be increased; and the biochar prepared from agricultural waste is used for adsorbing the gold, so that the waste can be recycled, the production cost can be lowered, and the energy consumption can be reduced.
Owner:NANKAI UNIV

Preparation method of biodegradable fallout radioactive material for treating cancer

InactiveCN101417135AConcentration control of radioactive substancesLow priceRadioactive preparation carriersAntineoplastic agentsBiocompatibility TestingAminolysis
The invention belongs to the technical field of polymer material and the field of biomedical engineering, in particular relates to a preparation method for a biodegradable radioactive particle used for curing cancer. The method comprises the following detailed steps: the basic material of the radioactive particle with the needed shape is prepared by using a macromolecular biodegradable material with excellent biocompatibility according to demands; the obtained basic material of the radioactive particle is put into a 0.1 to 0.4mol/l surface modified liquid for dipping and generating aminolysis and carrying out grafting reaction; purified water is used for washing the grafted basic material for removing dissociative functional groups; the obtained basic material is put into a coupling agent liquid to dip for 1 to 2 hours and then is coupled; the obtained basic material is put into the liquid to dip for 12 to 24 hours and then washed to remove the dissociative functional groups; a radioactive isotope is used for replacing the iodine element in the basic material obtained by step (4); and a decoration film is collocated into a liquid and is coated on the surface of the basic material, thus obtaining the needed product. The degradation product is innoxious and harmless, and can be discharged outside the body by metabolism. The preparation method is simple and low in cost.
Owner:TONGJI UNIV
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